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This article mainly established the analysis method to extract the oxine-copper residues in cucumber and soil with ion pair of antiphase HPLC and Ultrasonic-assisted solvent. This method mainly uses XBridge C18 column and UV detector by using waters phase of phosphatic buffered solution/acetonitrile (60:40, by vol) as mobile phase with 0.8 mL/min flow ratio and UV detection at 250 nm. The residue time was 4.71 minute. Accuracy, precision, and sensitivity of the method all satisfy the demands of pesticide residue analysis.

建立了黄瓜和土壤中喹啉铜的超声波辅助溶剂提取-反相离子对高效液相色谱法的残留分析方法,该方法使用XBridge C18色谱柱和可变波长紫外检测器,并以水相磷酸盐缓冲溶液-乙腈(体积比为60:40)作流动相;流速为0.8 mL/min;检测波长为250 nm;保留时间为4.71 min;该方法的准确度、精密度及灵敏度均满足农药残留分析的要求。

The ultrasonic-assisted solvent extraction and quantitative analysis of the oxine-copper residues in soil with ion pair of antiphase HPLC was established. This methods mainly uses XBridge C5 column and UV detector by using waters phase of phosphatic buffered solution/acetonitrile (60:40, by vol) as mobile phase with 0.8 mL/min flow ratio and UV detection at 245 nm. The residue time was 4.72 minute. The linear correlation of this method was 0.9987. The recovery rate was 76.2 to 108.7%. Comparatively standard deviation was 0.6 to 3.37%. The detection limits of method was 0.05 mg/kg.

建立了土壤中喹啉铜的超声波辅助溶剂提取-反相离子对高效液相色谱法的残留分析方法,该方法使用XBridge C18色谱柱和可变波长紫外检测器,并以水相磷酸盐缓冲体系-乙腈(体积比60:40)作流动相;流速为0.8mL/min;检测波长为245nm;保留时间为4.72min;线性相关系数为0.9987,回收率在76.2%~108.7%之间,相对标准偏差在0.6%~3.37%之间,对土壤的最低检出限为0.05mg/kg。

ConclusionThe clinical effect of electronic colorimeter is better than visual colorimeter and is a good supplementary tool for the clinician.

Easy shade Compact电子比色仪比色效果优于目测法,不失为一种比较好的辅助临床医生的比色工具。

Methods Proteins and peptides in CSF were separated by two-dimensional gel electrophoresis(2DE) and ultra-performance liquid chromatographer and identified by matrix assisted laser desorption ionization time of flight mass spectrometry(MALDI-TOF-MS) and electrospray ionization to study differential proteomic expression in the cerebrospinal fluid between patients with Demy- elinative disease and with other neurological diseases.

方法以中枢神经系统脱髓鞘疾病患者的脑脊液为研究对象,分别采用固相pH梯度双向凝胶电泳分离总蛋白质,凝胶经银染显色后,用图像分析软件进行比较分析、识别差异表达的蛋白质,离线应用基质辅助激光解析电离飞行时间质谱得到相应的肽指纹图谱;同时用超高压液相色谱分离酶解肽段,在线采用电喷雾四极杆飞行时间质谱鉴定肽段氨基酸序列;搜索数据库鉴定部分蛋白质。

To achieve high brightness,high contrast ratio and high color saturation of projectors,dichroic thin film of good performance is designed and manufactured.

为达到高亮度、高对比度和色彩逼真的图像输出,设计了性能优越的偏振光分色合色膜系,采用计算机辅助监控方法,膜系的成品率和性能得到了很大的提高。

Then, using the reasoning matrix between the unit colors and individual colors of the polychromatic sets, the reasoning and generation of geometric tolerance types are achieved.

介绍了各层的意义和各层之间的关系,利用多色集合理论对该模型进行描述,通过多色集合统一颜色和个人颜色的推理关系矩阵,实现了计算机辅助形位公差类型的推理生成,为计算机辅助形位公差类型推理的进一步形式化打下了基础。

The hyperchromatic irreversible temperature indicating coatings is prepared,which contains epoxy modified silicon resin as bond,cadmium red as major warm color pigment,phthalocyanine blue and peacock blue as assistant warm color pigment and other fillers.

以环氧改性有机硅树脂为粘结剂,以镉红为主热色颜料,酞菁蓝和海碧为辅助热色颜料,通过加入其他填料助剂,制备了多变色不可逆示温涂料,检测结果表明所研制的示温涂料具有良好的示温性能。

The polarization effects at the LHC can reach 16﹪, therefore, they provide feasible tests of the topcolor-assisted technicolor model.

因此,顶夸克的极化效应提供了一种切实可行的检验顶色辅助的人工色模型的方法。

The reason for this is illustrated by the fact that Thracian units revolted when a rumor spread that they were to be stationed far from Thrace.

例如色雷斯人的辅助部队因为有传言将会驻扎在远离色雷斯的地方而导致哗变,这个事实可以说明上述驻扎方式的理由。

4The Masson trichrome stain can be used for an important method for the observation of the fibrostic cells, The changes of the mast cell could be considered as an assist marker for the observation of the liver fibrogenesis.In addition the concentration of the hepatic hydroxyproline could be used for diagnosis of the hepatic fibrosis. clinical and experimental study.

Masson三色染色可以作为肝纤维化肝硬化组织细胞观察的一种重要方法:肝纤维化过程中,肥大细胞数量的动态变化,可以作为观察肝纤维化变化的一项辅助指标;肝脏羟脯氨酸的浓度变化可以作为肝纤维化的辅助诊断及应用于相关实验的研究。

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It has been put forward that there exists single Ball point and double Ball points on the symmetrical connecting-rod curves of equilateral mechanisms.

从鲍尔点的形成原理出发,分析对称连杆曲线上鲍尔点的产生条件,提出等边机构的对称连杆曲线上有单鲍尔点和双鲍尔点。

The factory affiliated to the Group primarily manufactures multiple-purpose pincers, baking kits, knives, scissors, kitchenware, gardening tools and beauty care kits as well as other hardware tools, the annual production value of which reaches US$ 30 million dollars.

集团所属工厂主要生产多用钳、烤具、刀具、剪刀、厨具、花园工具、美容套等五金产品,年生产总值3000万美元,产品价廉物美、选料上乘、质量保证,深受国内外客户的青睐

The eˉtiology of hemospermia is complicate,but almost of hemospermia are benign.

血精的原因很,以良性病变为主。