过氧化

Carboxylic acid was peroxidized in organic solvents catalyzed by lipase and glycidol was synthesized from allyl alcohol catalyzed by acid peroxide.

利用脂肪酶在有机介质中催化制备过氧酸，丙烯醇在过氧酸的作用下发生环氧化反应生成环氧丙醇。

Cyclic voltammetry indicated that there were Cr→Cr, Cr →Cr oxidation reaction on anode, while there were Cr→Cr, Cr→Cr, Cr →Cr deoxidization reaction on cathode. The graphite electrodes treated by acid and heating could enhance the reversibility and kinetic of the electrode reaction. The nature graphite electrodes had been eroded during charge/discharge process, while the graphite electrodes by activation could avoide corroding by hexad chromium ion. The reversibility and kinetic of the electrode reaction of chromium ion on activation electrode had been increased, so which indicated that graphite surface augment oxygenous function corps which could increase electrode hydrophile capability.

循环伏安实验表明：铬液流电池的电极反应非常复杂，在阳极存在Cr→Cr，Cr→Cr的氧化反应，在阴极存在Cr→Cr，Cr→Cr，Cr→Cr的还原反应；热处理的石墨电极和重铬酸钾处理的石墨电极能提高电极反应的活性和可逆性；在充放电实验中未处理的石墨电极发生严重腐蚀；分别用这两种方法处理过的石墨电极具有防止六价铬侵蚀的功能；铬离子在活化处理过的石墨电极上的反应活性和可逆性增加，可以认为：重铬酸钾溶液活化处理和加热处理后的石墨表面的含氧官能团增加，电极亲水性增强。

In every group, rabbits were subdivided into experimental and control subgroups. 2 Rabbits were bullets injected followed by continuous injected with 13C labeled leucine, glucose, and lactic acid; 3 Blood were drewed before and 150, 160, 170, and 180 min after the initiation of isotopes injection for material analysis; 4 Exhale gas were collected every 5 min in the first 30 min followed by every 30 min there after for material analysis; 5 After centrifuge in low temp the supernatant of the blood samples were collected and went through axon and anon exchange column treatment; 6 Treated blood sample was used for 13C labeled leucine, glucose lactic acid examination through mass spectrograph; 7 The exhale gas was collected for 13CO2 exam through gas-phase mass spectrograph; 8 CO2 total production rate (V13CO2), body various substances production, oxidation speed, and substances metabolic percentage all can be calculated through equations provided by references below; 9 Data was processed through student t test.

分亮氨酸、葡萄糖和乳酸三组各取健康新西兰兔16只，每组再分为高代谢脓毒症组和对照组两部分，建模方法同第一部分；2）三组分别先静脉弹丸式推注再持续灌注13C标记的亮氨酸、葡萄糖和乳酸；3）灌注前抽取动脉血作为背景值，灌注达150，160，170和180min分别抽取动脉血2ml用于质谱分析；4）实验开始后前30min中每5min收集呼出气一次，随后每30min收集呼出气一次，用于气相质谱分析；5）血样经过低温离心取上清液，过阳离子及阴离子交换树脂，再经衍生化处理；6）处理过的血样进入气相色谱－质谱仪，测量其13C标记的亮氨酸、葡萄糖和乳酸丰度；7）实验兔的呼出气通过13CO2气相质谱分析仪测定其中的13CO2丰度（E13CO2）；8）利用文献提供的公式算出CO2总生成率（V13CO2）以及机体各物质的通量、氧化速率以及物质代谢百分比等；9）数据分析处理采用t检验。

Our data suggest that widely used oxidation measures, such as ex-vivo LDL oxidizability, do not reflect the degree of atherosclerosis; and long-term beneficial effects of relatively low doses of antioxidants may be outweighed by high levels of plasma cholesterol in WHHL rabbits.

研究表明：广泛应用的氧化检测，例如体外LDL氧化度并不能反应动脉粥样硬化的程度；WHHL家兔血浆胆固醇水平过高会抵消长期给药抗氧化剂的疗效。

Since the relative antioxidant capacity of all the phenolic compounds was much higher than trolox in both assays, it is a good indication that phenolic compounds possess high antioxidation capacity against peroxy radicals.

由於酚类物质之相对抗氧化力均远高於trolox，表示酚类物质对过氧自由基具有很好的抗氧化效果。

ZnO nanoparticles were surface-modified by surfactants such as span-60,oleic acid,sodium laurate,andx as surface-modifier,and were added at the concentration of 0.5% in lquid paraffin to perform sedimentate test.

以山梨糖醇酐三油酸酯(span-60)、油酸、月桂酸钠和氟碳(C—Fx为表面活性剂对纳米氧化锌进行表面修饰，将修饰过的纳米氧化锌添加到液体石蜡中，使其质量分数为0.5%，进行沉降实验。

In terms of experimental results, ammonium persulfate oxidizes antimony trioxide into hydrous antimony pentoxide and is reduced itself into ammonium sulfate in aqueous medium of sulfuric acid.

结果指出，在硫酸介质中，过硫酸铵可将三氧化二锑氧化成固体水合五氧化二锑，自身则被还原成硫酸铵进入溶液。

Papers in the experimental part of our literature considered on the basis of the experimental exploration, and podophyllotoxin intermediates with the structural characteristics of a simple pepper aldehyde as the starting material,α,β-unsaturated carbonyl compounds are selective reduction lithium aluminum hydrogen reduction reaction as the key steps to have the Knoevenagel condensation, peracetic acid epoxy between chlorine and alkaline hydrogen peroxide epoxy, DCC condensation esterification reaction of the three podophyllotoxin intermediates.

论文实验部分我们在综合考虑文献的基础上，经过实验摸索，并结合鬼臼毒素中间体的结构特点以简单的胡椒醛为起始原料，对α，β-不饱和羰基化合物具有选择性还原的锂铝氢还原反应为关键步骤，先后经过Knoevenagel缩合，间氯过氧苯甲酸环氧化，碱性过氧化氢环氧化，DCC缩合酯化等反应合成了3个鬼臼毒素中间体。

Through the study of the crucible manufacture and its application in strong reducing atmosphere it was found that the used densified CaO crucible could decrease the absorption of calcium by the refractory and increase efficiency of calcium.

通过对氧化钙坩埚制造和使用的研究，发现用使用过的致密氧化钙旧坩埚可以减少坩埚对钙液的吸收，提高了钙利用率。

Infrared, ultraviolet, and mass spectrometry Gaoxiaoyexiang tests showed that benzene p rosin in neighbouring seats husband alkali metal objects with catalytic, the oxide containing hydroxy generated, ethylene, or a functional group, such as the Food oxide product.

红外、紫外、高效液相色谱和质谱测试表明，松香在邻苯二胺席夫碱金属配合物的催化下，氧化生成了含羟基、环氧基、过氧基等官能团的氧化产物。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。