谱

METHODS The contents of synephrine,neohesperidin,hesperidin, naringin and narirutin in the raw materials and the extracts of Citrus aurantium were determined by reversed-phase high performance liquid chromatography with an Inertsil ODS-3(4.6 mm×250 mm,5 μm) column, respectively.

方法采用高效液相色谱法，以InertsilODS-3(4.6mm×250mm，5μm)色谱柱分别对枳实及其提取物中辛弗林生物碱类成分和新橙皮苷、橙皮苷、柚皮苷、芸香柚皮苷黄酮类成分进行测定。

Results:β-L-D4A was successfully synthesized and confirmed by IR, NMR and MS. Autoradiographic bands showed similar for supernatant and intracellular HBV DNA. Episomal HBV DNA was inhibited in a dose-dependent manner. EC50 of 3 -L-D4A was 0.2 μM. The experiment of cytotoxicity gained its IC_(50) 200 μM.

结果经一系列步骤合成的化合物β-L-D4A经红外光谱、质谱和核磁共振谱鉴定正确；2.2.15细胞培养上清液病毒DNA的Southern印迹、自显影结果显示药物对病毒的抑制呈明显的浓度依赖性，计算出EC_(50)为0.2μM；细胞毒性实验显示IC_(50)为200μM。

Aromatic constituents of 3 mature starfruit (Averrhoa carambola L.) cultivars, B17, B10 and Singapore Red, were analyzed using HS-SPME-GC-MS method.

采用顶空固相微萃取取法，用气相色谱－质谱联用技术分析了3个杨桃品种成熟果实的香气成分。

The method examines by national import and export merchandise occupation standard SN0352-95:" Exit shellfish is paralytic " of law of proved recipe of check of sexual shellfish toxin determines the; of content of toxin of paralytic sex shellfish of snail flesh and its content content applies fluid photograph color atlas, mass spectra couplet is used detect toxin of snail flesh balloonfish and its ramification.

方法按国家进出口商品检验行业标准SN0352-95：&出口贝类麻痹性贝类毒素检验方法&测定螺肉及其内容物的麻痹性贝类毒素含量；应用液相色谱—质谱联用检测螺肉河豚毒素及其衍生物。

Result 1991, area of Lian Yun harbor produced half plait to knit grain snail 2003 toxic 11, 2004 Ningxia Yinchuan the snail when a; is toxic 1, toxicity test of acute of small white rat all check gives toxin of paralytic sex shellfish; color atlas of afore-mentioned photograph of fluid of classics of shellfish check appearance, mass spectra couplet gives balloonfish toxin TTX and its ramification with analytic check.

结果1991—2003年连云港地区发生半褶织纹螺中毒11起，2004年宁夏银川1起；时螺中毒1起，小白鼠急性毒性试验均检出麻痹性贝类毒素；上述贝类检样经液相色谱—质谱联用分析检出河豚毒素TTX及其衍生物。

The BAW detector combined with ion exclusion chromatography is used to determine short-carbon-chain organic acids in beehoney and beverages. NA and NAD in foods is also determined by IC-BAW.

本文以离子排斥色谱分离结合BAW检测，对峰蜜和饮料中的低分子有机酸进行了测定；也用离子交换色谱-BAW测定了常用食品中烟酸、烟酸胺的含量，实现质量监控。

Baseline separation of eight kinds of LCFAs (dodecanoic acid, tetradecanoic acid, palmitic acid, oleic acid, stearic acid, eicosanic acid, erudcic acid, behenic acid) was achieved within 2 min with high resolution performance.

建立了利用短的微径色谱柱直接测定食用油中未衍生化长链脂肪酸的快速气相色谱方法。C12~C22脂肪酸在2 min之内实现基线分离，定量标准曲线的相关系数大于0.988，最低检测限（S/N=3）为2.80~9.60 mg/L，回收率为

We firstly introduced benzoazole (including benzimidazole, benzoxazole and benzothiazole) into the meso-positions of porphines and obtained five new porphyrins 36a-e. Their structures were characterized by 1H NMR, MS, UV-vis spectra and fluorescence emission spectra.

将苯并唑类基团(苯并咪唑、苯并噁唑和苯并噻唑)引入到卟吩中位，得到5个新型卟啉36a-e衍生物，并经核磁氢谱、质谱、紫外吸收光谱和荧光发射光谱表征了化合物的结构。

A series of 2-acetylformanilides were prepared,followed by thiolation with Lowesson reagent to afford 2-acetylthioformanilides,which further reacted with Mn3·2H2O in glacial acetic acid under microwave irradiation to afford 2-acetyl benzothiazole s.

合成了一系列的硫代酰胺，研究了它们在微波辐射醋酸锰作用下发生氧化自由基环化反应，成功地合成了一系列2-乙酰基苯并噻唑衍生物，其结构经红外光谱、核磁共振谱和质谱得到了证实

This paper studies that TLC technology is applied to synthesis of benzylidene acetone .

将薄层色谱技术应用于苄叉丙酮的合成实验，通过薄层色谱对合成反应过程的监控，增加了实验的探究性，提高了学生分析问题、解决问题的能力

With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务，乐队在现实中树立了重要的影响。

But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.

不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐，因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。