谱

The Diels-Alder cycloadditions of [60] fullerene for preparation of optical limitingmaterials are discussed in chapter 3 and 6. Soluble cycloaddition derivatives of 〓aresynthesized by the reaction of 〓 with indene,1,1'-biindene andcyclopentadiene derivatives.〓Particular, the Diels-Alder cycloaddition of 〓 with1,1'-biindene under controlled conditions affords the stable monoadduct 〓〓of novel structure, which was confirmed by HPLC, FTIR, FD-MS,〓NMR,〓 NMR, HMQC and HMBC spectra, Its two bridgehead cage carbons resonate at70.91ppm, The 〓 NMR spectra showed 38 lines consistent with the 〓 symmetryassociated with [6,6] addition. The 〓 shows similar optical limitingproperties to that of 〓 in toluene for 8ns laser at wave length 532nm. Moreover, thehigh solubility of this adduct in polar solvents such as THF, acetone enables itsincorporation into sol-gel glass matrix. The thin films prepared via the sol-gel methodshow improved OL behaviour compared to those of 〓. The langmuir-Blodgett filmformation and uv-visible absorption of 〓 are also investigated. LBmonolayer of this compound is prepared on the air-water interface at 〓 mol/l. In chapter 4, three water-soluble derivatives of [60] fullerene: fullerol(1), theaddition product (2)of fullerol (1)with polyvinylpyrrolidone and fumaric acidderivative of 〓(3) are synthesized and characterized.

通过Diels-Alder环加成反应，用茚〓和1，1'-联茚〓及取代茂合成了一系列可溶性的〓环加成衍生物，发现可控制反应条件，使1，1'-联茚与〓反应，并高产率地得到具有新颖结构的单加成物，用HPLC、FTIR、FD-MS 及〓、HMQC、HMBC等多种波谱技术对其结构进行表征，测得它的两个〓杂化的桥头碳的化学位移为〓ppm，证明生成的衍生物为6∶6闭式环加成，〓NMR谱中共给出38个信号，表明〓联茚衍生物分子具有〓对称性；在波长532nm，脉冲宽度8ns的激光下，〓联茚衍生物的甲苯溶液的光限幅性能与〓的甲苯溶液相近，由于〓联茚单加成衍生物熱稳定性好，在四氢呋喃，丙酮等极性溶剂中溶解性好，能分别均匀地掺入溶胶-凝胶中，已发现它的溶胶(so1)光限幅性能优于纯〓的光限幅性能；使用Langmuir-Blodgett技术将〓联茚衍生物在空气和水的界面进行了LB单层膜和多层膜实验以及UV-Vis吸收谱研究，通过等温压缩曲线测试，证明浓度为〓〓时，〓联茚衍生物能够形成单层膜。

For AA8090 alloy without exfoliation , the EIS is comprised by a depressed capacitive arc at high frequency and an inductive arc at low frequency, and the inductive component weakens and also disappears with time.

结果表明，剥蚀发生之前，AA8090合金电化学阻抗谱由一个压缩的高频容抗弧和一个低频感抗弧组成，且低频感抗成分随浸泡时间延长而减弱并消失；一旦发生剥蚀，其电化学阻抗谱即由一个高频和一个低频两个容抗弧组成。

The experiments indicate the inkblot from the same brand and the same batch of carbonic ink is similar, but different notably from the different brand or the different batches.

结果表明同品牌同批次产品墨迹的谱图基本相同，而不同品牌或同品牌不同批次产品墨迹的谱图有明显差异。

Firstly,by using the estimating methodfor the compact embedding operators(from weighted Sobolev space to the weighted〓space),we obtain a necessary and sufficient condition for the discreteness of thespectrum of certain differential operators.Secondly,based on the property of thespectrum of difinitizable operators on the Krein space,we consider the left definitedifferential equations with middle deficiency indices,and give a completecharacterization for self-adjoint(J-self-adjoint)differential operators in theindefinite inner product space 〓.Especially,we prove that all the J-self-adjoint differential operators are definitizable.

我们首先运用加权Sobolev空间到加权〓空间嵌入算子紧性的判别方法，证明一类加权自伴微分算子具有离散谱的充要条件；然后，基于Krein空间上可定化算子谱的性质，对于具中间亏指数的左定型微分方程，建立其相应的微分算式在不定度规空间〓上所生成自伴算子的完备性刻画（特别证明了J-自伴微分算子具有可定化性）。

Firstly, applying spectral factorization to minimize an integral square performance criterion containing tracking error and control energy, an optimal control law for the nominal model is derived on condition of control energy constraint. Then, for model uncertainty, using spectral factorization to minimize the variance of the actual system performance from the nominal performance over all frequency range, a robust controller design method is abtained, which has optimal robustness of the system nominal performance to model errors.

首先针对控制对象的标称模型应用谱分解最小化一个包含跟踪误差和控制能量在内的积分平方性能指标，导出一个控制能量约束条件下的最优控制律；然后再针对模型不确定性应用谱分解最小化实际系统性能和标称性能在整个频段上的方差，得到一个鲁棒控制器的设计方法，可使系统的标称性能对模型误差具有最优的鲁棒性。

In addition, we find that the spectral index at radio bands varies with time, showing the form of inverse spectrum.

另外我们发现，谱指数随着时间而发生变化，这种变化在5GHz、8GHz和14.5GHz之间多表现为逆谱的形式。

The main contents include: Some preliminary theory (introduction to Sobolev spaces and variational formulations for differential equations); finite element methods for one-dimensional elliptic problems; the construction methods for general finite elements; error estimates for interpolation operators and inverse inequalities for finite element spaces; a priori and a posteriori error estimates for the finite element method for high-dimensional elliptic problems; some typical spectral methods for partial differential equations; error analysis for the spectral approximation for some linear and nonlinear partial differential equations.

主要内容有：准备知识（Sobolev空间的基本概念和主要结果，微分方程的变分描述）；一维椭圆型方程有限元方法；一般有限元的构造；插值算子误差估计和逆不等式；高维椭圆型方程的先验、后验误差估计；求解偏微分方程的几类谱方法；线性与非线性问题谱逼近的误差分析等。

The relationship between the inverse number density of particle of the laser transition levels and the discharge condition such as the discharge current, the He pressure and the temperature of Cd-reservior has been achieved. The discharge condition for obtaining maximum laser output was theoretically achieved.

分析了441.6nm谱线的激发机理及各种粒子的相互作用过程，导出了441.6nm谱线跃迁能级激励的理论模型及其粒子数密度速率方程，得到了粒子反转数密度与放电电流、氦气压强和镉炉温度等放电条件的关系，从理论上，定量得出了获得最大输出功率时的放电条件。

It gives an amplitude spectrum as the inverse of a biased amplitude spectrum of the CHF, and a phase spectrum as the phase spectrum of the CHF.

该滤波器的振幅是圆谐滤波器的振幅谱加偏移量后的逆函数，位相是圆谐滤波器的位相谱。

This paperexplores the way to analyze the time domain amplitude spectrum , frequency domain power spectrum and inverse frequency spectrum todetect faults with AI technology, especially expert system.

本文探讨了利用智能技术特别是专家系统来进行旋转机械的时域幅值谱、频域功率谱及倒频谱分析，从而进行故障诊断的方法和途径。

I am accused of being overreligious," she said in her quiet, frank manner,"but that does not prevent me thinking the children very cruel who obstinately commit such suicide.""

客人们在卡罗利娜·埃凯家里，举止就文雅一些，因为卡罗利娜的母亲治家很严厉。

Designed by French fashion house Herm è s, this elegant uniform was manufactured in our home, Hong Kong, and was the first without a hat.

由著名品牌 Herm è s 设计，这件高贵的制服是香港本土制造，是我们第一套不配帽子的制服。