谱

A series of bulkily substituted ferrocenium triiodides with general formula (RC5H4)2FeI3 have been synthesized and characterized by elementary analysis, IR spectrum, mass spectrum, ESR spectrum, Mossbauer spectrum and conductivity.

通过元素分析，红外光谱，质谱，顺磁共振谱，穆斯堡尔谱和电导率对这些化合物进行了表征。

A static headspace-gas chromatography-mass spectrometrymethod was used to analysis volatile compounds from the six kinds of Bupleurum from different areas.

运用静态顶空毛细管气相色谱质谱法对6种不同产地柴胡的挥发性成分进行了检测，并运用质谱检索和保留指数相结合的手段对检出的挥发性成分进行定性，6种柴胡中定性相对含量大于0.2%的挥发性成分60种。

The main constituents C_1 and C_2 of Gentaminycin were evaluated in per centage by nuclear magnetic resonance spectrometry and comparison of pre - sa - turation water suppression with routine spectrometry of GTM matetrial drug was made to evaluate and analyse the GTM injections produced by 7 different factories.

用核磁共振谱(~1H-NMR)对庆大霉素的主要组分C_1和C_2的百分含量进行了测定，用预饱和抑制水峰谱与GTM原料药的常规谱进行了比较，并对7个厂家的GTM注射液进行了测定分析。

The method is a useful tool by applying it to the resolution of model and real chromatographic signals.

通过对模拟色谱和实验色谱的比较，验证了该方法是一个很有用的工具，可以为色谱分析工作提供有力的帮助。

If carefully and properly used excellent chromatographic results and long column lifetime can be achieved.

如果小心和恰当的使用色谱柱，将得到好的色谱分析结果和延长色谱柱的使用寿命。

In order to clarify the rules of POD isoenzyme in the hazelnut, identify their blood relations between female, male and filial generations and select the superior parents for cross-breeding, we have studied the characteristics of peroxidase isoenzyme which are distributed in the 34 hazelnut varieties or lines by polyarclamide gel electrophoresis, The results showed that:POD isoenzymes of Corylus heterophylla Fisch, Corylus avellana L, and the hybrid of Corylus heterophylla Fisch × Corylus avellana L had obvious difference; some hybrids had lost P10 spectrum band of parents; the enzyme spectrum of 32 hybrid hazelnuts produced 'new hybrid spectrum bands'that could be considered as a mean to identify hybrids.

为了阐明过氧化物同工酶在榛品种中的分布规律，探讨平榛、欧榛及其杂种榛之间的亲缘关系，选育优势杂交亲本，本试验采用聚丙烯酰胺凝胶垂直电泳，研究了34个榛品种成熟叶过氧化物酶同工酶酶谱特征，结果表明：平榛、欧榛及其平欧杂种榛品种间酶谱具有较大差异；有的杂种品种遗失了父母本共有谱带P10；32个平欧杂种榛品种出现了双亲所不具有的新酶带，可作为鉴别杂种的一条途径。

Results When cellulase and pectinase compound,amlyse and diastatic enzyme were added in order in the method of stepwise biocatalysis,98% diosgenin from plants was extracted.IR spectrum of the product was in accordance with that of reference substance and the purity of it is more than 95% according to its HPLC chromatogram.

结果利用阶梯生物催化法，当纤维素酶和果胶酶复合酶制剂、淀粉酶以及糖化酶按顺序依次加入时，能够将植物中98%的薯蓣皂苷元提取出来，其产品的红外谱图与对照品谱图相吻合，经HPLC谱测定薯蓣皂苷元质量分数95%以上。

These data were used to infer the molecular formula and the elemental compositions of all the fragmental ions through software interpretation and, by further applying fragmentation regularities of mass spectrometry, the majority of ions were fully assigned. A base peak at m/z 402 in the mass spectrum was found as the molecular ion. The fragments were created mainly from the fragmentations of the tetrahydrofuran rings and the hydroxyl group. The most fragment products contain the dimethoxy phenyl group.

利用这些数据通过软件导出了分子式和所有碎片离子的元素组成，由此进一步根据质谱裂解规律对石梓醇分子的电子轰击质谱的主要裂解碎片给出了完全的归属，质谱中发现基峰为分子离子峰(m/z402)，裂解碎片主要来自双骈四氢呋喃环的裂解和羟基引起的裂解，绝大部分裂解产物包含二甲氧基苯基基团。

These genes are related to many plant functions, indicating that the heterosis was related with many metabolization pathways.1.2 The quantity of discrepant genes showed that the genetic discrepancy was notalways the same with the discrepancy of expressed genes, indicating that small-scale genetic discrepancy maybe result in large-scale genes discrepantly expression; in other way, some genetic discrepancies might not embodied on the discrepant genes in the experiment.1.3 Nine and eight discrepant genes were found respectively in the superior bulkand minor bulk in the dominant level.

1.2 各张芯片差异表达基因数量表明遗传差异与表达谱差异不尽一致，可能较小的遗传差异可以造成表达谱的巨大改变，而有些遗传变异可能没有在表达谱上表现出来。 1.3 从优势集团和负优势集团中分别找到9个和8个具显性表达水平的差异表达基因，研究表明显性表达水平的差异表达基因的聚合与杂种优势的表现没有相关性。

By time-varying filtering, we realize the signal selectivity and interference suppression, especially for the signals with time-varying power spectrum. It is shown herein that conventional eigenstructure based methods are lower dimensional special case of the time-frequency subspace fitting method. The closed-form array response estimation algorithms for blind source separation in wireless communication is also developed in the dissertation by exploiting the data structure of second-order statistics of the array output in the presence of multipath. The proposed method achieves array response estimation with little constraint on signal property and propagation environment such as scatters or angular spread. Moreover, the array utilized here can be of arbitrary geometry and even uncalibrated. Since the closed-form solution is obtained, no misconvergency may occur and large amount of computation can be saved. The equivalent feed model and corresponding optimization designation are proposed to realize the downlink multi-user selective transmission. By coherent and non-coherent superposition of the electromagnetical field, multiple beams can be formed using a single array, so that each co-channel user signal is transmitted in each beam and will not interfered with each other. The proposed system scheme implements the digital beamforming and the channel allocation in the base band, therefore is suitable for the utilization of the radio software technology. The feasibility and effectiveness of the proposed model are proved by the RF experiment.

在窄带条件下，GSC－SSF方法还可以提高阵列的虚拟孔径，从而提高估计的性能；可以证明，Cyclic DOA 和SC-SSF方法可看作该方法的特例或近似； 3、提出了二维GSC－SSF方法和宽带谱相关DOA矩阵方法，利用信号的循环平稳特性解决了宽带条件下二维 DOA 估计问题，并具有阵元数少、计算量较小的特点； 4、提出了时频子空间拟合和宽带时频DOA估计算法，将联合时频分析的理论和方法引入到阵列信号的空间谱估计研究中，利用时变滤波实现信号选择性测向和干扰抑制，特别适合于谱时变信号；可以证明传统特征结构法可看作是时频子空间拟合方法的特例； 5、提出了多用户环境下阵列响应的估计方法——CARE方法，该方法对信号结构和传播参数（主要是散射源分布与角度散布）的约束较少，适用于各种几何结构的阵列甚至未校准的阵列，能够直接得到阵列响应的闭式解，因此计算量小、稳健性好，不存在收敛问题； 6、提出了针对多用户下行选择性发送的阵列等效激励模型、优化设计方法及其系统实现方案，通过空间场的相干叠加与非相干叠加使得单一阵列能够形成多个波束，并保证各波束内的用户信号各不相同且相互干扰最小；其系统方案具有在基带实现数字波束成形、信道分配并便于软件无线电实现的特点，其有效性已得到外场实测数据的证实。

It has been put forward that there exists single Ball point and double Ball points on the symmetrical connecting-rod curves of equilateral mechanisms.

从鲍尔点的形成原理出发，分析对称连杆曲线上鲍尔点的产生条件，提出等边机构的对称连杆曲线上有单鲍尔点和双鲍尔点。

The factory affiliated to the Group primarily manufactures multiple-purpose pincers, baking kits, knives, scissors, kitchenware, gardening tools and beauty care kits as well as other hardware tools, the annual production value of which reaches US$ 30 million dollars.

集团所属工厂主要生产多用钳、烤具、刀具、剪刀、厨具、花园工具、美容套等五金产品，年生产总值3000万美元，产品价廉物美、选料上乘、质量保证，深受国内外客户的青睐