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The gasification efficiency increased and the molar fraction of H2 decreased with an increase in the reaction temperature. The decomposition of PVA was more complete at higher temperatures. At 24 MPa, 500℃ and 120 s, the TOC remove rate, the carbon gasification rate and the hydrogen gasification rate were up to 71.46%, 67.97% and 157.24% respectively. A change in the residence time had no significant effect on the molar fraction of gas production but an increase in the residence time could enhance the gasification efficiency of PVA. It was found that the intermediates were mainly alkane, cycloparaffin, aromatic hydrocarbons, and low-molecular weight acids. It was supposed that PVA was degraded into small molecules through breaking of C-C bonds. Parts of the molecules were converted into H2, CO, CH4 and CO2 while some was converted into aromatic hydrocarbons.

过程探索发现:反应温度的升高能提高PVA气化效率,但气体产物中H2的含量随反应温度的升高有所下降;随着反应温度的升高,PVA分解趋于彻底,在压力24MPa、温度500℃、停留时间120s的条件下,TOC去除率、有机碳气化率和氢气化率分别达到71.46%,67.97%和157.24%;停留时间的变化对气体产物含量没有明显的影响,但延长停留时间能提高PVA的气化效率;PVA气化反应中间产物主要为链状烷烃、环烷烃、芳香烃及小分子酸,根据中间产物出现的顺序推测PVA的降解为由C-C键断裂形成小分子物质,这些小分子物质一部分转化为H2,CO,CH4和CO2,一部分形成难降解的芳香族化合物。

The positive expression of Slit2 located in the cytoplast on oligodendrocyte and astrocyte.The positive cells were found at 3d after spinal cord injury, reached peak on 7d after injury, declining after 14d. The change of Slit2 was correlative with the rehabilitation and regeneration of the axon on the forepart period.

免疫组织化学检测:Slit2蛋白定位于星型胶质细胞和少突胶质细胞的胞浆,呈棕黄色染色,于脊髓损伤后第3 d出现,阳性细胞逐渐增多,于脊髓损伤后第7 d,Slit2阳性表达的细胞数达到高峰并趋于稳定,伤后第14 d开始逐渐下降,呈一过性增高。

The effect of tribology factors on bearing vibration is studied experimentally. AR model and WPT are used to processing the normal arid abnormal signals. The results are as follows:1. The vibration of ball bearings is caused by the tribology action of contact pairs of ball and ring races and has the essential of tribo-dynamics. Any factors affecting the tribology characteristics of contact pairs will affect vibration and noise of bearings consequently.2. Vibration characteristics of bearing keep almostly unchanged with the increasing of axial load expecting the increasing of nature frequencies. When radial load increasing with axial load unchanged, nature frequencies keep unchanged but some new vibration peaks appears in the spectrum.3. Vibration amplitudes are damped and nature frequency are enhanced with sufficient lubrication. Vibration and noise of bearings increase obviously and roar can happen and the contact surfaces scratch slightly under insufficient and unclean lubrication state. Bearing will be disabled in a few minutes without any lubrication.4. Bearing vibration is unstable under low speed. With the speed increasing, the vibration become stable and natural frequencies increase slightly but the amplitudes increase apparently.5. Bearing vibration can be excited only by some harmonics ofwaviness without lubrication and by all harmonics with lubrication based on the theoretical analysis.6. The nature frequencies of ball bearings decrease with the increasing sizes. When international clearance increasing, nature frequencies decrease in radial and increase in axial and angular and the amplitudes increase in radial and decrease in axial and angular. When the number of balls increasing, nature frequencies increase and amplitudes decrease. When the pitch diameter increasing, axial nature frequency increase and others nearly keep no change. When outer race groove curvature radius increasing, nature frequencies increase in radial and decrease in axial and angular and amplitudes keep no change in radial and increase in axial and angular. When inner race groove curvature radius increasing, nature frequencies decrease and amplitudes increase.7. The distortion in amplitude and frequency components of bearing vibration signals picked up by the present probe measurement method is founded and right conclusions cannot be achieved by the signals. When accelerometer is rigidly screwed with steel stud onto a flat outer surface of a ball bearing, vibration signal can be got without distortion and the reliability of research on bearing vibration is assured.8. AR model is suitable for large samples of bearing vibration signals, square root of length of samples can be used as the upper limitation of order determination and the FPE order selection criterion is effective. Many advantages of AR spectrum are founded over the classical based on FFT.9. Time-Frequency analysis is necessary for abnormal noise of ball bearings. WPT overcomes the principle shortcomings of STFT and proved to be a best tool to process the abnormal signals.

理论分析和试验研究表明: 1球轴承振动是钢球—滚道接触副中的各种摩擦学作用引起的,具有摩擦动力学的本质,任何对接触副的摩擦学特性有影响的因素都将对球轴承的振动和噪声特性产生影响; 2中心轴向载荷作用下,载荷增大使球轴承的固有振动频率升高,载荷越大同样的载荷增幅引起的频率升幅减小,足够大的中心轴向载荷作用下载荷的变化对球轴承振动的频率特性不会产生明显的影响; 3轴向和径向联合载荷作用下,径向载荷不大时球轴承振动的固有频率基本不变,但是可能引起变刚度激励的非线性振动,出现新的频峰,过大的径向载荷将使部分钢球脱离接触,使球轴承的振动和噪声呈现不稳定状态; 4润滑对球轴承的振动和噪声特性有重要的影响,良好的润滑对振动有明显的抑制作用,润滑不充分时,振动和噪声的水平会有明显增高,一定条件下还会激发接触副中的谐振,发出啸声,造成接触表面的伤害,无润滑干接触时,短时的运转就会损伤接触副表面,使振动和噪声迅速增大,并随时可能引发严重的磨损和卡滞失效;接触副润滑良好时,油膜的"刚化效应"使球轴承振动的固有频率有所提高,润滑剂中含有弥散性污浊时,振动的幅度总体升高,但弥散性污浊不会改变球轴承振动的频率特性;浙江大学博士学位论文:球轴承振动的研究 5低速时,球轴承振动的基本特征呈现不稳定状态,随着转速的提高,球轴承振动的频率特性趋于稳定,固有频率频峰升高; 6理论分析表明,干接触时钢球和滚道表面波纹度的某些谐波分量能激励球轴承的振动,振动的幅值与谐波幅值成正比,实际球轴承中钢球的分布不可能完全均匀,波纹度的激励作用会随时发生;润滑接触的分析表明,波纹度的任意谐波分量均能激励球轴承的振动; 7球轴承的几何和结构参数分析表明,球轴承尺寸越大,径向、轴向和角振动的固有频率越低;钢球中心圆直径增大,球轴承的径向和轴向振动的固有频率基本不变,角振动的固有频率有所上升,振动的幅频特性基本不变;径向游隙加大使球轴承的径向振动固有频率降低,轴向和角振动的固有频率有所升高,径向振动幅频特性的幅值升高,而轴向和角向降低;钢球的数量增多使球轴承振动的固有频率上升,幅频特性的幅值下降,径向振动的幅值下降最为明显;外圈沟曲率半径系数增大使球轴承径向振动的固有频率升高,轴向和角振动的固有频率降低,径向幅频特性基本不变,轴向和角向幅频特性幅值升高;内圈沟曲率半径系数增大使径向、轴向和角振动固有频率均下降,振动幅频特性的幅值均有升高; 8试验对比表明,传感器采用探针式安装时,由于探针接触副接触特性的影响,钡(量得到的球轴承振动信号有失真,采用专门设计和制作的试验球轴承,以固定式安装加速度计,首次测量得到了球轴承振动的真实信号,通过对振动信号的分析,验证了球轴承振动的理论模型; 9)基于时间序列分析的AR模型适用于大样本球轴承振动信号的分析,以样本长度的均方根值作定阶上界,FPE做判阶准则,给出的AR谱光滑,频率分辨率高,是球轴承振动分析的简便而可靠的手段; 10以时频域分析的小波包变换分析球轴承异音信号能够比较好地定位和聚焦异音发生的时间,时间间隔,频率范围,同样是球轴承振动分析的可靠的手段,可用作球轴承故障诊断技术。

Based on the criterion that the volume of estimated parameter's joint confidence region should be minimum, which is a sequential experimental design norm for optimal parameter estimation proposed by Box and Lucas, the observations for the adsorption of n -decane on 5 A molecular sieves were determined sequentially, and it is found that the observations should b.

根据Box和Lucas所提出的使待估参数联合置信域的容积趋于最小的参数估算的序贯实验设计准则,推导得出了正葵烷吸附等温线实验观测点的安排原则,发现对于一元线性模型,实验观测点应安排在可操作区的两端。

This study examined the alumina ceramic membrane to deal with high turbidity water flux changes in the law of decay was found in the early running flux decay rapidly, the latter tends to slow decay, a linear decline in the overall. 51qikan.

Key words: high-alumina ceramic membrane separation of water turbidity摘要:本实验研究了氧化铝陶瓷膜处理高浊度水时膜通量衰减变化规律,发现运行初期膜通量衰减很快,后期衰减趋于平缓,总体成线性下降。

First of all, the FEE project risk identification model based on feature map has been built, which is object-oriented and uses four main methods: direct mapping, project mapping, discrete decomposition mapping, and group mapping to identify the FEE project risk more completely, more scientifically and more efficiently.

在风险评判的过程中,研究利用人工神经网络技术和模糊系统理论,构建了基于"BP神经网络-模糊系统"串联模式的林业生态工程项目风险综合评判模型,从而有效地解决了项目风险的复杂性和非线性带来的多指标综合评价难题,并使用"相对属于"的概念使得风险等级的评判结果更加趋于合理。

The design method to reduce the configuration bend and deformer is adopted,so as to improve the static strength of deputy frame.

优化方案副构架最大等效应力较原方案降低13.96%~34.69%,结构刚度和应力趋于均匀,副构架静强度满足设计要求。

But in the complete degenerate case,the thermo-electric voltage decreases to zero,and in the complete non-degenerate case it isindependent of the statistical properties.

但是在粒子完全兼并的条件下,热电压趋于零;并且在完全非兼并条件下,热电压与统计参数g无关。

Energy consumption of every year become lower, but the degree of changing is degression .

当使用寿命超过50年时,单位面积年能耗值的变化将趋于平缓。

Deliquescent oxygen reduced with longer balance time and greater difference from standard occurred. Before balancing,deliquescent oxygen was close to saturation. The results under 20 ℃ met the standard.

结果: 以蒸馏水和纯净水作为稀释水水源,其BOD5都小于0.2 mg/L,均达到标准;平衡时间增长,当日溶解氧量趋于降低,与标准值的差值也逐渐增大,未经平衡的溶解氧量接近饱和;20 ℃时的测定结果达标。

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Singer Leona Lewis and former Led Zeppelin guitarist Jimmy Page emerged as the bus transformed into a grass-covered carnival float, and the pair combined for a rendition of "Whole Lotta Love".

歌手leona刘易斯和前率领的飞艇的吉他手吉米页出现巴士转化为基层所涵盖的嘉年华花车,和一双合并为一移交&整个lotta爱&。

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