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Result shows that the sulfur compounds in the diesel can react with iodomethane easily at room temperature, the most of sulfur compound derived into methylsulfonium salts; the homologue of benzothiophene get the higher conversion ratio and react selectivity than the homologue of dibenzothiophene. It is found that primarily sterically hindered alkylated DBT, for example, 4-or 4-, 6-DBT, is recalcitrant to be methylated.

结果表明:柴油中硫化物在室温条件下容易与碘甲烷发生甲基化反应,大部分硫化物转化为锍盐,总转化率超过80%,苯并噻吩类比二苯并噻吩类更易发生甲基衍生化反应,转化率也相应较高。

So far this method has been successfully applied to HPLC analysis of simple monosaccharides. A baseline separation of five monosaccharides was obtained under optimized isocratic condition. Both UV detector and electrospray ionization-Mass spectrometry were selected to determine the monosaccharide composition in real samples.

结合建立的衍生化方法与高效液相色谱HPLC,优化分离条件,并选择紫外和电喷雾—离子阱质谱两种检测模式对实际样品中所含的单糖进行分离分析,建立了5种单糖的常规定性定量方法。

Objective: To determine the amino acid composition and isoelectric point of porcine platelet-derived growth factor.

摘要目的:测定猪血小板衍生生长因子的氨基酸组成和等电点。

Two coordination polymers composed of in situ synthesized ligand deriving from isophthalic acid through the hydroxylation on the 2-position have been synthesized under hydrothermal conditions.

利用铜离子的氧化还原性质,以铜离子和间苯二甲酸在水热条件下反应使配体发生羟基化衍生成2,6-二羧基苯酚,并组装出2个含衍生配体的配位聚合物。

Methods Isothiocyanic acid base phenyl ester pre-column derivatization was used for the determination of three kinds of amino acids contents in the glu-ala-glycine chewable lablet by high performance liquid chromatography,the chromatography condition was inertsil ODS-3V4.6×250mm,5μm

方法谷丙甘氨酸咀嚼片中3种氨基酸含量测定采用异硫氰酸基苯酯柱前衍生化高效液相色谱法。色谱条件:色谱柱为Inertsil ODS-3V4.6mm×250mm,5μm

A method combining HPLC, a post-column derivation device and a fluorescent detector was used to determine residues of ten carbamate pesticides (aldicarb sulfoxide, aldicarb sulfone, oxamyl, methomyl, 3-hydroxy carbofuran, aldicarb, propaxur, carbofuran, carbaryl and methiocarb) in 68 vegetable and 32 soil samples under four different cultivation systems (traditional kailyard, open field vegetable base, green house and paddy) were collected from a certain city in South Jiangsu.

本研究采用高效液相色谱-柱后衍生-荧光检测法分析了苏南某市4种不同种植方式下(传统菜地、露天蔬菜基地、大棚蔬菜基地和水稻田)68个蔬菜样品和32个土壤样品中10种N-甲基氨基甲酸酯类农药(涕灭威、涕灭威砜、涕灭威亚砜、杀线威、灭多威、残杀威、克百威、3-羟基克百威、甲萘威和灭虫威)的残留量,结果表明在蔬菜中检出的氨基甲酸酯农药残留水平多处于0.2~23μgkg^-1,土壤中为0.1~10μgkg^-1;土壤中3-羟基克百威和灭虫威全部检出,其最高检测浓度分别为10μgkg^-1和1.64μgkg^-1,其他农药仅有少数检出。

In this early era of the Expanded Universe, Kenner Toys even considered adding different colored stormtroopers into their assortment of action figures, but Lucasfilm ultimately decided to stick with what was in the movies.

在这衍生宇宙的早期阶段,肯纳玩具公司甚至考虑把不同颜色的冲锋队制作成各式各样的活动人偶,但卢卡斯影业最终决定坚持电影里出现的冲锋队形象。

A method of high performance liquid chromatography-fluorescence detection for the simultaneous determination of kynurenine and kynurenic acid in serum was developed.

建立了在线衍生、双波长高效液相色谱-荧光检测器同时检测血清中犬尿氨酸(kynurenine, Kyn)和犬尿喹啉酸(kynurenic acid, KYNA)含量的方法。

Among these three designs,"laddering" is then further designed into three other generations of "Hyper-Functional Bodies".

衍生折梯改写的三阶段「超」功能身体设计。

The synthesis of reactive ladderlike polysiloxane is one of the most challenging tasks, from which a series of novel functional ladderlike polysiloxane can be prepared.

而合成具有反应性的梯形聚硅氧烷更是一个重要的前沿课题,可以进一步衍生出一系列新型的梯形主链的功能高分子。

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This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。

There is no differences of cell proliferation vitality between labeled and unlabeled NSCs.

双标记神经干细胞的增殖、分化活力与未标记神经干细胞相比无改变。