角度测定法

A method for the determination of high-content of copper in copper materials by flame atomic absorption spectrophotometry using sub-sensitive spectral line at 249.20 nm is reported in this paper.

中文摘要：利用铜的原子吸收光谱次灵敏线249.20 nm，并适当偏转燃烧器角度，原子吸收分光光度法测定含铜物料中的高含量铜。

Aiming at the target through X12 sight of TV goniometry, the firer presses the firing trigger and keeps the cross hairs of the sight on the target.

通过电视角度测定法的X12瞄准具对准目标，发射者按发射板机和保持瞄准具的交叉瞄准线在目标上。

In the process of J determination by J-R curve method, the result measured using this equation can get a very good agreement with that measured by low blow test.

在J-R阻力曲线法测定材料的J时，用该方程可得到与小角度冲击方法相一致的测试结果。

In this dissertation, firstly, the conditions of isolation and purification of specific toxin fractions produced by Exserohilum turcicum has been studied, and a high-efficient method has been established;secondly, the toxins were analysed by UV-Vis spectrophotometry;then the effect of specific toxin on death rate of corn leaves protoplast was studied by FDA as a tinct reagent;finally, using ANS as a probe and SDS-PAGE to study the membrane protein of the corn leaves with Htl gene. In a word, the aim of the research is to search some existent evidences of the toxin binding site on protoplasmic membrane, and provide proofs for nosogenesis of specific toxin in terms of cytology and the molecular biology.

本研究对玉米大斑病菌1号小种毒素的特异性组分进行分离，建立了高效的特异性毒素分离纯化方法，并对其进行了紫外波谱分析；用荧光素双醋酸酯染色法，测定了毒素特异性组分对原生质体死亡率的影响；进而用1-苯胺基-8-萘磺酸荧光探针标记法和SDS-PAGE电泳法对特异性毒素组分与Htl基因玉米细胞互作过程中的质膜蛋白进行了研究，旨在证明Htl基因玉米细胞质膜上存在特异性毒素组分结合蛋白，为从细胞和分子生物学角度阐明毒素的致病机理提供证据。

In this paper, total logistics amounts are chosen as evaluation index, and artificial time series are designed to solve the shortness of statistical data in Chinese logistics. Spectrum estimation theory depicts time characteristics in frequency domain thus has such benefit than time domain methods. This paper evaluates the period of Chinese logistics using spectrum estimation. Stationarity of artificial series is verified, parameter sensitivity of truncation point is analyzed, six periods with different delay window are compared, and significance of period evaluated is tested.

中国物流统计数据缺乏，客观上限制了对其周期规律的研究，本文选取社会物流总额作为测度指标，设计了一种人工序列，解决了统计数据过短问题；谱估计法从频域角度揭示客观事物的时间特性，在研究时间序列周期波动方面具有时域分析法所不具备的优势，作者采用谱估计法对中国物流发展周期进行测定，检验了指标序列平稳性，分析了截断点参数灵敏度，比较了6种不同滞后窗下周期值，并检验了所测得周期的显著性。

Starting from the solubility of disperse dyes, the solubility, up-taking rate, migrating rate of dis_perse Yellow M-4G, Red 3B and Blue 2BLN at different concentration of Leveling Agent GS were tested by poly_mer thin-film bag method, thus demonstrating the hyperchromic effect and achromic effect of leveling agent during dyeing with disperse dyes.

从分散染料溶解度的角度出发，采用聚合物薄膜袋法测定了分散黄M－ 4G、分散红3B、分散蓝2BLN 三种分散染料在匀染剂GS 不同浓度时的溶解度以及上染率、移染率，从而展示了匀染剂在分散染料染色中的&增色效应&和&消色效应&，并从染色理论上推论了产生这两种效应的原理。

The dopamine release in vivo was monitored by fast cyclic voltammetry and the concentrations of DA and its metabolites dihydroxy-phenylacetic acid and homovanillic acid were determined by high performance liquid chromatography electrochemical detection in the process study. In addition, the effects of some traditional Chinese herbs and related marine drug on behavioral changes were also evaluated in order to provide some suggestive clue for rational drug design of anti-Parkinon's disease .

许多因素都参与PD的DA能神经元的死亡，所以，本研究在制备PD动物模型的基础上，应用国内率先引进的快速周期伏安法检测设备在体动态监测DA的释放，同时应用另一种电化学检测技术—高效液相色谱电化学检测法离体检测DA及其代谢产物二羟苯乙酸和高香草酸的含量，结合行为学测定及其它方法，研究了雌激素和铁在PD发病中的作用，以及一些药物，如吲哚醌、牛磺酸、铁离子螯合剂、胆囊收缩素（CCK-8）、乌鸡白凤丸有效成份、大豆异黄酮及海洋酸性寡糖HSH971，对DA能神经元的影响，从DA能神经递质角度对PD的发病机理提供进一步的实验依据，并为PD的预防和治疗提供新的干预措施。

In this thesis, the phase diagram of Zn-Al binary system on 10~69.5 w% was reinvestigated by using differential scanning calorimeter, X-ray diffraction and pushrod dilatometer. The process of isothermal transformation during the aging of high-Aluminum-Zinc-based alloy was studied by using differential scanning calorimetry, and the aging behavior of the alloy was analyzed at the aspect of thermal analysis kinetics. The change of microstructure which the alloy was being heated was observed on high-temperature metallurgical microscope. The microstructure and wear-friction properties were compared among the alloys treated with several different heat treatment processes, and a model for heat treatment processes was proposed based on artificial neural network,so as to predict the relationship between friction coefficient and parameters of aging treatment such as aging temperature and time.

本文采用高温X射线衍射、示差扫描量热分析、热膨胀等方法重新测定含锌量范围为10％～69.5％的Zn-Al系二元相图，利用示差扫描量热分析法，研究高铝锌基合金时效等温转变过程，并从热分析动力学的角度分析高铝锌基合金合金时效行为；使用高温金相显微镜观察合金加热时的组织变化；比较几种不同热处理工艺对高铝锌基合金显微组织与耐磨性能的影响并利用人工神经网络建立高铝锌基合金热处理工艺模型，预测合金摩擦系数随时效温度及时间变化规律。

The absorption and distribution of chromium were studied in ryeusing nutrient culture technique and pot experiment.

采用不同浓度K2CrO4(0，0.4，0.8和1.2 mmol/L)的Hoagland营养液处理黑麦幼苗，测定铬在黑麦体内的亚细胞分布、铬化学形态及不同部位的积累。

By analyzing theory foundation of mathematical morphology in the digital image processing, researching morphology arithmetic of the binary Image, discussing two basic forms for the least structure element: dilation and erosion.

通过分析数学形态学在图像中的理论基础，研究二值图像的形态分析算法，探讨最小结构元素的两种基本形态：膨胀和腐蚀；分析了数学形态学复杂算法的基本原理，把数学形态学的部分并行处理理念引入到家实际应用中。