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It is demonstrated that the chiral quaternary ammonium salts catalysts exhibit promising catalytic properties for the substrate. Part III: The synthesis and the characterizing of the macroporous aminomethyl resin-supported cinchona alkaloid complexes and the study on its catalytic properties The part consists of two subsections. the macroporous aminomethyl resin -supported cinchona alkaloid complexes were synthesized by the stuff (cinchonine, quinine and macroporous aminomethyl resin). Their structures were characterized by means of elemental analysis, XPS, TG/DTA; the chiral polymer-supported complexes were first used as catalysts for the reduction of ketones. Their catalytic properties for the reduction processes were investigated. The comparison of the products e.e., the conversion of the substrate among different reduction processes was employed with determined by HPLC. The effects of the time, the temperature, the ratio of catalyst to substrate, reaction solvent as well as the recycle times were also discussed.

第三章聚-4-氨甲基苯乙烯负载金鸡纳碱金属络合物的合成与表征及其不对称催化性能研究本章分为两节,以辛可宁和奎宁及聚-4-氨甲基苯乙烯为原料,合成了4种聚-4-氨甲基苯乙烯负载金鸡纳碱络合物催化剂,并对它们的结构用元素分析、X-射线光电子能谱、TG/DTA等几种测试手段进行了表征;首次将所合成的手性高分子负载的金属络合物用于催化芳香酮不对称还原反应,详细研究了所得的手性高分子负载的金属络合物对不同底物的催化性能,用HPLC等分析手段定量检测了还原过程的底物转化率及其产物对映异构体选择性,并考察了反应时间、反应温度、催化剂和底物投料比、反应溶剂和循环次数对催化性能的影响。

Microscope and image analysis technique are adopted in 《JB/T 7990-1998》. The "grain size" tested by microscope is expressed by the "largest breadth" of the grain image. When the grain size is tested by image analysis instrument, the grain size is expressed by the diameter of a circle whose area equals the grain image's.

JB/T7990-1998》规定用图像分析仪或显微镜测量粒度,显微镜法测量的"粒度"是以颗粒投影的"最大宽度"来表征的,而用图像分析仪测量的"粒度"指的是"等面积圆直径",即,用与颗粒投影面积相等的圆的直径表征颗粒粒度。

In this paper, on the basis of predecessor research,β-diketone derivative ligand, Pyrazolyl ligand and their eight transition metal complexes were synthesized.

本论文是在前人研究的基础上选择合成并表征了一种β-二酮类配体和一种多吡唑类配体及其八个过渡金属配合物,并解析了它们的单晶结构,进行了元素分析、红外光谱、紫外光谱等表征,并研究了它们的发光性能和热稳定性能。

A combination of DLS and SLS was used to characterize the temperature dependence of the diameter and structure of the nanoparticles and the corresponding hollow spheres, and it was found that the temperature dependence is completely reversible.

用DLS跟踪了纳米粒子的核酶解过程中散射光强和粒径的变化,并用FTIR,SEM和TEM表征了酶解前后纳米粒子的结构和形貌的变化;结合采用DLS和SLS技术表征了纳米粒子和空心球的粒径及结构对温度的依赖性,发现PNIPAM空心球的温敏性变化是完全可逆的。

The morphology of the products we obtained show a new high-symmetry dodecahedral shape, a nano-chain structure also can be obtained.

通过一系列表征手段对产物进行了详细的表征,并讨论提出了影响产物形貌的因素和产物形成的机理。

The ethylate tantalum film is characterized by FT-IR spectra, XRD and SEM, and the TaC coating is characterized by XRD and SEM.

用红外光谱、XRD及SEM分析和表征醇基钽膜,用XRD和SEM分析和表征TaC涂层。

The catalysts for the combustion of ethyl acetat ewer eprepared using Fe,Co,Cu,Cr,and Mn metal oxides as active components supported on Al2O3-Ce0.5Zr0.5O2 mixed oxides and characterized by X-ray diffraction,temperature programmed reduction,oxygen storage capacity measurement,BET surface area,XPS measurement,and activity test.

制备了Fe,Co,Cu,Cr和Mn金属氧化物催化剂,所用载体为Al2O3-Ce0.5Zr0.5O2复合氧化物。利用X射线衍射,程序升温还原,储氧量测试,BET比表面测试和光电子能谱表征了催化剂。并利用活性测试表征了各种催化剂对乙酸乙酯催化燃烧能力。

Preparation and characterization of graft epoxy resin/silica hybrid aqueous dispersions and their films Epoxy resin/silica hybrid dispersion with solid content 30% was prepared by in-situ dispersing graft epoxy resin with silica sol and water.

接枝环氧树脂水分散液的制备及其表征通过BPO引发甲基丙烯酸和苯乙烯接枝高分子量环氧树脂的反应,合成了亲水性的环氧树脂,并利用索氏抽提的方法对产物进行了分离和表征

All this means to emphasize the imperativeness to improving the evaluation of marketing risk for our nations commercial bank.Then this paper set up an index system for three kinds of important marketing risk factors separately, given the corresponding weight to each kind of risk and to each index of each risk factor, thus got the score of every kind of risk and score of the comprehensive marketing risk, and analyzed this respectively.

论文首先通过各种方法识别了影响商业银行营销活动的所有营销风险,然后分别对三类重要的营销风险因素建立了能够表征它们的指标体系,对每类风险和表征每个风险因素的指标都赋予了相应的权重,从而得到了每一类风险的得分和综合营销风险的得分,并对此分别进行了分析。

The influence of high temperature and high pressure on foaming agent's properties in opened and closed system, and influence of the change of foaming agent's properties on foaming capacity and foam stabilizing capacity are also studied. The multiple regression theory is used to establish the quantitative characteristic functions of foaming agent versus temperature and pressure. Based on the Gibbs Principle, the quantitative characterization is carried out on relation of foam system's free energy versus its surface tension, surface area and concentration, and the analysis of energy concluded that the disintegration of the foam is inconvertible. At the same time, the influence of change of foam's shape and structure on distribution of reservoir temperature and pressure is qualitatively described, and the coupling mechanism between temperature field, pressure field and chemical field is systematically expounded.

同时,研究了不封闭体系、封闭体系下高温、高压对发泡剂性质的影响,以及发泡剂性质的改变对其发泡性能、稳泡性能的影响;采用泡沫实验的相关结果,运用多元回归理论,建立温度、压力与发泡剂浓度的定量表征函数;基于Gibbs原理,对高温、高压下泡沫体系的自由能与其表面张力、体系中液体的表面积以及浓度关系进行定量化的表征研究,从能量的角度得出了泡沫衰变过程具有不可逆性;同时定性地描述了泡沫形态、结构的变化对油藏温度和压力分布的影响,系统地阐述了温度场、压力场、化学场间的耦合作用机理。

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However, as the name(read-only memory)implies, CD disks cannot be written onorchanged in any way.

然而,正如其名字所指出的那样,CD盘不能写,也不能用任何方式改变其内容。

Galvanizes steel pallet is mainly export which suits standard packing of European Union, the North America. galvanizes steel pallet is suitable to heavy rack. Pallet surface can design plate type, corrugated and the gap form, satisfies the different requirements.

镀锌钢托盘多用于出口,替代木托盘,免薰蒸,符合欧盟、北美各国对出口货物包装材料的法令要求;喷涂钢托盘适用于重载上货架之用,托盘表面根据需要制作成平板状、波纹状及间隔形式,满足不同的使用要求。

A single payment file can be uploaded from an ERP system to effect all pan-China RMB payments and overseas payments in all currencies.

付款指令文件可从您的 ERP 系统上传到我们的电子银行系统来只是国内及对海外各种币种付款。