角峰

X-ray diffraction is one of the most common and efficient ways to measure a superlattice structure. This dissertation displays the detail results for characterization of Ge〓Si〓/Si superlattices by x-ray diffraction (including x-ray small angle diffraction and double crystal diffraction). It was found, when the growth temperature is lower, the intensities of xray small angle diffraction peaks are modulated by a periodical function, which indicates that both sets of interfaces of the superlattice is highly flat; when the growth temperature is higher, the diffraction peak intensities are simply decay with the increase of diffraction vector, which indicates that one set of interfaces is highly flat but another is not; when the growth temperature is very high, the diffraction peaks are reduced more rapidly, which indicates that both sets of interfaces are not ideal.

本文详细介绍了用X-射线衍射（包括X-射线小角衍射和双晶衍射）方法对Ge〓Si〓/Si超晶格结构特性测试的结果，尤其是发现，当Ge〓Si〓/Si超晶格的生长温度较低时，X-射线小角衍射谱峰的强度随着衍射波矢的增加而周期性调制，表明超晶格的两套界面都十分平整；当生长温度较高时，Ge〓Si〓Si超晶格的X-射线小角衍射谱峰的强度随着衍射波矢呈简单的衰减变化，对应于超晶格内有一套界面不平整的情况；当生长温度进一步提高时，X-射线小角衍射峰明显减少，表明超晶格内两套界面都不理想。

The effect of tribology factors on bearing vibration is studied experimentally. AR model and WPT are used to processing the normal arid abnormal signals. The results are as follows:1. The vibration of ball bearings is caused by the tribology action of contact pairs of ball and ring races and has the essential of tribo-dynamics. Any factors affecting the tribology characteristics of contact pairs will affect vibration and noise of bearings consequently.2. Vibration characteristics of bearing keep almostly unchanged with the increasing of axial load expecting the increasing of nature frequencies. When radial load increasing with axial load unchanged, nature frequencies keep unchanged but some new vibration peaks appears in the spectrum.3. Vibration amplitudes are damped and nature frequency are enhanced with sufficient lubrication. Vibration and noise of bearings increase obviously and roar can happen and the contact surfaces scratch slightly under insufficient and unclean lubrication state. Bearing will be disabled in a few minutes without any lubrication.4. Bearing vibration is unstable under low speed. With the speed increasing, the vibration become stable and natural frequencies increase slightly but the amplitudes increase apparently.5. Bearing vibration can be excited only by some harmonics ofwaviness without lubrication and by all harmonics with lubrication based on the theoretical analysis.6. The nature frequencies of ball bearings decrease with the increasing sizes. When international clearance increasing, nature frequencies decrease in radial and increase in axial and angular and the amplitudes increase in radial and decrease in axial and angular. When the number of balls increasing, nature frequencies increase and amplitudes decrease. When the pitch diameter increasing, axial nature frequency increase and others nearly keep no change. When outer race groove curvature radius increasing, nature frequencies increase in radial and decrease in axial and angular and amplitudes keep no change in radial and increase in axial and angular. When inner race groove curvature radius increasing, nature frequencies decrease and amplitudes increase.7. The distortion in amplitude and frequency components of bearing vibration signals picked up by the present probe measurement method is founded and right conclusions cannot be achieved by the signals. When accelerometer is rigidly screwed with steel stud onto a flat outer surface of a ball bearing, vibration signal can be got without distortion and the reliability of research on bearing vibration is assured.8. AR model is suitable for large samples of bearing vibration signals, square root of length of samples can be used as the upper limitation of order determination and the FPE order selection criterion is effective. Many advantages of AR spectrum are founded over the classical based on FFT.9. Time-Frequency analysis is necessary for abnormal noise of ball bearings. WPT overcomes the principle shortcomings of STFT and proved to be a best tool to process the abnormal signals.

理论分析和试验研究表明： 1球轴承振动是钢球—滚道接触副中的各种摩擦学作用引起的，具有摩擦动力学的本质，任何对接触副的摩擦学特性有影响的因素都将对球轴承的振动和噪声特性产生影响； 2中心轴向载荷作用下，载荷增大使球轴承的固有振动频率升高，载荷越大同样的载荷增幅引起的频率升幅减小，足够大的中心轴向载荷作用下载荷的变化对球轴承振动的频率特性不会产生明显的影响； 3轴向和径向联合载荷作用下，径向载荷不大时球轴承振动的固有频率基本不变，但是可能引起变刚度激励的非线性振动，出现新的频峰，过大的径向载荷将使部分钢球脱离接触，使球轴承的振动和噪声呈现不稳定状态； 4润滑对球轴承的振动和噪声特性有重要的影响，良好的润滑对振动有明显的抑制作用，润滑不充分时，振动和噪声的水平会有明显增高，一定条件下还会激发接触副中的谐振，发出啸声，造成接触表面的伤害，无润滑干接触时，短时的运转就会损伤接触副表面，使振动和噪声迅速增大，并随时可能引发严重的磨损和卡滞失效；接触副润滑良好时，油膜的"刚化效应"使球轴承振动的固有频率有所提高，润滑剂中含有弥散性污浊时，振动的幅度总体升高，但弥散性污浊不会改变球轴承振动的频率特性；浙江大学博士学位论文：球轴承振动的研究 5低速时，球轴承振动的基本特征呈现不稳定状态，随着转速的提高，球轴承振动的频率特性趋于稳定，固有频率频峰升高； 6理论分析表明，干接触时钢球和滚道表面波纹度的某些谐波分量能激励球轴承的振动，振动的幅值与谐波幅值成正比，实际球轴承中钢球的分布不可能完全均匀，波纹度的激励作用会随时发生；润滑接触的分析表明，波纹度的任意谐波分量均能激励球轴承的振动； 7球轴承的几何和结构参数分析表明，球轴承尺寸越大，径向、轴向和角振动的固有频率越低；钢球中心圆直径增大，球轴承的径向和轴向振动的固有频率基本不变，角振动的固有频率有所上升，振动的幅频特性基本不变；径向游隙加大使球轴承的径向振动固有频率降低，轴向和角振动的固有频率有所升高，径向振动幅频特性的幅值升高，而轴向和角向降低；钢球的数量增多使球轴承振动的固有频率上升，幅频特性的幅值下降，径向振动的幅值下降最为明显；外圈沟曲率半径系数增大使球轴承径向振动的固有频率升高，轴向和角振动的固有频率降低，径向幅频特性基本不变，轴向和角向幅频特性幅值升高；内圈沟曲率半径系数增大使径向、轴向和角振动固有频率均下降，振动幅频特性的幅值均有升高； 8试验对比表明，传感器采用探针式安装时，由于探针接触副接触特性的影响，钡(量得到的球轴承振动信号有失真，采用专门设计和制作的试验球轴承，以固定式安装加速度计，首次测量得到了球轴承振动的真实信号，通过对振动信号的分析，验证了球轴承振动的理论模型； 9)基于时间序列分析的AR模型适用于大样本球轴承振动信号的分析，以样本长度的均方根值作定阶上界，FPE做判阶准则，给出的AR谱光滑，频率分辨率高，是球轴承振动分析的简便而可靠的手段； 10以时频域分析的小波包变换分析球轴承异音信号能够比较好地定位和聚焦异音发生的时间，时间间隔，频率范围，同样是球轴承振动分析的可靠的手段，可用作球轴承故障诊断技术。

The refractive index of metal effects mainly resonance depth and the half peak breadth. There is an optimum metal thickness with the largest resonance depth and the smallest reflection coefficient. The refractive index and thickness of dielectric layer and recording layer impact resonance angle and the half peak breadth.

金属薄膜的折射率是影响共振半峰宽度和共振深度的主要因素，计算表明存在一个最佳的金属层厚度，使得共振深度最大，反射系数最小；介质层和记录层的折射率和厚度的变化均会影响共振角的大小和共振峰半峰宽的变化。

In this dissertation, we optimized the thinkness of each layer of TFEL devices using the layered optimization method to obtain ZnS: Ce〓 TFEL devices. Accoding to the energy level structure of Ce〓, two criteria for distinguishing the EL of Ce〓 were found out, from which it was conduded that the TFEL of ZnS: Ce〓 comes from 5d→4f transition of Ce〓. The measurement of brightness waveform showed that the TFEL of ZnS: Ce〓 was the luminescence from independent centers. and there were the field induced-delocalization in this process anf it〓s the cause of low TFEL efficiency of ZnS: Ce〓. In this dissertation, different influence factors on TFEL of ZnS: Ce〓 were sdudied. The influence of different host lattice is different: The blue/green ratio of ZnS: Ce〓 in hexagonal system of ZnS is larger than that in cubic system of ZnS, and the TFEL peaks in hexagonal system of ZnS moves toward longer wavelength compared with that in cubic system of ZnS. The adding buffer layer was used in this stage. The solubility of Ce〓 in ZnS was small and it was another limit to TFEL brightness of ZnS: Ce〓 device. The solubility of Ce〓 increased ten times when using Li ions as flux, so that the TFEL brightness of ZnS: Ce〓 was enhanced. It was found that the appearing of ZnO in active layer improves the TFEL of ZnS: Ce〓: the brightness and the wave range of ZnS: Ce〓TFEL were enhanced.

本文采用TFEL的分层优化方案，优化组合了各膜层厚度，选择最佳制备条件，得到了ZnS：Ce〓的TFEL；根据Ce〓的能级结构，找到了判别Ce〓的EL的两个简单依据，并据此断定ZnS：Ce〓的TFEL的两个发射峰分别属于Ce〓的〓和〓跃迁；亮度波形测量表明ZnS：Ce〓的TFEL属于分立中心发光，分析认为在此过程中存在着较严重的场致离化，这也是ZnS：Ce〓的TFEL效率较低的一个原因；本文考查了影响ZnS：Ce〓的TFEL的各种因素，发现：基质的晶体结构对ZnS：Ce〓的TFEL有所影响，在六角相ZnS中Ce〓的TFEL优于立方相ZnS中Ce〓的TFEL：发射峰的蓝-绿比相对较大，且光谱向短波方向移动，在此项研究中本文采用了在发光层前增镀过渡层的办法，过渡层为六角晶相的ZnO；限制ZnS：Ce〓的TFEL器件亮度的一个原因是Ce〓在ZnS中的溶解度低，本文用Li离子作助溶剂增大了Ce〓的溶解度，增大幅度为一个量级，并且ZnS：Ce〓的TFEL亮度明显提高；从ZnS：Ce〓的TFEL光谱来看ZnS：Ce〓的TFEL波长覆盖范围较小，亮度也不高，达不到做为白色TFEL材料的要求，需要寻找新的白色TFEL材料；在研究ZnS：Ce〓的TFEL中还发现：发光层中ZnO的出现有利于ZnS：Ce〓的TFEL：发射峰变宽、亮度增大。

According to the H NMRstudy, it was found that the protons on the cyclopentadienyl ring of 〓 were not splitted, but when one proton on the cyclopentadienylring was substituted by methyl, that is in〓 complexes, thefour protons on the ring were splitted into four groups,the 〓 between the onesignal and the others is large, the total splitting is over 2ppm. The splittings werealso affected by the halides linked with the titanium, they increase according to theorder of CI, Br, I. By the study of the 〓 Sn NMR, it is found that the chemicalshifts of 〓 are present in low field. It is assume that the large space strain causesthe angles of the tin linked with ligands deviate from the normal tetrahedral anglesresults low field shift for 〓Sn. And by MS study,there were no molecular ions for 〓 complexes in the spectra. However, for 〓 when X=CI,Br,NCO and Ar is tolyl or phenyl group,there were molecular ions,but theirabundances were very small,and no that for the iodide was found.

钛上的卤素对茂环氢的裂分也有影响，依〓，Br，I顺序，卤素对茂环氢的裂分依次加大；通过对〓的研究发现，以上这些化合物〓的化学位移都出现在低场，认为大的空间张力造成的锡的键角偏离正常的锡的四面体键角是造成〓化学位移出现在低场的原因；对这些化合物质谱的研究发现，〓系列化合物得不到分子离子峰，而〓系列的化合物，当X=〓，NCO和苯环上不带取代基或只带甲基时，则出现分子离子峰，但丰度很低，而相应的碘化物和其它化合物则没出现分子离子峰。

The glacial heritages of this period interspersed most wildly, such as glacial valleys, cirques, horns, knife-edge crest, morainic boulder, end moraine bars, lateral moraine bars, morainic platforms, morainic hills, morainic lakes and glacial lakes, they are the most magnificent glacial landform heritages in the geopark.

该次冰期遗迹在区内分布最广，冰蚀槽谷、冰斗、角峰、刃脊、冰碛漂砾，终碛垅，侧碛垅，冰碛平台，冰碛丘陵，冰碛湖，冰川湖遍布，构成区内最壮观的冰川地貌遗迹。

Jungfraujoch is the most glaciated part of the Alps, containing Europe's largest glacier and a range of classic glacial features such as U-shaped valleys, cirques, horn peaks and moraines.

少女山冈是阿尔卑斯山冰蚀现象最显著的部分，有欧洲最大的冰川和一系列典型冰川地貌，如 U 形峡谷、冰斗、角峰及冰碛。

Jungfraujoch is the most glaciated part of the Alps, containing Europe's largest glacier and a range of classic glacial features such as U-shaped valleys, cirques, horn peaks and moraines.

少女山岗是阿尔卑斯山冰蚀现象最显著的部分，有欧洲最大的冰川和一系列典型冰川地貌，如U型峡谷、冰斗、角峰及冰碛。

Jungfraujoch is the most glaciated part of the Alps, containing Europes largest glacier and a range of classic glacial features such as U-shaped valleys, cirques, horn peaks and moraines.

少女山岗是阿尔卑斯山冰蚀现象最显著的部分，有欧洲最大的冰川和一系列典型冰川地貌，如U型峡谷、冰斗、角峰及冰碛。

Glacial geology role not only shaped a lot of strange glacial terrain, such as glacial valleys, cirques, horn peaks, edge ridges, hanging valleys, sheep, stone back .

冰川的地质作用不仅塑造了许多奇特的冰蚀地形，如冰川槽谷、冰斗、角峰、刃脊、悬谷、羊背石等。

In the negative and interrogative forms, of course, this is identical to the non-emphatic forms.

。但是，在否定句或疑问句里，这种带有"do"的方法表达的效果却没有什么强调的意思。

Go down on one's knees;kneel down

屈膝跪下。。。下跪祈祷