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Structure unit 2 was conveniently synthesized from 3-cyanopyridine by methylation, rearrangement reaction, and reduction of formyl.

以价廉易得的3-氰基吡啶为原料,通过甲基化、重排、还原三步反应合成了结构单元2。

In the presence of NaH and in DMF, the acyclic crown ethers 1a and 1b were synthesized by the reaction of di-or triethyleneglycol ditosylate and o-methoxymethoxybenzyl alcohol, which was obtained from salicylaldehyde via the protection of the hydroxyl group with chloromethyl methyl ether followed by the reduction of the formyl group with NaBH4. The hydrolysis of 1a and 1b with dilute hydrochloric acid provided the diphenolic type acyclic crown ethers 2a and 2b respectively in good yield.

将水杨醛与碱和氯甲基甲基醚反应,再经过NaBH4还原,即制得邻苯甲醇,然后将其在DMF中与NaH和二甘醇二对甲苯磺酸酯反应,得开链冠醚1a和1b.1a和1b经稀酸水解,即脱保护而分别生成新的酚型开链冠醚2a和2b。

Antifolate Alimta derived from pyrrolo[2,3-d]pyrimidine is a multitargeted antitumor agent, it can inhibit at least five major folate-dependent enzymes: thymidylate synthase, dihydrofolate reductase, glycinamide ribonucleo -tide formyltransferase, aminoimidazole ribonucleotide formyl transferase and C-1 tetrahydrofolate synthetase(C1-S).

吡咯并[2,3-d]嘧啶类叶酸拮抗剂Alimta是一种多靶向的抗癌药物,它能抑制至少五种叶酸依赖性酶:胸苷合成酶、二氢叶酸还原酶、叶酰多聚谷氨酸合成酶、甘氨酰胺核糖核苷酸转甲酰酶及C1-四氢叶酸合成酶(C1-S)。。

This model indicates that the sulfur isotopes, whose values tend to be negative fractionate to a large scale because of the reductive process of dissimilating bacteria of sulfate.

根据内蒙古乌达矿区高硫煤9煤层(有机硫同位素值 d 34 S=-12.3‰~5.8‰,黄铁矿硫同位素值 d 34 S=-18.7‰~1.1‰)和低硫煤13煤层(有机硫同位素值 d 34 S 为8.9‰~ 11.5‰,黄铁矿硫同位素值 d 34 S 为8.3‰~ 9.7‰)剖面上有机硫和黄铁矿硫同位素的组成,结合煤岩学特征的综合分析以及黄铁矿化菌落和蓝藻胶壳的发现,提出了高硫煤中硫的演化模式,认为高硫煤中硫的同位素由于硫酸盐的异化细菌还原作用导致硫同位素大规模分馏,使之趋于负值。

The article analyzed the Franz Schubert's Piano Sonata, Op.120 all-around with the elements of multidimensional structures, such as the pitch, rhythm, and textures. It discussed the effect of change and ratio to the drive and structure of the music through the three aspects of combination: the synchronous change and symmetry ratio of the element rhythm, the asynchronies change and the asymmetry ratio of the element rhythm, and the synchronous with asynchronies changes, and compared them with the Heinrich Schenker system.

内容提要:本文以舒伯特《钢琴奏鸣曲OP.120》为例,对该部作品的音高、节奏、织体等多维音乐要素进行了综合分析,从要素节律的"同步变化"和要素节律间的"匀称比率"、要素节律的"异步变化"和要素节律间的"非匀称比率"以及要素节律的"同步变化"、"异步变化"的结合三方面,来探讨了这些"变化"、"比率"对音乐的动力、结构力的作用,并与申克的还原体系分析方法进行了比较。

The abilities of red cabbage extract scavenging HO, ABTS(superscript +) and FRAP were studied by using chromogenic reaction and UV-vis spectrophotometry.

方法]采用化学显色和紫外可见分光光度法考察紫甘蓝提取物清除在自由基、ABTS和铁离子还原力的能力。

Heating the solutions with the presence of sucrose resulted in the large enhancement of FRAP yet decreasing monomeric ACN.

另外,在抗氧化能力方面,DPPH清除百分比不论任何处理,加热前没有明显差异;FRAP还原能力及TEAC总抗氧化能力,则凡添加蔗糖者,加热后皆急速上升。

On the antioxidant capacity analysis, the total phenol content, vitamin C remaining, DPPH scavenging ability and FRAP reducing power of dried guava slice by addition phenolic compounds after formation cross-linkage was higher than that of the control.

在抗氧化力方面,添加酚类的乾燥番石榴果片及蜜饯在形成交联后的总酚含量、维生C残留量、DPPH自由基清除能力及FRAP还原力均高於对照组。

While being used, it will change the bound water into free water through touching soil and plants, directly and continuously discharge water in a long time to plant growth.

它在使用时通过与土壤、植物接触,将束缚水还原为自由水,直接和不间断地释放,可用做植物生长的长效水源,最后在微生物的作用下发生生物降解,对土壤没有任何污染、残留。

Theoretical and experimental studies on temperature drop process of freight car bearing under natural convection are done.

为此提出以还原轴承温度的方法描述拦停报警时轴承的实际温度。

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However, as the name(read-only memory)implies, CD disks cannot be written onorchanged in any way.

然而,正如其名字所指出的那样,CD盘不能写,也不能用任何方式改变其内容。

Galvanizes steel pallet is mainly export which suits standard packing of European Union, the North America. galvanizes steel pallet is suitable to heavy rack. Pallet surface can design plate type, corrugated and the gap form, satisfies the different requirements.

镀锌钢托盘多用于出口,替代木托盘,免薰蒸,符合欧盟、北美各国对出口货物包装材料的法令要求;喷涂钢托盘适用于重载上货架之用,托盘表面根据需要制作成平板状、波纹状及间隔形式,满足不同的使用要求。

A single payment file can be uploaded from an ERP system to effect all pan-China RMB payments and overseas payments in all currencies.

付款指令文件可从您的 ERP 系统上传到我们的电子银行系统来只是国内及对海外各种币种付款。