谱色

In addition, the preparation and package and store for standard reference materials of antioxidant BHT are studied.

本论文主要叙述了对工业品防老剂BHT的重结晶提纯和区域熔融提纯(自行设计和制造了区域熔融仪，申请了发明专利)来制定防老剂BHT标准物质的研究：通过实验确定了乙醇重结晶提纯工艺；利用自行设计区域熔融装置，拟定操作规程和技术条件；确定提纯样品的高效液相色谱法和差示扫描量热法的纯度检测条件和实验方法；用高效液相色谱检验BHT标准物质的均匀性、稳定性；分别用高效液相色谱法和差示扫描量热法测定这种标准物质的不确定度评定及两种不同原理检测的定值分析；最后确定标准物质BHT的纯度和合成标准不确定度：标准物质的制备、包装及贮存。

The TLC of them were concordance.They presented the same color fluorescence in the corresponding position at the ultraviolet light(365nm). After the vanillic aldehyde sulphuric acid ethanol solution developed, violet color spots presented at the same place. Reference substance of Polysaccharide presented violet color ,but in the corresponding position the crude and the prepared didn't show the spots . It proves that the chemical constituents of Polygala Root may not have changed after stir-baked with honey.

生远志正丁醇部位色谱和蜜远志正丁醇部位色谱基本一致：紫外灯（365 nm）下二者在相应位置呈相同颜色荧光，香草醛硫酸乙醇溶液显色后二者在相应位置的几个斑点均呈紫罗兰色，且远志皂苷元对照品斑点呈紫罗兰色，而在与其相应位置生远志供试品和蜜远志供试品均未检视到相应斑点。

The sporophore of Cordyceps militaris and the cordycepin content of intermediate products were monitored in the whole course according to the relation between fixed and mobile phases of solvents in a combination system of binary and quaternary solvents, in which the applied methods were successively supercritical fluid extraction, alcohol sedimentation, low-pressure normal-phase silica-gel chromatography, reversed-phase high-performance liquid chromatography and fractional crystallization.

根据溶剂的固定相与流动相之间的相对关系，采用了二元和四元组合的溶剂系统，顺次采用超临界流体萃取法、醇沉法、低压正相硅胶色谱法、反相高效制备液相色谱法、分步结晶法和反相高效液相色谱法，子实体及其中间产物中的虫草素含量变化情况。

Chapter 7 A Fused Silica PLOT Column Prepared with Nanotube Titanic Acid Adsorbent and the Influence of Treatment on Its Behavior In the chapter, the nanotubed titanic acid H〓Ti〓O〓(OH 〓 was synthesized in our laboratory, morphology and structure of nanotubed titanic acid was investigated, a fused silica PLOT column was prepared with used that as a new kind of stationary phase in gas-solid adsorption chromatography.

第七章 钛酸纳米管PLOT石英毛细管色谱柱的制备及热处理对色谱保留性能影响研究在实验室合成了具有较大比表面积和纳米管特性的钛酸纳米管，对其热处理前后的形貌和结构进行了表征，将其作为气-固色谱吸附剂制备出一种新型钛酸纳米管PLOT石英毛细管柱，同时考察了这种纳米管结构的钛酸作为固定相对C〓～C〓烷烃混合物、空气、SF〓以及CO和CO〓的分离能力。

In this paper,the effects of pH,concentration of buffer and triethylamine in mobile phase on chromatographic behavior of oxymatrine,sophoridine and matrine were studied by using ion exchange chromatography and their mechanisms were discussed.

采用离子交换色谱法，以氧化苦参碱、槐定碱、苦参碱3种生物碱为对象，研究了流动相pH、缓冲液浓度及三乙胺加入量等色谱条件对生物碱色谱行为的影响，并探讨了其作用机制。

Reverse-phase chromatography was employed for chiral separation of tropine acid enantiomers on the cellulose tribenzoate chiral stationary phases coated on a small-particle spherical silica support in an eluant system consisting of a mixture of alcohol and water.

摘 要：以乙醇-水流动相，用纤维素-三作为手性固定相对外消旋体托品酸进行了高效液相色谱手性分离考察了不同比例的乙醇-水流动相、不同流速以及用不同醇类酯化对托品酸酯在手性色谱柱上的色谱行为。

OBJECTIVE To determine the relative and absolute molecular weight of working reference substance of Grifolafrondosa beta-Glucan and compare the two analysis methods.

目的测定灰树花倍他葡聚糖工作对照品的相对及绝对分子质量，并对两种分析方法进行比较。方法色谱柱为TSK-G4000PW，流动相为0.7%硫酸钠(含0.02%叠氮化钠)或0.2%叠氮化钠溶液，流速为0.5 mL.min-1，柱温为35℃，高效凝胶渗透色谱法用示差折光检测器，高效凝胶渗透色谱和激光光散射联用法用DNDC仪和激光光散射仪联用。

The optimal carrier gas velocity of prepared SE-30 series capillary chromatographic columns was studied and used to separate isomeric compounds. The efficiency of SE-30 capillary chromatographic columns has been studied with different diameters, film thicknesses and oven temperatures, using n-do-decane, phenol, aminobenzene, and butyl acetate as test samples.

研究自制的SE-30系列毛细管气相色谱柱的载气最佳线速度，并应用于同分异构体的色谱分离分别用十二烷、苯酚、苯胺、醋酸丁酯作试祥在不同载气线速条件下对不同口径、不同膜厚、不同柱温的SE-30毛细管色谱柱的柱效进行考察，并在最佳线速度条件下分离异戊醇、硝基氯苯、硝基甲苯及二乙苯同分异构体体系。

After nucleosides were extracted from urine on phenyl boronic acid affinity chromatography, the analysis was performed on a column (4.6 mm i.d.X250 mm, 5 μm) at 22 ℃ using a lineargradient elution comprising 25 mmol/L KH2PO4 solution (pH 4.55) and 60% methanol in water with UV detection at 260 nm.

通过苯基硼酸亲和色谱法提取尿中核苷，在色谱柱(4.6 mm i.d.X250 mm， 5 μm)上以25 mmol/L磷酸二氢钾溶液(pH 4.55)和60%的甲醇水溶液作为流动相进行二元梯度淋洗，于22 ℃下进行反相色谱分离，260 nm处紫外检测。

The method is a useful tool by applying it to the resolution of model and real chromatographic signals.

通过对模拟色谱和实验色谱的比较，验证了该方法是一个很有用的工具，可以为色谱分析工作提供有力的帮助。

However, as the name（read－only memory）implies, CD disks cannot be written onorchanged in any way.

然而，正如其名字所指出的那样，CD盘不能写，也不能用任何方式改变其内容。

Galvanizes steel pallet is mainly export which suits standard packing of European Union, the North America. galvanizes steel pallet is suitable to heavy rack. Pallet surface can design plate type, corrugated and the gap form, satisfies the different requirements.

镀锌钢托盘多用于出口，替代木托盘，免薰蒸，符合欧盟、北美各国对出口货物包装材料的法令要求；喷涂钢托盘适用于重载上货架之用，托盘表面根据需要制作成平板状、波纹状及间隔形式，满足不同的使用要求。