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First, a chlorinator was self-designed in this paper, and dichloride of 2-methyl-1-propene was synthesized by 2-methyl-1-propene reacted with chlorine fast in this reactor. By means of the Orthogonal Experiments design and single factor experiments, the influence of several reaction variables on the yield were examined and the optimum reaction conditions under the intervallic operation were obtained, the yield and selectivity of dichloride of 2-methyl-1-prop-ene were more than 65% and 80% respectively. Second, the preparation of 2-methylene-1, 3-propanediol, which dichloride of 2-methyl-1-propene reacted with alkali was investigated. By means of the Orthogonal Experiments design and single factor experiments, the influence of several reaction variables on the yield were examined and the optimum reaction conditions under the intervallic operation were obtained, the conversion of dichloride of 2-methyl-1-propene was 100%. Moreover the preparation of MPO, which 2-methylene-1, 3-propanediol reacted with hydrogen, in presence of Al_2O_3-Pd catalyst, was gotten, and the product was appraised.

本文在氯化反应过程中,自行设计制作出了氯化管式反应器,在该反应器中异丁烯和氯气迅速混合反应生成二氯异丁烯,根据该氯化反应特征利用正交试验和单因素试验考察了有关因素的影响并优化得到了最佳工艺条件,二氯异丁烯的总收率达65%以上,选择性达80%;接着,对二氯异丁烯进行水解反应制得了2-甲烯-1,3-丙二醇,讨论了相关因素对水解反应的影响,并通过正交试验和单因素试验得到了较佳工艺条件,二氯异丁烯的转化率达100%;同时还对制备的2-甲烯-1,3-丙二醇在常压下采用三氧化二铝负载钯催化剂催化加氢得目的产物MPO,并对产品进行了鉴定,从而打通了整个工艺路线。

In view of practical problem during Sulige gas field development, this paper complete follow study content. Study material balance theory of two district compound gas reservoir. Carry out stress sensitivity experiment on matrix rock and labor created fracture core from Sulige gas field with America Core Company high pressure high temperature flow experimental instrument to study stress sensitivity change rule of different permeability matrix rock and created fracture core at the condition of time and again switch on and off well and different drawdown pressure. Carry out depletion experiment on matrix rock of different permeability serial combination with different kinds of allocation, using double core clamper serial connected experimental apparatus, to study gas well production performance of bi-zonal compound low permeability reservoir during low pressure production stage. At the basis of experimental study, establish single well simulation model to analyze development index infection caused by stress sensibility and production performance infection rule caused by inner formation and outer formation of bi-zonal compound gas reservoir permeability variation while considering stress sensitivity.

针对苏里格低渗气田开发中存在的实际问题,完成以下研究内容;研究了两区复合气藏物质平衡原理;利用美国岩芯公司高温高压流动实验仪,对取自苏里格气田基质岩芯和人工造缝岩芯进行应力敏感实验,研究不同渗透率基质岩芯和造缝岩芯在多次开关井和不同生产压差条件下的应力敏感变化规律;采用双岩芯夹持器串联实验装置,对不同渗透率串联组合的基质岩芯进行各种配产条件下的衰竭实验,研究两区复合的低渗储层气井在低压生产阶段的生产动态特征;在实验研究的基础上,建立单井模拟模型分析储层应力敏感性和非均质性对开发指标的影响,研究考虑应力敏感时两区复合气藏储层中内区和外区渗透率变化对开发动态的影响规律。

The discourse analysis theory and one-to-one dialogue are kept inanalyzing the application of the rhetorical question to the discourse, for example, its place, type, coherence, condition, choice model, feedback, reduction and clear-up.

本文运用会话分析理论,以两人对话式话语为对象详细分析了反问句在话语进程中的作用,主要包括:反问句在话语中出现的位置;对话中反问句出现的类型:反问句的话轮衔接功能;反问句作为应对句的话语制约机制;对话中反问句的选择模式;对话中反问句如何作为馈语出现;对话中反问句话语功能的弱化现象;对话中反问句的应对语是如何对反诘意味进行消解的。

This thesis reviews the bankruptcy process of that plant, classifies the contradictions and problems in the process, analyzes the essential factors to ensure the steady execution of resource dry - out enterprises closedown and bankruptcy process, brings forward some key points which should be grasped in such cases, and puts forward advice on some problems from which no conclusion is drawn yet for the moment.

本文通过对桐柏银矿破产操作过程的回顾,对企业破产操作中出现的矛盾和问题进行了分类,对保证确保资源枯竭矿山企业关闭破产操作平稳实施的一些主要因素进行了分析,提出了这类企业关闭破产操作中应把握的要点。

Donn Colby, who will include it in a panel he is coordinating concerning homosexuality in Vietnamese society and culture.

我已经与 Donn Colby 博士就我的计划进行了讨论,他对在越南社会和文化中存在的同性爱现象怀有同样的关注,他会将我的计划纳入到他所在的小组中进行讨论。

The other is communistic moral constructing with the selfless principle in the commie and the advanced mentality people.

我国当前的道德建设应当分为两个层次:一是在普通公民中进行以集体主义为原则的社会主义道德建设;二是在共产党员和一切先进分子中进行以大公无私为原则的共产主义道德建设。

In order to optimize an effective combined preservative applied to the orange juice preservation, the authors studied the synergistic effect of biological and chemical combined preservative which contained Nisin, potassium sorbate, EDTA and sodium isoascorbate in preservation of orange juice compared to preservation effect of each aforementioned additive in individual use. Results show that the growth of microorganisms can not be inhibited completely using each aforementioned additive in single use.

该文以天然生物防腐剂乳酸链球菌素、化学防腐剂山梨酸钾、乙二胺四乙酸以及食品抗氧化剂异Vc钠为原料,对通过复配后得到的各组复合型防腐剂在橙汁保鲜中的协同增效作用进行研究,并且与单一的防腐剂保鲜效果进行比较,得出一组适合在橙汁中使用的高效复合型防腐剂。

Parametric evaluation function can condense the complicated multi-objective and multi-constrait problem into a single-objective unconstrained problem, then solved with conjugate gradient method.The parametric evaluation function method decreases the optimization difficulty,and makes the solution away from the boundary of feasible region during the optimization process,which makes all the objectives optimized simultaneously.

参数评价函数把复杂的多目标多约束优化问题转化为单目标无约束问题,然后用共轭梯度法进行求解,不但降低了求解难度,而且使得在优化过程中其解远离可行域的边界,保证了对多目标中所有目标同时进行优化。

First design a reasonable XML Schema structure and under the restriction of XML Schema use XML to describe the UML class diagram and the related specification, and then extract the test specification of method from XML test script. Test specification refers to predicate sequences in the form of conjunctive normal form, extracted from basic constraint conditions of variables included in test scripts and expected outputs. Each conjunctive normal form can be transformed to an inequation set, and adopt 1×1 domain test strategy to every inequation set to produce the domain test matrix, which in turn produce the test case.

首先设计合理的XML Schema结构,并在该XML Schema的有效性约束下,用XML对UML类图及相关性约束进行脚本描述;其次对XML测试脚本进行分析,提取方法的测试规约说明,所谓测试规约说明就是从测试脚本中包含的变量的基本约束条件以及期望输出中抽取得到的以合取范式形式存在的谓词序列;每一合取范式对应一个不等式组,对每一个不等式组采用1×1域测试策略,生成域测试矩阵,最终得到测试用例。

The short tandem repeats is a kind of DNA sequence formed repeatedly and connectively subjected to a core unit of several base pairs.The non-interfered multi-PCR was applied with 3 loci in the same reaction system.By using the technique of denaturing polyacrylamide gel electrophoresis and silver stain,the allele frequencies distributions of 3loci:F13A01,FESFPS and vWA in 10 minority populations only resided in Yunnan Province:Bai,Dai,Achang,Jingpo,Deang,Lahu,Bulang,Hani,Pumi and Jino.A satisfactory result was obtained and some significant genetic differences were noticed in different populations.

短串联重复序列是由几个碱基对作为核心单位串联重复形成的-类DNA序列,应用3个位点在同一反应体系中进行互不干扰的多重PCR,采用高分辨力的聚丙烯酰胺凝胶电泳分离、银染法显影技术,对云南省特有的白族、傣族、阿昌族、景颇族、德昂族、拉族、布朗族、哈尼族、普米族和基诺族等10个少数民族的F13AO1、FESFPS和vWA3个位点等位基因的基因频率分布进行了调查,获得了满意的结果,在不同群体中发现一些有意义的遗传差异。

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The absorption and distribution of chromium were studied in ryeusing nutrient culture technique and pot experiment.

采用不同浓度K2CrO4(0,0.4,0.8和1.2 mmol/L)的Hoagland营养液处理黑麦幼苗,测定铬在黑麦体内的亚细胞分布、铬化学形态及不同部位的积累。

By analyzing theory foundation of mathematical morphology in the digital image processing, researching morphology arithmetic of the binary Image, discussing two basic forms for the least structure element: dilation and erosion.

通过分析数学形态学在图像中的理论基础,研究二值图像的形态分析算法,探讨最小结构元素的两种基本形态:膨胀和腐蚀;分析了数学形态学复杂算法的基本原理,把数学形态学的部分并行处理理念引入到家实际应用中。

Have a good policy environment, real estate, secondary and tertiary markets can develop more rapidly and improved.

有一个良好的政策环境,房地产,二级和三级市场的发展更加迅速改善。