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In comparison with the pure standards and the retention indices RI(subscript s reported in the literature, a total of 302 volatile compounds were identified in Changyu XO brandy, including 30 alcohols, 35 aldehydes and ketones, 20 carboxylic acids, 104 esters, 24 substituted benzenes and derivatives, 14 phenolic derivatives, 14 acetals, 16 furan derivatives, 22 terpenic and norisoprenoidic derivatives and 23 others.

实验先采用液-液萃取方法提取张裕XO级白兰地的挥发性成分,然后将酸性成分与碱性和中性成分分离,再采用柱色分离手段将其分离为若干个级分并浓缩,采用气相色-质、标准品比对、保留指数值比较等方法对分离得到的各级分中的成分进行了鉴定,在白兰地中共鉴定出302种挥发性成分,包括醇30种、醛酮类35种、酸类20种、酯类104种、苯同系物及其衍生物24种、酚类14种、缩醛14种、呋喃类16种、萜烯类22种和其他物质23种。

The neutral/basic fraction was furthermore separated into 4 fractions using silica gel normal phase chromatography, and each fraction was then concentrated and analyzed using gas chromatography-mass spectrometry. In comparison with the pure standards and the retention indices reported in the literature, a total of 302 volatile compounds were identified in Changyu XO brandy, including 30 alcohols, 35 aldehydes and ketones, 20 carboxylic acids, 104 esters, 24 substituted benzenes and derivatives, 14 phenolic derivatives, 14 acetals, 16 furan derivatives, 22 terpenic and norisoprenoidic derivatives and 23 others.

实验先采用液-液萃取方法提取张裕XO级白兰地的挥发性成分,然后将酸性成分与碱性和中性成分分离,再采用柱色分离手段将其分离为若干个级分并浓缩,采用气相色-质、标准品比对、保留指数值比较等方法对分离得到的各级分中的成分进行了鉴定,在白兰地中共鉴定出302种挥发性成分,包括醇30种、醛酮类35种、酸类20种、酯类104种、苯同系物及其衍生物24种、酚类14种、缩醛14种、呋喃类16种、萜烯类22种和其他物质23种。

The result showed that epidemic strain of various samples had variation, and antibacterial spectrum of the antibacterials distinguished anlage antibacterial spectrum.

第三,以药物为依据,观察各类抗菌药物的抗菌变化。结果:各标本流行菌株有所变化,各抗菌药物的抗菌与其原始抗菌有所不同。

The differences of zymograms were significant between three blackfly species and each species had its own special zymogram. The main band among intraspecific individuals or between the larvae and pupae was alike, however, other enzyme bands were different.

结果 3蚋种的EST同工酶酶共显示10条酶带,种间存在明显差异,具有各自的特征性酶,种内个体之间、幼虫与蛹之间酶主带相同,非主带略有差异。

In this thesis, two chemical structural models were constructed based on several structure parameters derived from FTIR and 13C NMR data, which were processed by curve-fitting and curve-resolved. Modified models were obtained by simulation oftheir molecular vibration spectra using Cerius 4.6/IR module andthe structural parameters from 13C NMR. Potential energy, bondenergy and non-bond energy of the minimum-energy conformations of coal macromolecules were calculated by molecular mechanics calculation and molecular dynamics simulation. These results demonstrate the importance of hydrogen bonding and van der Waals interactions in the formation and stabilization of coal macromolecular structure, and a strongest tendency of hydrogen bonding interactions to increase with the coal molecules but the Coulombs force.

本文运用煤结构的傅立叶红外光和固体核磁共振碳~(13C NMR测试方法所得的结果,经过图分峰、分析,计算出若干表征煤大分子结构参数,并综合前人的经验和共识,利用计算机分子绘图软件系统构建了表征两种褐煤的化学结构模型,在Cerius~2 4.6/IR模块中计算了分子振动红外光,同时结合碳所计算的分子结构参数拟合、修正了该结构模型,得到了能表征这两种煤样的分子结构模型,作为用分子动力学模拟和量子化学计算的初始结构模型。

Hydrogen gas discharge source was used to bombard target of non-crystalloid deuterate polyethylene polymethylmethacrylate,etc.The scattering spectrum was measured.

引出氢气放电产生的射线和粒子流打在非晶聚氘乙烯C2D4和有机玻璃C5H8O2等靶上,测得其散射上有多条尖锐的X线,其中除一条外都是原始中没有的。

ESI-MS and HPLC were used to determine molecular weight and composition of amino acids of methionine enkephalin and to check its purity to establish its quality standard.

采用液相色-质联用仪检测蛋氨酸脑啡肽分子量和鉴别蛋氨酸脑啡肽的各氨基酸组成,反相高效液相色测定蛋氨酸脑啡肽含量。

The 9 kinds of elements, 6 kinds of fatty acids and 15 kinds of amino acids in the reddish fish scale were studied by ICP-AES, GC-MS and HPLC in this paper.

用等离子体发射光法、气相色-质联用分析法和高效液相色法分别测定了金线鱼鱼鳞中9种元素、6种脂肪酸和15种氨基酸的含量。

The composition of fatty acids in oil and fat was detected by gas chromatography and fire ionization detector at home,however,the reports about the separation and detection of triglyceride in oil and fat were very little.

对油脂的分析,国内主要是采用气相色分离和火焰离子化检测器检测其中的脂肪酸组成,而对甘油酯的分离和检测报道较少,国外研究者利用色和质联用技术对甘油三酯的分离和检测做了大量的研究。

Our company also supply SunTech column, the column theoretical plate number up to 80,000 / m and above, PH 2.0-9.2 around tailing factor 0.90-1.12, while the prices of imports of the same specification, only the other half of the column .

我公司另外还供应suntech 色柱,此色柱理论塔板数可达80000块/米以上,PH 2.0-9.2左右,拖尾因子0.90-1.12,而价格只有其他相同规格进口色柱一半。

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