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In Chapter 1, the ubiquity of chiral phenomena and its important role in various disciplines, the methods for enantiomer separation, the principles of direct chromatographic separation of enantiomers and the status of chiral CGC are discussed and/or reviewed.

第一章论述或评述了手性特征的普遍性和在众多学科中的重要性、手性分离方法、色谱直接分离手性化合物对映体的基本理论、手性气相色谱研究现状。

A region superresolution spectrum estimation method based on coventional DFT computation is presented for obtaining one dimensional range profile, which has the advantages of real-time in computation and robustness under clutter and noise background over general superresolution methods. A iterative extropolation method based on both priori knowledge provided by conventional DFT spectrum and matching filtering process of target return data is also presented for range profile processing, which has the advantages of robustness in improving range resolution, suppressing clutter and noise.

在目标一维距离成像谱估计中,提出了以常规DFT为基础的邻域超分辨谱估计方法,它与普通超分辨算法相比,具有实时性强、在杂波与噪声背景中稳健性好的优点;在外推成像处理中,提出了以常规DFT目标结构图像为约束条件并结合目标信号准匹配滤波处理的迭代外推算法,其优点是稳健性好,能适度地提高距离分辨力但保留适度的抗杂波抗噪声能力。

Firstly,by using the estimating methodfor the compact embedding operators(from weighted Sobolev space to the weighted〓space),we obtain a necessary and sufficient condition for the discreteness of thespectrum of certain differential operators.Secondly,based on the property of thespectrum of difinitizable operators on the Krein space,we consider the left definitedifferential equations with middle deficiency indices,and give a completecharacterization for self-adjoint(J-self-adjoint)differential operators in theindefinite inner product space 〓.Especially,we prove that all the J-self-adjoint differential operators are definitizable.

我们首先运用加权Sobolev空间到加权〓空间嵌入算子紧性的判别方法,证明一类加权自伴微分算子具有离散谱的充要条件;然后,基于Krein空间上可定化算子谱的性质,对于具中间亏指数的左定型微分方程,建立其相应的微分算式在不定度规空间〓上所生成自伴算子的完备性刻画(特别证明了J-自伴微分算子具有可定化性)。

For the one-dimensional p-Laplacian with indefinite weights, four sequences of periodic and anti-periodic eigenvalues are given by introducing the rotation number function, and these eigenvalues are the endpoints of the preimage intervals of the rotation number function at nonnegative integers.

本文以带变号权函数和带变号势函数的一维p-Laplacian为基本模型,系统地阐述了特征值的旋转数方法、带正权Dirichlet特征值的最佳估计、特征值在正则和奇异渐近半线性方程的可解性中的应用、Fucik谱的旋转数方法以及Fucik谱在周期解的扭转性和多解性中的应用。

The quantity computed is the expected clutter power at the output of any specified range gate by the method of integrating reflected energy between constant Doppler loci in range-gate circles with a model of sum and difference antenna gain pattern for APAR. Base on the analyzing of APAR terrain clutter spectrum, Rayleigh, Correlated Log-Normal and Weibull distribution terrain clutter of APAR general pulse signal was simulated with the method of zero memory nolinearity transform.④The Doppler frequency of target echo is simulated on video frequency in this dissertation.

该软件采用了用C语言建立框架结构,而在程序高重复部分和有运算速度要求的地方,用汇编语言编写具有高并行能力程序的方法,不仅满足了系统高运算速度和实时性的要求,也使得软件系统结构模块化,代码具有良好的维护性和重用性;③对机载相控阵雷达HPRF、MPRF的和、差通道地面杂波功率谱进行了较为全面的研究,通过建立由四个子波束构成的机载相控阵雷达杂波和差波束天线方向图数学模型,选取体现高度线杂波的修正的地面后向散射模型,以载机平飞为例,采用沿距离门——等多普勒线区域积分的方法,得到了杂波功率谱,并利用零记忆非线性变换法实现了机载相控阵雷达常规脉冲情况下瑞利分布、对数正态分布和韦布尔分布地面杂波的模拟;④提出了采用在视频上对目标回波的多普勒频率进行模拟的方法。

Due to existing signal processing technology's shortage such aslow measurement, narrow measurement range precision and other poor performance, we introduced a high-precise signal processing technology:firstly,to get power spectrum with Hanning windowed Welch modified periodogram, search its peak value frequency;secondly, to apply zooming analysis via Goertzel algorithm;at last,to get a highly precise doppler frequency with energy centrobaric rectifying algorithm.

针对存在的缺点,本文提出了一种应用于激光多普勒测速的高精度信号处理技术,即首先利用加Hanning窗的Welch修正周期图算法得到信号功率谱,搜索其谱峰值频率,接着利用Goertzel频谱细化算法对搜索的谱峰进行细化分析,再引入能量重心频谱校正算法对细化后的谱峰进行校正分析,从而将离散频谱分析算法、频谱细化算法和频谱校正算法三者有机结合起来,充分发挥各自的优点:通过加Hanning窗的Welch修正周期图算法快速得到功率谱及峰值频率,通过Goertzel算法获得分析频带的高分辨率频谱,然后通过能量重心校正算法对细化后的频谱进行高精度校正,这样不仅保证了算法的高效性,而且大大提高了分析的精度。

This project will mass produce high purity paralytic shellfish toxins using a combination of photobioreactor, HPLC-MS and NMR approaches, and develop novel PSTs detection method based on fluorescent characteristics of crown ethers, and finally apply this product and method for PSTs monitoring in

本项目将分离纯化中国沿海典型麻痹性贝毒C1/C2,GTX1/4,GTX2/3和GTX5,运用液相色谱-质谱联用技术和核磁共振等方法定量毒素纯度和含量,制备高纯度毒素标样,建立麻痹性贝毒的大规模生物生产技术;合成筛选适宜的毒素化学传感器—冠状醚,优化毒素和冠状醚的反应体系,结合多重时间分辨荧光技术,建立麻痹性贝毒多重时间分辨荧光检测技术,并用于水产品中麻痹性贝毒的检测。

This project will mass produce high purity paralytic shellfish toxins using a combination of photobioreactor, HPLC-MS and NMR approaches, and develop novel PSTs detection method based on fluorescent characteristics of crown ethers, and finally apply this product and method for PSTs monitoring in seafoods.

本项目将分离纯化中国沿海典型麻痹性贝毒 C1/C2 , GTX1/4 , GTX2/3 和 GTX5 ,运用液相色谱-质谱联用技术和核磁共振等方法定量毒素纯度和含量,制备高纯度毒素标样,建立麻痹性贝毒的大规模生物生产技术;合成筛选适宜的毒素化学传感器—冠状醚,优化毒素和冠状醚的反应体系,结合多重时间分辨荧光技术,建立麻痹性贝毒多重时间分辨荧光检测技术,并用于水产品中麻痹性贝毒的检测。

A detailed discuss in selection of detector, chromatographic column, method of preconcentration in gas chromatographic determinations, which is the most practical technique among analysis of sulphur-containing compounds, and prospects of analytical testing techniques for volatile organic sulfur in water are presented in this paper.

气相色谱技术是测试该类物质的实用技术,从检测器的选择、色谱柱的选择和预富集方法三个方面详细介绍了采用气相色谱分析水中微量挥发性有机硫化物过程中遇到的主要问题和解决方法,并展望了水中微量挥发性有机硫化物分析测试技术的发展方向。

A detailed discuss in selection of detector, chromatographic column, method of preconcentration in gas chromatographic determinations, which is the most practical technique among analysis of sulphur-containing compounds, and prospects of analytical testing techniques for volatile organic sulfur in water are presented in this paper. Contents

气相色谱技术是测试该类物质的实用技术,从检测器的选择、色谱柱的选择和预富集方法三个方面详细介绍了采用气相色谱分析水中微量挥发性有机硫化物过程中遇到的主要问题和解决方法,并展望了水中微量挥发性有机硫化物分析测试技术的发展方向。

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