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It is introduced briefly the modification way and result of lignosulphonate as coal-water slurry additive and determination of the adsorption film thicknesses of the LS and modified lignosulphonate on the smooth surface of coal and microscopic slide by the method of elliptical polarization .

简要介绍了木质素磺酸钠用作水煤浆添加剂的改性方法及结果,并采用椭圆偏振法测定了木钠及改性木钠在光滑的煤表面和载波片表面的吸附膜厚度,定量地对比了添加剂在固体表面吸附的空间位阻作用的大小。

The characteristic of machined surface of high speed machining aluminum alloy 7050-T7451 is researched by micrographic experiments and analysis. The formation mechanics of machined metamorphism layer has been analyzed and studied. The dislocation-energy model in machined metamorphism layer was established and applied to explain the micrographic mechanics work-hardening using the thermo-mechanical coupling deformation theory and dislocation theory. The experimental results show that the interaction of high dislocation density effect on hardening is more remarkable than that of thermal stress in high speed machining.

利用显微观察方法对铝合金7050-T7451高速铣削加工的工件表面断面和不同深度的表层的微观形貌特征进行系统的研究,确定了高速切削加工铝合金7050-T7451的表面变质层深度为30~35μm;应用位错能量研究了高速铣削加工过程的热力耦合对变质层的影响机理,并通过微观形貌观察证明:与普通切削相比,高速铣削表层塑性变形的能量和位错密度更高;建立了位错密度的加工硬化的动力学模型,研究了加工硬化的热-力耦合形成机理;对微观裂纹的形成机理进行了理论分析,证明位错密度高的高速切削过程中较低速加工更容易产生明显的微裂纹,从分子级乃至原子级的水平进一步揭示高速切削加工表面变质层的形成特征。

Results D Cell morphology : Osteoblasts adhered tightly to five different titanium surface; On G surface, osteoblasts were spindle-shaped along the groove; Osteoblasts were cubic, multangular and abundant cytoplasm on SB surface and TPS surface, spreading in all directions.

①细胞粘附形态:成骨细胞在五种不同处理钛片表面粘附生长,SB组、TPS组表面细胞为多边形,胞浆丰富,有多个伪足突起呈分化表型;G组表面细胞胞体沿打磨沟嵴的方向伸展呈长梭形,少见伪足突起。

The stability of GA-PBCA-NP was also studied.ResultsDue to the agglomerationg of nanoparticles with no stabilizer,it was difficult to preparate.GA-PBCA-NP produced by the two methods both had spheric and smooth outer appearance,uniform distribution,nonadherence and stability.The diameter,ebeding ratio and drug loading in GA-PBCA-NP produced by emulsification polymerization and interfacial polymerization methods were 90~600 nm and 200 nm,60.49% and 73.87%,18.15% and 22.23%,respectively.

结果未添加稳定剂的纳米球表面粘连团聚现象严重,难以成球;乳化聚合法制备的GA-PBCA-NP在透射电镜下观察表面圆整光滑,粒子之间不团聚,不黏连,粒径范围在90~600 nm,包封率为60.49%,载药量为18.15%;界面缩聚法制得的纳米粒表面圆整光滑,粒子之间不团聚,不黏连,粒径大小均匀,都在200 nm左右,包封率为73.87%,载药量为22.23%,两种方法制备的稳定性都较好。

GA-PBCA-NP produced by the two methods both had spheric and smooth outer appearance,uniform distribution,nonadherence and stability.The diameter,ebeding ratio and drug loading in GA-PBCA-NP produced by emulsification polymerization and interfacial polymerization methods were 90~600 nm and 200 nm,60.49% and 73.87%,18.15% and 22.23%,respectively.ConclusionIt is important to add dextran 70 in preparation.

结果未添加稳定剂的纳米球表面粘连团聚现象严重,难以成球;乳化聚合法制备的GA-PBCA-NP在透射电镜下观察表面圆整光滑,粒子之间不团聚,不黏连,粒径范围在90~600 nm,包封率为60.49%,载药量为18.15%;界面缩聚法制得的纳米粒表面圆整光滑,粒子之间不团聚,不黏连,粒径大小均匀,都在200 nm左右,包封率为73.87%,载药量为22.23%,两种方法制备的稳定性都较好。

The nanoplex were smaller than the unmodified nHAP; thelipiodol/nanoplex emulsion, with the mean diameter at 75±11.8nm can disperse moreuniformly and be more soluble and stable, contrary to the unmodified nHAP and nanoplex Conclusion: Nanoplex/pDNA mass ratios greater than 15 had exhibited completepDNA absorption onto positive charged polyplex and pDNA protection from thedestruction of nucleinase in rabbit serum. Unmodified nHAP may can\'t induce effectivegene delivery.PartⅡThe construction of the recombint eukaryotic expressive vector ofwild-type human p53 and RbObjective: To construct the recombint eukaryotic expressive vector of wild-type humanp53 and Rb by utilizing the theory of molecular medicine.

结果nHAP颗粒本身大小小于100nm,但由于颗粒表面本身带负电,不能包括有效地结合及保护DNA;经Ca~(2+)修饰后,颗粒可带正电,可一定程度地结合和保护DNA,但聚合物本身的中性电与带负电的细胞膜结合,而且本身的颗粒则变地容易聚集而成为很大的颗粒,也不利于细胞的吞噬;经PLL修饰后,颗粒溶解性提高,直径变小,表面带正电,电泳结果显示PLL-nHAP颗粒可包括有效地结合和保护DNA免受兔血清的破坏,而且复合物表面的正电也包括有利于与细胞膜的结合与吞噬。

As our studies showed, silylation of mesoporous molecular sieves with alkoxysilane was an usual method of linking desired organical groups. However, as a result, the a lot of silanol groups still existed on the surface of mosoporous molecular sieves after silylation, which maybe affect the interface property and its catalystic activity. Based on this consideration, a novel method was proposed that a mixture of trichlorosilanes was used to silylate mesoporous molecular sieves, introducing both the further reactive group and hyhrophobic methyl group in one pot.

正如研究表明,通过硅氧烷与介孔分子筛表面的硅羟基反应是常见的键连有机基团的方法,但表面仍会剩余较多的硅羟基,硅羟基的存在会严重影响到介孔分子筛表面性质及催化活性,为此笔者提出采用混合的三氯化硅烷一步硅烷化介孔分子筛,在孔道内同时引入可进一步功能化的氯丙基或氯苄基和疏水性的甲基。

The results show that air plasma causes surface wettability improvement, surface roughness, surface oxidization and nitration.

结果表明:处理后表面润湿性改善,表面微结构形貌粗糙化,表面发生氧化和氮化。

The adsorption of polyoxyethylene alkyl ether surfactants (Brij 30 and Brij 35) on synthetic smectite clay nanoparticles and the interactions between them have been investigated through surface tension, zeta potential and rheology properties measurements, showing that Brij 30 and Brij 35 are adsorbed onto Laponite surface, and the adsorption is increased with decreasing oxyethyl groups.

通过表面张力、Zeta电位和流变学参数的测定,研究了聚氧乙烯烷基醚类非离子型表面活性剂(Brij 30和Brij 35)在合成锂皂石纳米颗粒表面的吸附及对Laponite水分散体系中颗粒间相互作用和体系粘度的影响。结果表明,这类表面活性剂能显著地吸附在Laponite颗粒表面上,且吸附量随其分子中POE链长短而不同。

By means of contrasted immobilization of denitrifying bacterium on several kinds of carbon fibers, the effect of physical and chemical characteristics such as specific surface area, precursor and recycle, especially the surface oxygenic functional group on these carbon fibers was investigated.

通过对比反硝化菌在不同基体碳纤维表面的固着化及碳纤维表面含氧官能团对菌种的固着化实验,研究了碳纤维(基体、比表面积、循环利用性等)特性,尤其表面含氧官能团对反硝化菌固着化的影响。

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