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The polymerization reacts from the inverse emulsion . Selecting white oil as continuous medium , Span60 and TX-10 as the complex emulsifier , AM-01﹑(NH4)2S2O4 and NaHSO3 as new-type complex initiator , the copolymerization of dimethylamino ethyl acrylate methyl chloride/acrylamide was developed . The effects of the concentration of monomer﹑emulsifier and initiator﹑ temperature﹑reaction time and pH on the molecular weight﹑intrinsic viscostity﹑conversion ratio and cation degree of copolymer were studied .

以反相乳液为初始聚合体系,油酸失水山梨醇酯Span60和辛基酚聚氧乙烯醚TX-10构成复配乳化剂,白油为连续介质,AM-01、过硫酸铵和亚硫酸氢钠组成新型复合引发体系,进行丙烯酰胺/(2-甲基丙烯酰氧乙基)三甲基氯化铵的反相准微乳液共聚合,研究了单体浓度、乳化剂、反应温度、反应时间、pH等因素对聚合产品分子量、特性粘数、转化率及阳离子度的影响。

Many achievements cant change into practical productivity. There are many reasons for the low translation rate, include the distemperedness of extensive system, the low ability of users ,and the applicability of the results.

导致农业科技成果转化率不高的原因很复杂,既有推广应用体系不健全的问题,也有成果应用主体的科技意识和接受能力差的问题,还与成果本身适用性密切相关。

Results showed that the monomer conversion increased slightly in the presence of the crosslinking agents The size of particles decreased slowh as the amount of cmsslinking agent increased.and the size distribution of the particles broadened at a higher amount of cmsslinking agent Divinyl benzene was more effective than ethyl glycol dimethyl methacrylate to make polymer crosslinked.During alkali treatment process,void latex particles can be obtained when no DVB or less than 0.5 wt% of EGDMA was used,while muhihollow structure was generated when DVB or more than 1.0 wt% of EGDMA was introduced.The volume expansion of the particles decreased with increasing the amount of emsslinkirlg agents.

结果表明,体系中加入交联剂后,单体转化率都有不同程度的提高;随交联剂用量的增加,乳胶粒粒径略有减小,交联剂用量较高时,乳胶粒粒径分布加宽;二乙烯基苯的交联效率稍高于双甲基丙烯酸乙二醇酯;不加入交联剂及EGDMA用量低于0.5%时,处理后乳胶粒呈空腔结构,加入DVB及EGDMA用量高于1.0%时,处理后乳胶粒呈多孔结构,并且乳胶粒体积增量随交联剂用量的增加而减小。

The reaction performance of Pt-Sn-Li/Al_2O3/FeCrAl catalyst was measured,and the properties of the catalyst were characterized.It was found that reaction temperature,LHSV and the molar ratio of hydrogen to alkane have greatly affected on the catalytic performance of the Pt-Sn-Li/Al_2O_3/FeCrAl catalyst.Under a set of optimal reaction conditions,at 0.1 MPa,470℃,the molar ratio of hydrogen to alkane of 4 and LHSV of 0.14 mL·m~(-2)·h~(-1),the dodecane conversion is 6%,and the dodecene selectivity is about 72%.

结果表明:工业催化剂的催化性能比至今实验室制备的γ-Al_2O_3和SBA-15颗粒负载型颗粒状催化剂的性能好;反应温度、液时空速和氢烃摩尔比对Pt-Sn-Li/Al_2O_3/FeCrAl金属基整体式催化剂脱氢性能都有重要影响,最适宜的反应条件是压力为0.1 MPa,反应温度为470℃,进料氢烃摩尔比为4和LHSV为0.14 mL·m~(-2)·h~(-1),此时十二烷的转化率约为6%,十二烯的选择性约为72%;活性组分涂层与金属基体结合良好。

The construction of recombinant UNPase provided a basis for the research on biocatalysed synthesis of adenosine. In comparison with uridine, inosine was the better donar of pentose-1-phosphorate. In the reaction mixture composed of 30 mmolL^(-1)inosine, 10 mmolL^(-1) adenine, and 30 mmolL^(-1) pH 7.5 phosphate buffer and 0.5% wet cells gave a high yield of 85.57% at 60℃ in 3h.

在此基础上研究了不同诱导条件对蛋白表达量的影响分别以肌苷和尿苷为核糖供体研究重组菌转化腺苷的条件,发现肌苷最适合作为核糖供体,在30mmolL^(-1)pH7.5的Na2HPO4-KH2PO4缓冲液中,以30mmolL肌苷和10mmolL^(-1)腺漂呤作底物,加入0.5%基因工程湿菌体60℃反应3h,腺苷的转化率为85.57%。

Results: the results showed that extracts of Artemsia dracunculus L. at the dose of 7.5%,3.75%,1.875% 20 ml/kg.w, can cause a signficant increase of WBC (P.05), thymus index, spleen index,(P.05) phagocytic rate and phagocytic index of phagocyte,(P.05) the transformation rate of the spleen lymphocytes,(P.05) and the serum IL-2(P.05),serum hemolysin concentration 50%( P.05)in immunodepressed mice. Conclusions: extracts oil from Artemsia dracunculus L. can significantly enhance the non-specific, cell-mediated and humoral immunological function in immunodepressed mice.

结果:与模型组比较,椒蒿挥发油各组均能升高小鼠外周血白细胞数(P<0.05);均能升高胸腺指数(P<0.05)、脾指数(P<0.05);均能提高免疫受抑小鼠腹腔巨噬细胞的吞噬率,吞噬指数(P<0.05);均能升高脾淋巴细胞转化率(P<0.05);椒蒿挥发油各组血清IL-2值明显高于环磷酰胺对照组(P<0.05);椒蒿挥发油各组均可升高小鼠的血清半数溶血值(P<0.05)。

Solid superacids SO~2-_4/TiO_2-Al_2O_3 were prepared and used to catalyze the esterfication of iso-octyl alcohol and by-products in oxidization reaction of durene,which were pretreated before esterifying reaction.

考察了催化剂用量、异辛醇与混合酸的质量比、反应时间等因素对酯化反应的影响,确定了较佳的反应工艺条件:m∶m∶m=0.01∶3.18∶1,反应时间为3 h,在此反应条件下预处理后的混合酸转化率可达到99.9%。

Study on the driving forces of land use/cover temporal-spatial change. On the basis of the systematical study on natural and social-ecomic factors including climate, population, technology and affluence status etc. during the past 50 years in this area, the multivariate statistics simulation models of LUCC were developed for two periods of 1950's-1980's and 1986-2000 respectively. Then, the Thiesson polygon method was used to the spatial allocation of soci-economic factors, thereby the spatial relationship between land use degree change and socieconomic factor variation was detected within GIS. Based on the analysis of the integrative characters in different geographical divisions, the electivity index was employed to describe the possible impacts of the natural landscape structure on spatial differentiation of land use transition. At last, correlation analysis between major roads and the distribution of land use change was made.

分析近50年气候资料和人文因子在不同年代的变化特点,系统地研究了气温和降水等自然因子和人口、农牧业发展、经济状况等人文因子对区域土地利用变化的影响;从时间序列的角度分析了50年代至80年代初和80年代中期至2000年两个时段土地利用/土地覆被变化的驱动因子,在相关分析的基础上,分时段建立了区域土地利用/覆被变化的自然-人文影响统计诊断模型;针对不同经济类型区选择典型县,分析近15年土地利用变化外在人文驱动力的区域相似性和差异性;尝试以THIESSEN多边形方法进行社会经济统计数据的空间化处理,探讨了土地利用程度变化与人文因素变化的空间相关关系;以优先指数模型和土地利用类型转化率与距交通干线距离的相关模型分析了景观自然与人文结构对土地利用空间转化过程的影响。

The immuneregulating action that briefed on the electropuncture further regulated each other throughthe neural peptide / neurotransmitter, hormone and CK. 6Function laws, which compare point: Dazhui is good at suppressing theinflammation, while Mingmen is strong to the regulating immune function; it is Feixuethat has regulating action too.

比较腧穴的免疫调节作用规律:大椎穴的抗炎治疗作用(如足爪肿胀率、下丘脑 CRH 含量,血清 TNFα含量)较强,命门穴对于免疫调节作用(如脾脏 T、B 淋巴细胞转化率、IL-2 活性、肾上腺 IL-2 含量等)较强,非穴也具有一定的抗炎免疫作用,但弱于大椎穴及命门穴。

Considering the effect of m any factors when the reaction reaches balance, and in order to increase t he rate of the product, the rate of the changing of sulfate dimthyle, we det ermined the best condition at last. The temperature is between 80 ℃ and 90 ℃. The for mula of the materials is 3∶1~4∶1.The time of reaction is between 4 and 5 hour s.

考虑反应达平衡时诸多因素的影响以及有利于提高产品的产率、硫酸二甲酯的转化率等问题,最后确定了最佳条件:反应温度为80~90 ℃之间,原料配比为3∶1~4∶1,反应时间为4~5 h。

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