进行实验

This paper designs four simulation experiments to verify the CSAPFBA algorithm, and the results of the four simulation experiments are given. This paper lengthways compares the CSAPFBA algorithm with the CSFQ algorithm and breadthwise compares the CSAPFBA algorithm with the CSPAFA algorithm so as to analyze the performance of the CSAPFBA algorithm from the theoretical and experimental aspects.

本文设计了4组模拟实验验证CSAPFBA算法并且给出了模拟实验结果，将CSAPFBA算法分别和CSFQ算法、CSPAFA算法进行了纵向比较、横向比较以便从理论和实验两个方面分析CSAPFBA算法的性能。

Preparation of the cathode includes:shaping under the press of 40Mpa, sintering at 550℃for 1 hour and at 900℃for 8 hours and threading with molybdenum bar; Considering the literatures we choose CaCl2 as salt for preparation titanium. Pretreatment of salt is for 1 hour at 100℃and for 2 hours at 300℃. Partial pressure of oxygen which need lower than 5.11×10-7Pa to reduct titanium oxides and hygroscopic property of salt need a sealed equipment to electrolyse. And finally successfully designed a satisfied one and the results show that the equipment can be satisfied the requirment of the experiment. Flow of the inert gas is 1.5L/min, the voltage is 2.8 V, temperature is 850℃and time is 2 hours during pre-electrolysis. Flow of the inert gas is 0.2L/min, the voltage is 3.1 V, temperature is 900℃and time changes with the mass of TiO2 during electrolysis, namely the greater need the longer time; To eliminate influence of salt and other impurities, the products need to wash with distilled water and dilute chlorhydric acid , then wash with dilute hydrochloric acid under supersonic wave assistant. Finally, electrometical properties of the electrolysis of TiO2 is researched by cyclic voltammetry and chronoamperometry, and results show that there are two main reodox steps, namely from TiO2 to TiO and from TiO to Ti.

阴极制备主要包括40MPa压力下模压成型、两段式烧结(1小时内升至550℃保温1小时，再1小时升温至900℃保温8小时)及烧结后TiO2块打孔用钼棒串接三个主要环节；实验中选用CaCl2作为电解熔盐，并对其进行预处理(100℃，保温1小时； 300℃，保温2小时)；经热力学计算，还原钛氧化物的氧分压至少要低于5.11×10-7Pa，结合电解过程中所用熔盐CaCl2有极强的吸水性的特点，电解装置应有较高的密封性，自行设计了一套密封性可靠的电解装置，便于实验过程中熔盐预处理和氧分压的控制；通过干燥处理预电解过程中Ar流量大约为1.5L/min、电压为2.8 V、温度为850℃、时间为2小时，电解过程中Ar流量大约为0.2L/min、电压为3.1V、温度为900℃，实验结果表明电解时间与TiO2质量密切相关，质量越大需要电解的时间越长；通过自来水冲洗—稀盐酸浸泡、洗涤—在超声波辅助作用下稀盐酸洗涤，可减少熔盐及其它杂质对电解产物检测结果的影响；最后，通过循环伏安法、计时电流法对电解机理的研究，确定电解还原TiO2制备金属钛主要经历了TiO2-TiO-Ti的过程。

On the basis of previously research, this paper re-probe into the mechanism of electro-chemist mechanical manufacturing process, making the rational technological parameter, and developing the manufacturing equipment. Through a lot of technology tests, get a lot of labratory data, accordingly, researched the surface feature of the electro-chemist manufacturing process, and deeply discussed its influence on the work piece feature. The last result is that: the electro-chemist mechanical manufacturing process can reduce the low-frequency component significantly, but on high-frequency component, it has little influence, having obviously positive pole flat effect. After manufacture, the tip parts on the surface of the work piece is cut off, there is micro "high land" shape, the parameter for surface roughness is reduced a lot, the surface outline of the work piece is negative, the bearing length rate is cliffy. Also the surface quality of the work piece is improved. This can help to avoid changing the shape, improve the feature of rub, gear and reduce the time to suit. This would also ensure the precision and result in a longer work piece life.

在以前研究的基础上，本论文重新探讨了电化学机械复合光整加工工艺的机理，确定了较合理的工艺参数，对电化学机械复合光整加工设备进行了改进，通过工艺实验广泛地搜集了大量实验数据，依据实验数据，多角度地研究了电化学机械复合光整加工的表面形貌特点，并且从理论上深入讨论了电化学机械复合光整加工表面形貌对工件工作性能的影响，最后得出的结论为：电化学机械复合光整加工对工件原始表面的低频成分有较大程度的降低，而对高频成分影响较小，有明显的阳极整平作用，被加工工件表面的尖峰状凸起被去除，工件表面呈现出微观&高原型&，表面轮廓不平度高度特性参数大幅度降低，工件表面轮廓分布集中，且呈负偏态，轮廓偏斜度为负值，轮廓支承长度率曲线陡峭，工件的表面质量得到综合改善，这对提高零件的抗接触变形能力、改善摩擦、磨损性能、降低工件的磨合时间、提高工件的精度保持性、延长工件的寿命均有利。

Analytical results show that: Anode evaporation rate, which determines mostly the production rate of UFMP, is influenced by the many factors including electric parameters of arc, ambient conditions and material properties et al; Existence and increase of anode ejection can influence the production rate and property of UFMP; It is firstly found and investigated that surface connexity phenomenon of Al anode material. Analyses and calculation show that formation of anode spot and existence of self-magnetic field force play an important part in surface connexity process; Effects of cathode material on prepared UFMP is also experimentally studied and theoretically analysed. It shows that effect of the cathode is inconsiderable under the experimental conditions used in the study. At last, the experimental results found in part one are analysed and discussed in detail.

然后详细分析了电弧与电极间的相互作用过程，结果表明：决定超微粉产率的阳极材料蒸发率受许多因素影响，它主要与电弧电参量，环境条件及材料性质有关；阳极表面液滴喷溅的存在和加剧将严重地影响所制超微粉的产率和性质；首次发现和实验研究了Al阳极表面凸起现象，并对此现象进行了详细的理论分析和实际估算，认为阳极斑点的形成及自磁场作用力的存在在该过程中起着重用作用；实验研究和理论分析了阴极材料对所制超微粉的影响，认为在本文所用实验方法及条件下，阴极材料对粉的影响很小。

Based on the existing experiment condition, the institute of physical culture of Nanchang Hangkong University has innovated traditional experiment teaching and schemed out comprehensive experiment, which combined book knowledge and sports practice consanguineously.

南昌航空大学体育学院根据实验室现有条件，对传统实验教学进行改革，设计成综合性实验。该实验既与课本知识紧密结合，又与运动实践密切相关。

Its thermodynamic characteristic is gimilar to R410A. Contrast experiments by air enthalpy difference method are performed. Experimental results indicate that without modification to system components, cycle performances of M3 are close to R410A. Its cooling capacity is slightly smaller than R410A. It has a greater COP and low power consumpt...

在标准的空气焓差实验台上对M3、R410A进行了对比实验，实验结果表明，在不改动系统部件的情况下，新工质M3可保证R410A系统的循环性能基本无大的变化，其循环性能接近R410A，制冷量稍小，但COP值大，耗功少，具有替代新系统中R410A的潜力。

Finally, the effect of the complete recycling use of distilled effluent on ethanol fermentation was examined in order to save the cost for the treatment of waste distillage and promote cleansing production. Based on the data of 13 circulations, although the average fermentation time needed to be extended to 30~40 hours, over 12.5% ethanol was achieved, at the same time, residual reducing sugar and total sugar were maintained below 0.70% and 0.90%, which indicates that the negative effect of the completely recycling use of waste distillage was limited, and the waste distillage can be completely recycled within the fermentation system.

在此基础上，从减轻废糟液处理负荷，实现清洁生产的需要出发，进行了无种子罐条件下酒精蒸馏废液直接全循环使用的自絮凝颗粒酵母酒精连续发酵实验研究，十三次全循环运行得到的实验数据，与无废液循环的实验结果相比，虽然平均发酵时间略增至30h～40h，但发酵终点酒精浓度仍达到12.5％以上，残还原糖和残总糖分别在0.70％和0.90％以下，说明循环积累物对发酵的影响有限，废糟液直接全循环使用的工艺技术路线可行。

This thesis investigates the profile extraction and shape optimization on the result of topology optimization of planar compliant mechanisms. The main context includes the following work:(1) summarizing and analyzing the recent research status, some harvest and unsolved problems;(2) analyzing the conceptual design of planar path-generating compliant mechanisms and its mathematical model and tools;(3) Modifying the method of density contour as the method of profile extraction, and developing a method to optimize the density function in the profile extraction according to the requirement of the design of compliant mechanism;(4) developing a method to abstract the compliant mechanism into a form of links and joints by using the principle of connectivity on topology;(5) developing a method of shape optimization of planar path-generating compliant mechanisms, by representing the profile of the abstracted compliant mechanism as simple curves such as straight lines and arcs, establishing the models of the size optimization of the parameters of these curves, so that the compliant mechanism has a machinable shape;(6) At last, proving the feasibleness and effectiveness of the design method by making simulation design and validating it in FEA software.

主要工作包括：(1)分析了柔顺机构拓扑优化和形状优化的研究现状，分析了目前柔顺机构的研究重点、主要成果和尚未解决的问题；(2)分析了基于SIMP的柔顺机构概念设计方法及其相关工具和模型；(3)针对柔顺机构轮廓提取的特殊要求，提出了密度等值线法的改进方案，对密度函数插值点密度值进行优化，提出优化模型和选择优化算法；(4)根据轨迹输出平面全柔顺机构自身的形状特点，提出了轨迹输出平面全柔顺机构的抽象方法，即应用拓扑学上的连通性原理将柔顺机构抽象成杆件和结点形式，并对相应的数学原理进行了证明；(5)提出了平面全柔顺机构的形状还原和尺寸优化方法，对抽象的柔顺机构进行还原，将其轮廓还原成简单曲线的连接，从而建立尺寸优化模型，对机构进行尺寸优化设计，在得到可加工的机构轮廓的同时又能对关键部位进行特别处理；(6)进行了柔顺机构的数值仿真设计，并将所得设计结果导入商用有限元软件中进行仿真实验，证明了设计方法的可行性和有效性。

Degradation test in vitro was carried out in phosphate buffer solution (0.1M, pH7. 4) at 37 ℃. The buffer solution was changed daily. Degradation test in vivo was implanted the sample to subdermal in adult ICH rat in the scapular area lateral to the dorsal midline. At suitable time the samples were recovered. Molecular weight changes in surface layer and bulk of polymer sample were measured by GPC and weight loss was determined gravimetrically. It was found that the degradation behavior can be regulated by changing the composition of copolymers. The critical compositions from surface to bulk degradation behavior for PGCA, PLCA, PLMCA, PLDCA systems were 15-20, 20-30, 30- 40, 40 of mol percent GA or LA unit in copolymers, respectively. The degradation behavior of PGCA, PLCA, PLMCA, PLDCA systems were compared and analysed. Some factors influencing the degradation character, such as copolymer composition, hydrophobicity, crystallinity and enzyme affect etc. played important role.

体外实验中材料降解环境为37℃，0.1M，pH7.4磷酸缓冲溶液，每天换液，定期取样；体内实验中将聚合物试样埋置于ICH小白鼠背部肩胛骨皮下部位，定期处死小鼠，取样，将体内体外样品进行重量损失及试样内外层分子量变化测定，分析各聚合物试样降解行为特性，实验结果证明，改变共聚物组成，可以调节各聚合体系降解行为特性，对PGCA，PLCA，PLMCA，PLDCA共聚体系，交酯摩尔百分含量15-20％，20-30％，30-40％，40％分别为各体系内降解行为特性由表面降解型向本体降解型过渡的临界转折点，交酯含量较低的聚合物不同程度地表现表面降解行为特性，论文对各共聚体系体内外降解行为作了分析对照，例如共聚物组成对材料降解速度与降解行为的影响；生物体内酶对降解行为的影响；材料亲疏水性，聚合物链段结晶行为及碳酸酯结构对材料降解行为的影响等，得出交酯/环碳酸酯共聚体系降解行为一些共性和规律。

By analyzing these data,it was concluded that:1The combustion of wood,including rate of heat release,total heat release,effective heat of combustion,mass loss rate,smoke ratio,specific extinction area,concentration of CO_2 and the yield of CO_2Y_(CO2,were decreased considerably by the treatment of FRW;2There is a strong synergistic effect of fire retardance between GUP and boric acid;3The trend of MLR curve of FZ was similar to its RHR curve,weight loss and heat release were happened mainly in flaming phase;4Char formation of wood was markedly accelerated by FRW,which indicated that catalytic charring effect of FRW on wood is the primary side in its fire-retardation mechanism.

对于组成和结构变异性很大的木材而言，由于CONE实验所使用的样品量相对于其他分析方法要大得多，因而实验结果比较有代表性。此外，CONE实验可在模拟火灾条件下进行，这是该方法的又一突出的优点[5～6]。木材阻燃剂FRW主要由磷酸脒基脲和硼酸组成，此外还含有

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。