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The adopt the analytical method announced by environmental protection administration NIEA A715.12B "volatile organic compounds detection method at air - stainless steel canister/analyze mass spectrograph of gaseous phase ", to effectively analyze the air samples inside the station, to find out the space distribution and concentration of volatile organic compounds at the service station.

研究分析方法采用环保署公告NIEA A715.12B「空气中挥发性有机物检测方法-不袗采样筒/气相层析质谱仪法」,期望有效分析加油站内空气样品,对站内空气中各挥发性有机物物种进行定性与定量分析,以了解站内挥发性有机物空间分布与浓度分布情况,提供国内相关资料库与相关立法规范参考。

The method on trans fatty acids analysis in food is very important. The effects of methylate sodium, potassium hydroxide, sulfuric acid and boron trifluoride in methanol and their different concentration and dosage on TFA analysis were studied. The chromatographic condition and the influence of time and temperature on the esterifation of TFA using boron trifluoride in methanol were optimized. A method for analyzing TFA were established by GC based on boron trifluoride in methanol and RT-2560(100m×0.25mm×0.2μm) capillary column.

研究了甲醇钠-甲醇、氢氧化钾-甲醇、浓硫酸-甲醇和三氟化硼-甲醇4种甲酯化试剂的浓度、用量及甲酯化时间和温度对反式脂肪酸检测的影响,优化了色谱条件,建立了以三氟化硼-甲醇法甲酯化,RT-2560(100m×0.25mm×0.2μm)毛细管柱为基础的反式脂肪酸气相色谱检测方法,C18:1-9 t, C18:1-11 t, C18:2-9 t, 12 t和C22:1-13 t 4种反式脂肪酸的最小检出浓度在0.774.08 mg/kg之间。4种反式脂肪酸不同添标浓度回收率为98.44%101.23%,重复测定的相对标准差在0.22%1.31%之间,有较好的准确度和重现性。

Missirlis in article [1]. At the same time, a sufficient condition for convergence of the PSD method is given to be compared when the coefficient matrix A of the linear system Ax = b is a symmetric, positively defective matrix. In §3.2, an example is given to state that the range of our sufficient condition is wider than theorem 3.3 of article [1]. On the other hand, following a.n analogous approach of [14] and starting the functional relationshipwe have a perfect analysis for the PSD method to converge and optimum valves for the involved parameters under different conditions.Under the assumptions that A is a consistent ordered matrix with nonvanishing diagonal elements and the eigenvalues of the Jacobi matrix of A are real,we get necessary and sufficient conditions for the PSD method to convergence.The result is equal to theorem 1 of article [9].Under the same condition, we can see the optimal parameter and of corresponding spectral radius of thePSD method in [8]:(2)When A is a consistent ordered matrix with nonvanishing diagonal elements and the eigenvalues of the Jacobi matrix of A are imaginary or zero,we get necessary and sufficient conditions for the PSD method to convergence.In chapter 3, the optimal parameter and of corresponding spectral radius of the PSD method are given by table 3.3. Moreover, under the assumption 0

Missirlis在文献[1]中定理3.3的不准确,同时给出了当线性方程组Ax=b的系数矩阵A为对称正定阵时,PSD迭代法收敛的一个充分条件与之比较,并且在§2.3中用实例说明了对于一部分矩阵而言本文得到的充分条件广于[1]中定理3.3的充分条件;另一方面,按照文献[14]的方法,我们从PSD迭代法的特征值λ与其Jacobi迭代矩阵B的特征值μ的关系式:出发,在不同条件下对PSD迭代法的收敛性和最优参数以及最优谱半径进行了完整的分析:(1)在系数矩阵A为(1,1)相容次序矩阵且对角元全不为零,其Jacobi迭代矩阵B的特征值全为实数的条件下,给出了PSD迭代法收敛的充分必要条件,此结果与[9]中的定理1等价,此时最优参数及最优谱半径由[8]得:(2)第三章表3.3中给出了,当系数矩阵A为(1,1)相容次序矩阵且对角元全不为零,其Jacobi迭代矩阵B的特征值全为纯虚数或零时的PSD迭代法的收敛范围和最优参数,并且我们可以得到当0

In chapter5, the serial properties of numerical range of operator polynomial are put firstly. Secondly, the relation between numerical range of operator polynomial and n-numerical range are considered. Thirdly, in the light of matrix norm, matrix singular value, the regions and bounds of numerical range and spectrum of operator polynomial are dicussed carefully.

第五章研究了算子多项式数值域的性质、算子多项式数值域与n-次数值域的关系,特别地利用矩阵范数、矩阵的奇异值、非负矩阵的理论、友矩阵为工具,给出了算子多项式数值域及谱的范围全面刻画,并深刻地研究了算子线性束的正则性的等价条件及谱分布。

This paper determined the olfactory respones of Tetranychus viennensis to different plants odors with "Y" olfactometer and petri-dish, volatiles from leaves of different plants were absorbed with SPME and analyzed with GC-MS (gas chromatograph-mass spectrometer). At the same time, the effects of different host plants on the development of Tetranychus viennensis were determined by means of the leaf-dish rearing method , in addition, the contents of some chemicals in the leaves of different plants were also determined.

本文用"Y"形嗅觉仪法和培养皿法测试了山楂叶螨Tetranychus viennenis Zacher对不同植物气味物质的嗅觉反应,并利用固相微萃取SPME吸附、用气相色谱—质谱联用仪GC-MS(gas chromatograph-mass spectrometer)分析了不同植物叶片的挥发性物质成分:同时采用海绵水盘法饲养山楂叶螨,研究了不同植物对山楂叶螨生长发育的影响,并测定了不同植物叶片中一些生化物质的相对含量。

Based on the array signal processing and the eigenstructure decomposition method, the signal subspace and the noise subspace are achieved by reconstructing and decomposing the data matrix collected by the array sensors. By using the orthogonal properties of the two subspaces, the information about the velocities and bearings of spatial moving targets can be exactly obtained.

本文提出一种超分辨的二维谱估计方法,它利用的是阵列处理技术,对天线接收数据进行本征分析,将信号数据张成一个空间并对其进行分解,根据正交原理分割成信号子空间和噪声子空间,构造出噪声本征矢量,利用信号子空间与噪声子空间的正交性,在空间谱上形成极值点,从而达到对方向和速度的二维高分辨率估计。

Chiral separation of D -, L -phenylglycine by RP-HPLC was accomplished by adding a complex of optically active L -Phe-Cu2+ to the mobile phase. Chiral separation mechanism was further elucidated in light of unambiguously assigning the structure of the elutents from RP-HPLC by taking advantage of tandem mass spectrometry due to its unique capability of structural identification of the unknows.

以含 L -苯丙氨酸铜配位络合物的溶液作为手性流动相,采用反相高效液相色谱法拆分了非衍生苯甘氨酸对映体,使用质谱对拆分组分进行了结构鉴定,得到了拆分组分的化学结构,用量子化学计算预测了该结构的最稳定构象。

By means of the semigroup theory, spectrum theory, positive cone theory, integrated equation theory and optimal control theory, we obtain the existence of thresholds of these models, the existence and stability of the infection- free equilibrium and the endemic steady state, and the existence of optimal vaccination strategies, etc.

运用泛函分析中的半群理论、谱理论、正锥理论以及积分方程理论和最优控制理论,系统地研究了这些模型的阈值的存在性,无病平衡态和地方病平衡态的存在性和稳定性,最优接种疫苗策略的存在性等。

On a ZORBAX Stable Bound (2.150 mm, 1.8 m), the rutin、quercitrin、quercitrin-3-O-giucoside and quercitrin-3-O-galactose could be separated completely with 0.05 mol/L potassium dihydrogen phosphate and methanol as mobile phase (40:60,V/V) at a flow rate of 0.3 ml/min and detected with a photodiode array detector .

在色谱柱为ZORBAX Stable Bound (2.150 mm, 1.8 m),流动相为0.05 mol/L的磷酸二氢钾缓冲溶液-甲醇(40:60,V/V),流速为0.3 ml/min,在检测波长为360 nm的色谱条件下,芦丁、槲皮素、槲皮素-3-O-葡萄糖苷和槲皮素-3-O-半乳糖苷分离效果好,方法灵敏度高,重现性好,用于测定雪莲果叶中的上述几种黄酮芦丁型黄酮,效果满意。

The RAPD was used to study the genetic diversity of 19 KinXin series potato cultivars. The result showed that 52 RAPD bands were amplified using 7 primer, among them 43 bands were polymorphic, and 4~9 bands were amplified in each lane. The RAPD analysis indicated that the genetic distance of 19 potato cultivars was between 0.17~0.72, average value was 0.39. When all of the polymorphic bands were analysed by cluster analysis, 19 potato cultivars were classified into 3 groups. The analysis showed that there existed close sibship among the majority of potato cultivars, and the genetic distance between the minority cultivars and the others is longer, which indicate that the genetic basis of KeXin series potato cultivars is wide.

利用RAPD标记技术对19份克新系列马铃薯品种进行了遗传多样性分析,分别提取19份马铃薯品种的DNA,进行随机引物多态性扩增,从1000条随机引物中初步筛选出7条有多态性的引物进行详细研究,每条RAPD引物扩增出4~9条带,共获得52条带,其中多态性条带为43条;19份马铃薯品种的遗传距离介于0.17~0.72之间,平均值为0.39,平均遗传距离介于0.31~0.51之间;聚类分析结果在GS=0.53处可将克新系列马铃薯品种划分为三类,聚类结果与系谱分析基本相符,同时也说明克新系列马铃薯的遗传基础有所拓宽。

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In the United States, chronic alcoholism and hepatitis C are the most common ones.

在美国,慢性酒精中毒,肝炎是最常见的。

If you have any questions, you can contact me anytime.

如果有任何问题,你可以随时联系我。

Very pretty, but the airport looks more fascinating The other party wisecracked.

很漂亮,不过停机坪更迷人。那人俏皮地答道。