进行中的

First, some critical problems in crystal growth like crystal seeding, Zn dephlegmation, geometrical selection and temperature fields are discussed in theory, and the possible kinds of defects appeared in crystal growth progress and the reasons are carefully researched. To control the concentration of Cd vacancies, a new method by which the Cd vacancies were compensated with excess Cd in the Cd rich starting materials has been developed, and a new kind of two-area tube furnace with good linear temperature distribution was designed.

首先，本文从理论上对坩埚下降法生长碲锌镉单晶体中的成核、Zn分凝、几何淘汰生长与温场等关键性问题进行了讨论，对在生长过程中可能出现的各种缺陷类型和形成原因进行了详细分析，提出了碲锌镉单晶体生长过程中Cd空位缺陷控制原理及方法，并针对坩埚下降法生长特点自行设计了两区域独立加热管式生长炉，获得具有较好线性分布的温场。

This work, concentrated on the asymmetric allylation of aldehydes controlled by different chiral auxiliaries prepared from rotational pure tartaric acid, can be divided into three parts.The first part aims to review the developments of chiral drugs and asymmetric synthesis, from which derived the present research topic backgrounds and works.Synthesis and applications of allylation from aldehydes are the second part of the thesis. By optimizing the reaction conditions, such as solvents, temperature, time and chiral auxiliaries like N,N\'-dibenzyl tartamide, N,N\'-p-dimethylphenyl tartamide, N,N\'-o-dimethylphenyl tartamide, N,N\'-o-dichlorophenyl tartamide, N,N\'-a-dinaphyl tartamide, N,N\'-dicyclohexyl tartamide and N,N\'-diphenyl tartamide, ideal experimenttal conditions are obtained according to HPLC monitoring, as well as the auxiliaries\' recoveries experiments. Starting from benzaldehyde and 3-bromopropaldehyde, N,N\'-dibenzyl tartamide is considered the best auxiliary in this reaction.

本文介绍了醛的不对称烯丙基化反应，以光学纯酒石酸为原料，研究了不同构型手性配体在醛的烯丙基化反应中的立体选择性，全文共分三部分十个章节：第一部分对当前手性药物和手性技术进行了概述，并由此展开了本文的研究背景和任务；第二部分为有机合成部分，对醛的不对称烯丙基化反应进行了深入探讨，以苯甲醛为原料对反应条件进行优化，在优化的反应条件下对制备的七种可回收手性酰胺配体(N-苄基酒石酸二酰胺、N-对甲苯基酒石酸二酰胺、N-邻甲苯基酒石酸二酰胺、N-邻氯苯基酒石酸二酰胺、N-a-萘基酒石酸二酰胺、N-环己基酒石酸二酰胺和N-苯基酒石酸二酰胺)进行筛选，优化配体回收实验条件，最终确定出N-苄基酒石酸二酰胺在苯甲醛的不对称烯丙基化反应中具有较大优越性，结晶回收的手性配体光学纯度保持不变。

In this research work, the technology of microbial conversion was studied in order to establish an environment friendly method for the production of doxorubicin. A doxA gene encoding Daunorubicin C-14 hydroxylase was cloned from a daunorubicin-producing strain Streptomyces coeruleorubidus SIPI 1482. Some plasmids for the expression of doxA gene were constructed and transformed into S.

本研究对微生物转化法替代现有工艺生产阿霉素进行了探索，从柔红霉素产生菌天蓝淡红链霉菌SIPI 1482中克隆了柔红霉素C-14羟化酶基因，构建了doxA基因的链霉菌表达质粒，导入变铅青链霉菌TK24中获得了柔红霉素转化基因工程菌，并研究了doxA基因在工程菌中的表达，最后还对工程菌转化柔红霉素生成阿霉素的发酵工艺进行了初步研究。

Total RNA was extracted from venom cells from Gloydius intermedius, FLE gene was amplified by RT-PCR. Then it was connected to pMD18-T vector by TA cloning. At last, sequencing and analysis the genesequence.

从中介蝮蛇毒腺细胞中提取总RNA，通过RT-PCR法扩增纤溶酶基因，与pMD18-T载体连接进行TA克隆，再进行序列的测定并且对该序列进行分析。

Methods:Total RNA was extracted from venom cells from Gloydius intermedius,FLE gene was amplified by RT-PCR.Then it was connected to pMD18-T vector by TA cloning.At last,sequencing and analysis the gene sequence.

材料及方法：从中介蝮蛇毒腺细胞中提取总RNA，通过RT-PCR法扩增纤溶酶基因，与pMD18-T载体连接进行TA克隆，再进行序列的测定并且对该序列进行分析。

A method for the separation and determination of Pueraria lobata isoflavonoid extract by reversed-phase high performance liquid chromatography was proposed.

采用反相高效液相色谱法，在C1 8柱上以甲醇水为流动相进行梯度洗脱，在 0～ 1 0min内将葛根黄酮提取物进行分离，并在 2 5 0nm检测，采用标准加入法对实际样品中的葛根素含量进行了分析。

Of Fe , Cu in the metal phase and Mg, Si in the silicate phases to understand the processes of mixing of metal and silicate phases and further decipher the mechanism of formation of mesosiderite;(2) to study in detail the geochemical characteristics of each phase in the meteorite, to provide necessaryevidence for the model of formation of mesosiderite;(3) to study and update in detail the composition of each phase in the meteorite, and provide a new and complete set of data for understanding the mechanism of formation of mesosiderite.

Cu和硅酸盐相中的Mg， Si等中等挥发性元素的稳定同位素进行分析，判断中铁陨石的金属相和硅酸盐相混合过程的环境特征，进而阐明中铁陨石的形成机制；（2）对这块陨石的各相进行详尽的地球化学分析，通过这些相的地球化学关系判断中铁陨石的形成机制，对中铁陨石的形成模型提供必要的制约和证据；（3）全面更新对中铁陨石各矿物相化学成份的认识，为中铁陨石的成因之谜的全面揭开提供最新最完整的数据。

In addition, a pre-column derivatization HPLC method was applied to the determination of Astragaloside Ⅳ; the flavonoids was determined by full-range HPLC scanning; a colorimetric method was developed for the determination of flavonoids and saponins. Hierarchical cluster analysis was performed on three constituents of different Radix Astragali species, and its result was compared with those of traditional phytoecological identification and the pharmacological quality assessment.

本研究以比色法测定了黄芪中总皂苷的含量，以柱前衍生化高效液相色谱法测定了黄芪中黄芪甲苷的含量；以比色法测定了黄芪中总黄酮成分的含量，以反相高效液相色谱法测定了黄芪中毛蕊异黄酮和毛蕊异黄酮苷的含量；以黄芪中的黄芪甲苷、毛蕊异黄酮和毛蕊异黄酮苷为主要特征对不同品种的黄芪进行了系统聚类分析，并将聚类结果与传统生药学鉴定和药理质量评价结果进行了比较。

The spring back in the distortion process was predicted by finite element method, and the predicted results were analyzed to find out the reason lead to spring back, and so as to precompensate the spring back.

利用有限元仿真对其变形过程中的回弹进行预测，并对预测结果进行研究，找出回弹根源，从而对其回弹进行预先补偿。

The prequalification of bidders,evaluating methods and contract clause of the fiduciary duty institution bidding for highway project are discussed.

对公路建设项目代建制招投标中的投标人资格条件、代建制评审办法及代建制招标文件中合同条款的设立进行了分析；并对政府部门在代建制招投标中应进行的监管提出了建议。

Do you know, i need you to come back

你知道吗，我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。