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After derivatization with 9-fluolenylmeghyl chloroformate at 40℃ in alkalescent environment (pH=8.0), taurine in samples was separated and quantified by HPLC.

在硼酸盐缓冲溶液存在的弱碱性(pH=8.0)环境中样品中的牛磺酸与9-氯甲酸芴甲酯在40℃水浴中反应生成衍生化产物,用反相高效液相色谱法检测定量。

Methods Determination of DNJ by derivatization with 9-fluorenylmethyl chloroformate and followed by reversed-phase high-performance liquid chromatography and a fluorescence detector; the inhibitory curves on α-glucosidase at the enzymatic level and the activities to α-aglucosidase in vitro were observed in the everted sac experiment.

以氯甲酸药甲酯柱前衍生RP-HPLC荧光检测法对DNJ进行分析;在酶水平测定样品的α-糖苷酶抑制曲线,在离体水平用反转肠囊实验测定样品的α-糖苷酶抑制活性。

After acid hydrolysis of urine, primary amino acids were derivatized with ortho-phthaldialdehyde and removed from the sample by use of silica gel, followed by devivatized of hydroxyproline with 9-fluorenylmethyl chloroformate, and then injected into a C8 reversed-phase column.

采用邻苯二甲醛和芴甲基氯甲酸酯两个衍生剂,先后处理尿标本,以国产C8柱为固定相,在醋酸钠缓冲液中加入23%的乙腈作为洗脱液,3,4-脱氢脯氨酸作为内标。

I have tried to learn about the interacting energy between the emerging life and its motherch39rs body in my explorations of the "chora," and record the mental and perceptual process in my art.

2002年二月明白自己体内进驻了一个生命体后,对於这个神秘的空间衍生了一个与它共存的使命感,我试从「阴性空间」的探究中,认识小生命与母体的能量互动,并进而将知性与感性的过程纪录在创作里。

Objective To investigate the expression of pigment epitheliumderived factor and vascular endothelial growth factor in choroidal melanoma.

目的 观察脉络膜黑色素瘤中血管内皮生长因子和色素上皮衍生因子的表达,探讨两者在脉络膜黑色素瘤血管生成、肿瘤生长和浸润转移中的作用。

According to the determination of fatty acids, we established an HPLC method for the analysis of VPA in serum by RP-HPLC after transfered VPA into an ester which has chromophoric characteristics.

本文参照脂肪酸衍生化测定条件,建立了将丙戊酸转化为具有紫外吸收特征的酯,再经紫外检测的RP-HPLC测定方法。

The Victorian English people have endured multipuzzling of identities ofsex, class and culture. The striking of all these contradictories has made the apparently peacefulmanors be complected by multiple anxieties of identity. The metaphor manor/Eden brings anothermetaphor manor/Paradise Lost, as a ramification.

维多利亚时代的英国人经受着性别、阶级、文化身份的多重困扰,种种矛盾的撞击使得表面祥和的庄园交织着多重的身份焦虑,庄园/伊甸园衍生出庄园/失乐园的隐喻。

Retroreflector array is used as pseudo phase conjugator in the system. The fidelity of the conjugate wave and matching problem of the retroreflector array and Hartmann-Shack wavefront sensor is discussed. Several data fusion methods are presented in order to having two Hartmann-Shack wavefront sensors control one set of wavefront corrector. The misalignment errors of Hartmann-Shack wavefront sensor and arrangement errors of wavefront sensor and deformable mirror are analyzed. At the same time, numerical work based on the data of practically system, such as 61 element AO system, are done corresponding to the problem respectively and the results are given.The system of CP/CM AO is setup to fulfill all the functions.

针对不同的应用环境,提出了四种CP/CM衍生光路;进行了关键器件——角反射器阵列的保真度分析,给出了角反射器阵列作为伪相位共轭器件,与哈特曼—夏克波前传感器的匹配条件,认为角反射器阵列的布局要与哈特曼波前传感器的微透镜阵列布局完全对应,才能达到最优探测效果;提出了四种双哈特曼传感器控制一套波前校正器的数据融合方式,并逐一进行了分析,认为加修正因子斜率融合和电压融合方式在目前工程中是适用的,并进行了相应的数值模拟;给出了哈特曼传感器自身的调整误差分析过程,得到了误差可通过常规标定消除的判断依据;通过数值计算,得到了常规自适应光学系统和CP/CM系统哈特曼传感器和变形镜的对准误差对系统性能的影响,给出了两种系统对于不同对准误差情况下校正效果的变化情况和相应系统容限;以37单元自适应光学系统为基础,搭建了CP/CM自适应光学系统光路,并完成了系列CP/CM功能实现实验,运用双哈特曼传感器数据融合,成功实现了CP/CM自适应光学系统的闭环实验。

Retroreflector array is used as pseudo phase conjugator in the system. The fidelity of the conjugate wave and matching problem of the retroreflector array and Hartmann-Shack wavefront sensor is discussed. Several data fusion methods are presented in order to having two Hartmann-Shack wavefront sensors control one set of wavefront corrector. The misalignment errors of Hartmann-Shack wavefront sensor and arrangement errors of wavefront sensor and deformable mirror are analyzed. At the same time, numerical work based on the data of practically system, such as 61 element AO system, are done corresponding to the problem respectively and the results are given. The system of CP/CM AO is setup to fulfill all the functions. Through the data fusion of two Hartmann-Shack wavefront sensors, the system runs successfully and realizes the close loop. It lays a good foundation for the application of CP/CM AO. Another aspect of this paper is to expand the working band of Hartmann-Shack wavefront sensor through Frequency Transfer of Nonlinear Optics.

针对不同的应用环境,提出了四种CP/CM衍生光路;进行了关键器件——角反射器阵列的保真度分析,给出了角反射器阵列作为伪相位共轭器件,与哈特曼—夏克波前传感器的匹配条件,认为角反射器阵列的布局要与哈特曼波前传感器的微透镜阵列布局完全对应,才能达到最优探测效果;提出了四种双哈特曼传感器控制一套波前校正器的数据融合方式,并逐一进行了分析,认为加修正因子斜率融合和电压融合方式在目前工程中是适用的,并进行了相应的数值模拟;给出了哈特曼传感器自身的调整误差分析过程,得到了误差可通过常规标定消除的判断依据;通过数值计算,得到了常规自适应光学系统和CP/CM系统哈特曼传感器和变形镜的对准误差对系统性能的影响,给出了两种系统对于不同对准误差情况下校正效果的变化情况和相应系统容限;以37单元自适应光学系统为基础,搭建了CP/CM自适应光学系统光路,并完成了系列CP/CM功能实现实验,运用双哈特曼传感器数据融合,成功实现了CP/CM自适应光学系统的闭环实验。

This supported that Stemonaceae should be separated from Liliales and placed in Pandanales. Affinities and speciation of the species in Croomia The two Asian species of Croomia were more closely related to each other than either is to Northern American species.

Croomia的种间关系该属的3个种中,北美的C.pauciflora与两个亚洲种在分子树上已经分歧,根据单倍型和分子树该种与亚洲种的分离时间较早,很可能是从C.japonica的日本居群衍生形成或迁移到北美大陆的。

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