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The zymogram and activity of esterase isozyme also varied obviously with the changes of cambial activity.

酯酶同工酶的酶谱和酶活性亦随形成层的活动状态而发生明显变化,可能与木质部细胞分化成熟、细胞壁木质化以及冬季提高植物抗寒性有关。

Kinds of hot pepper materials were used for experiment. The correlation amongphysiological and biochemical characteristics, agronomic characters and resistance todisease characters was studied and the genetic relationship of 12 pepper materials wasidentified by using POD isozymes, the content of capsicin was determined by HighPerformance Liquid Chromatography.

本试验以12个辣椒品种或材料为试材,研究了辣椒生理生化特性、农艺性状和抗病性间相关性;应用POD同工酶对12个辣椒材料,进行亲缘关系的鉴定;高效液相色谱法测定辣椒素。

In this article,the development of molecular imprinted technology and mechanism of chiral recognition were introduced.

介绍了分子印迹技术及其手性识别机理的最新研究进展,对该技术在色谱分离领域的应用现状、存在的问题及解决方法进行了重点评述,并展望了其今后的发展方向。

To study the bioactive components from water soluble extract of the Chinese eaglewood, various column chromatography of Chinese eaglewood led to the isolation of ten compounds. Their structures were elucidated as 2,3-bis(3-hydroxyphenyl)- propan-1-ol (1), [(2R,3R)-3-(4-amino-3,5-dimethoxyphenyl)oxiran-2-yl]methanol (2), 8-chloro-4'- methoxy-5,6,7,3'-tetrahydroxy-2-(2-phenethyl)-5,6,7,8-tetrahydrochromone (3), 4'-methoxy-5,6,7,3'-tetrahydroxy-2--5,6,7,8-tetrahydrochromone (4), the isomer of 4 (5), 4'-methoxy-5,6,7,8-tetrahydroxy-2-(3'-hydroxyphenethyl)-5,6,7,8- tetrahydrochromenone (6), 4'-methoxyisoagarotetrol (7), 6-hydroxy-2-(2-hydroxy-2- phenethyl)-chromone (8), 6-hydroxy-2-(2-phenethyl)-chromone (9), 6-hydroxy-2-(4'- hydroxy-2-phenethyl)-chromone (10), and Guaiacylacetone (11) by means of spectral analysis and comparison with references.

为了进一步发现沉香中具有生理活性的化学成分,本文对国产沉香的水溶性成分进行了研究,从中分离得到11个化合物,通过红外、紫外、质谱、核磁共振(1H-NMR, 13C-NMR, COSY, HSQC, HMBC, ROESY)波谱解析,分别鉴定为:2,3-二(3-羟基苯基)-丙-1-醇(1),[(2R,3R)-3-(4-氨基-3,5-二甲氧苯基)-2-氧化烯基]甲醇(2),8-氯-4'-甲氧基-5,6,7,3'-四羟基-2-(2-苯乙基)-5,6,7,8-四氢色原酮(3),4'-甲氧基-5,6,7,3'-四羟基-2-(2-苯乙基)-5,6,7,8-四氢色原酮(4),化合物3的差向异构体(5),4'-甲氧基-5,6,7,8-四羟基-2-(3'-羟基-2-苯乙基)-5,6,7,8-四氢色原酮(6),4'-甲氧基异沉香四醇(7),6-羟基-2-(2-羟基-2-苯乙基)色原酮(8),6-羟基-2-(2-苯乙基)色原酮(9),6-羟基-2-(4'-羟基-2-苯乙基)色原酮(10)和Guaiacylacetone (11)。

Results As compared to DM control group, levels of GSP, myocardial enzymes and myocardial Ang Ⅱ were much lower in APS group, while levels of insulin, C-peptide and plasma Ang Ⅱ were the same. Levels of expression of collagen Ⅰ and the ratio of collagen Ⅰ/collagen Ⅲ in APS group were lower than those in DM group. APS group showed lower levels of chymase mRNA expression and activity than those in DM control group, while there was no diference in ACE mRNA expression and activity between the two groups.

结果 APS组血糖、糖化血清蛋白、心肌酶谱和心肌Ang Ⅱ水平较DM组显著下降,胰岛素、C肽、血浆AngⅡ水平和DM组无差异;APS组心肌Ⅰ型胶原表达和Ⅰ/Ⅲ型胶原比值较DM组显著下降;APS组chymase mRNA表达和活性均显著低于DM组,ACE基因的表达和活性与DM组无显著性差异。

High-resolution two-dimensional polyacrylamide gel electrophoresis, followed by computer-assisted analysis was used to screen the proteins pattern between normal and Ng mutant colleterial gland to find quantitative and qualitative difference in proteins expression.

分别对家蚕的正常及Ng突变体雌蛾性附腺分泌部组织的蛋白质进行提取,并采用双向凝胶电泳和计算机辅助分析方法,对提取的蛋白质混合物进行分离和比较分析,并对主要差异表达的蛋白质用质谱鉴定。

High-resolution two-dimensional polyacrylamide gel electrophoresis, followed by computer-assisted analysis was used to screen the proteins pattern between normal and Ng mutant colleterial gland to find quantitative and qualitative difference in proteins expression.

分别对家蚕的正常及Ng突变体雌蛾性附腺分泌部组织的蛋白质进行提取,并采用双向凝胶电泳和电脑辅助分析方法,对提取的蛋白质混合物进行分离和比较分析,并对主要差异表达的蛋白质用质谱鉴定。

The range of MIC90 was-10 μg/ml. The susceptibility rates of the strains to other 10 agents were nearly or equal to 0%. Different plasmid profile strains had almost the same antimicrobial susceptibilities. 25 strains (including 18 strains harboring 34-80×106 plasmids) selectively examined to have no self-transmissible conjugative plasmid.

88.6%,MIC90为-10 μg/ml),对卡那霉素等其余10种药物的敏感率很低或不敏感,不同质粒谱菌株对药物的敏感性几乎相同,对包括 18株含34-80×106质粒在内的 25株菌进行接合转移试验,未检出传递性耐药性质粒。

Keywords alkane; cyclane ;aliphatic alcohol;aliphatic ketone;gas chromatography retention index;molecule shape index;electrotopological state index

烷烃;环烷烃;脂肪醇;脂肪酮;色谱保留指数;分子形状指数;电性拓扑状态指数

Potassium salt of dicyclopentadienyl dicarboxylate DCPD(COOK2 was applied to CPE as crosslinking agent and a crosslinked product with 81.79% gel content was obtained in solution reaction.

以溶液反应法研究了CPE与DCPD:的交联反应,制得了凝胶量在80%以上的共价交联CPE,考察了不同牌号CPE、催化剂及其用量、反应温度、反应时间及其交联剂用量对CPE凝胶形成量的影响;通过对比实验和IR谱图证明了该凝胶确由CPE与DCPD:经双端醋化反应生成;通过反应溶解性实验验证了共价交联CPE的热可逆转化特性。

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