谱

Changes of endogenous ZT and GA3 in stems and leaves of spring shoots of citrus Satsuma on the stock of Poncirus trifoliuta during the period o flower bud formation were determined by HPLC and TLC respectively.

用高效液相色谱法和薄层荧光色谱法分别测定了宫川温州蜜柑花芽分化过程中内源玉米素和赤霉酸(GA3)的含量变化。

An ion-chromatography method was described for the determination of Cu, Ni and Zn in scandium oxide.

离子色谱法测定氧化钪中的铜、镍、锌潘炳贤，周春山，熊兴安，王艳，徐卫红（中南工业大学化学化工新技术研究所，长沙，410083）摘要介绍了离子色谱法对氧化钪中的Cu，Ni，Zn等元素的分离和测定。

Results It's indicated that the improved cepstrum method can minimize the influence of transducer impulse response and tissue scatterer properties. It also can be easily implemented with little computation.

结果 改进的倒谱方法能有效减少超声换能器脉冲响应和组织散射特性对倒谱的干扰，而且实现简单，计算量小。

For radical polymeric PMMA, there were two main degradation models in N〓: the end-chain scission model and the random chain-breaking model.

采用质谱和色谱研究了PMMA和单体MMA在快速升温条件下，在不同温度和不同气氛中的热分解以及燃烧反应，并由此推测了PMMA在空气中燃烧反应的主要历程。

Then it analyzes the unstable and stable signals by applying Short Term Fourier Transform , Wavelet Packet Auto-Regressive Model Spectrum , the Second Order Cyclostationary Spectrum as well as chaos-fractal theory, extracts the fault features of analysis objects.

采用了短时Fourier变换、小波包AR谱、二阶循环谱方法及混沌分形理论分析了稳态和非稳态振动信号，提取出了分析对象的故障特征。

The essential oil from stem, flower, leaf, root, nutlet and seedcase of Cleidiocarpon cavaleriei were extracted and its chemical constituents were analyzed by GC-MS.

用气相色谱-质谱对挥发油化学成分进行分析，并应用面积归一化法测定各成分的相对百分含量。

Angular spectral is spectral value map formed by estimating semblable coefficients of fast and slow shear wave or the variation of amplitude ratio of fast and slow shear wave with times and angles at a specified space point based on semblable theory of fast and slow shear wave, the angle value of this space point at a given time can be got by picking the maximum of angular spectral; the study reveals that fast and slow shear wave with different polarization direction should be separated using different rotation formula, eight formulas of separating fast and slow shear wave using clockwise rotation and counterclockwise rotation have been derived, and gained energy assignment rule and phase coincidence rule, in real data estimation, the rotation formula used for separating fast and slow shear wave can be uniquely determined on the two discriminating rules. On the basis of semblable theory of fast and slow shear wave, the delay time corresponding to the maximum of semblable coefficients at a specified point in a given time window is the delay time of fast and slow shear wave, delay time section of fast and slow shear wave can be got by moving space point and smoothing time window. The vertical variation values of delay time of fast and slow shear wave reflect the effect degree of vertical fractured reservoir on fast and slow shear wave which is defined as anisotropic coefficient, and section map of anisotropic coefficient can be obtained.

角度谱就是利用快慢横波的相似性原理，在某一空间点求出快慢横波的相似系数或快慢横波的振幅比值随着时间和角度的变化而形成的谱值图，拾取其极大值就得到该空间点某一时间的角度值；在研究中发现分离不同偏振方向的快慢横波应该采用不同的旋转公式，推导出了利用顺时针旋转和逆时针旋转分离快慢横波的八个公式，并给出了能量分配准则和相位一致性准则两个判别准则，在实际计算中利用这两个判别准则能唯一地确定分离快慢横波的旋转公式；根据快慢横波的相似性原理，在某一给定点和给定时窗内最大相似系数对应的延迟时间就是快慢横波的延迟时间，随着空间点的移动和时窗的滑动就可以得到快慢横波延迟时间的剖面图；快慢横波延迟时间与慢横波传播时间的比值定义为裂缝密度，并求出了裂缝密度剖面图；快慢横波延迟时间纵向上的变化值的大小反映了纵向上裂隙层对快慢横波影响的大小，定义为各向异性系数，并求出了各向异性系数的剖面图。

Compound 3 was obtained from Senecio kaschkarovii for the first time and, Compound 4 is a new compound. Compound 4s absolute configuration had been determined by CD, NMR and NOE.

通过CD谱及NMR、NOE差谱研究了化合物4的立体化学，并按Dreiding models构筑了该化合物分子的立体化学结构，确定该化合物应为Non-steroid型构象。

The procedure involves the use of a capillary chromatography column (HP-INNOWAX, 30 m×0.53 mm×1.0 um) and FID detector. The result showes that 4 solvents are completely separated, the regression equation coefficients of 4 solvents are above 0.99, the recoveries are 90%~110% and the RSDs are less than 2.0% respectively.

实验的色谱柱为HP-INNOWAX(30 m×0.53 mm×1.0μm)毛细管色谱柱，检测器为氢火焰离子化检测器。4种溶剂均达到完全分离，各溶剂线性实验所得回归方程的相关系数均大于0.99，加标回收率为90%~110%，RSD.0%(n=6)。

In the region upstream of vortex breakdown, the sectional streamlines emanating from the leading edge spiral inward to primary vortex and in the region downstream of the breakdown, on the other hand, the streamlines separating from the leading edge are not entrained into the vortex core in the instantaneous sense. Along the axis, the topology of the primary vortex alters several times starting from stable focus near the apex to unstable focus, and lasts back to stable focus near wake edge, the stable hmit cycle and unstable limit cycle are shown in this evolution.

发现在截面流线谱中，即使奇点的类型、数目及位置相同，奇点的连接方式也有可能不同；旋涡破裂点前，主涡由来自前缘的力线卷绕而成，主涡焦点与前缘半鞍点相连，旋涡破裂后，来自前缘的力线不再卷入主涡，主涡焦点与对称面上的鞍点相连：在流体由翼尖流向后缘的过程中，截面流线谱的拓扑结构发生了多次变化，主涡焦点相继由稳定状态转变为不稳定状态，最后又转化为稳定状态，并先后出现了稳定的极限环及不稳定极限环。

It has been put forward that there exists single Ball point and double Ball points on the symmetrical connecting-rod curves of equilateral mechanisms.

从鲍尔点的形成原理出发，分析对称连杆曲线上鲍尔点的产生条件，提出等边机构的对称连杆曲线上有单鲍尔点和双鲍尔点。

The factory affiliated to the Group primarily manufactures multiple-purpose pincers, baking kits, knives, scissors, kitchenware, gardening tools and beauty care kits as well as other hardware tools, the annual production value of which reaches US$ 30 million dollars.

集团所属工厂主要生产多用钳、烤具、刀具、剪刀、厨具、花园工具、美容套等五金产品，年生产总值3000万美元，产品价廉物美、选料上乘、质量保证，深受国内外客户的青睐