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The TiO2 particles were characterized by TEM, XRD and BET. The result shows the product is quasi spherical rutile titania nanoparticles with stable product quality. The nanotitania powders can be prepared with different sizes and even dispersion by controlling reaction conditions. This method is simple and may be employed to prepare rutile nanocrystals without heat treatment.

经透射电子显微镜、X-射线衍射和比表面分析,得到的样品为金红石型,其粒子近似呈球形,通过控制反应条件可以得到不同粒径的分散均匀的纳米二氧化钛粉体。

Porous alumina templates with different apertures were fabricated by changing the oxidation voltage in two-step anodic oxidation, and then Cu nanowires were synthesized in porous alumina by the alternating current electrochemical deposition method. The Cu/PAA was analyzed by SEM and XRD, the results have shown that Cu nanowires were indeed synthesized in porous alumina which had the same diameter and good structure of wire grating.

通过改变二次氧化过程中的氧化电压,制备了不同孔径的多孔Al模板;采用交流电沉积的方法,制备了含Cu阳极PAA膜。X射线衍射分析表明,阳极PAA膜上确有Cu生成;扫描电镜显示,Cu纳米线粗细均匀,具有很好的线栅结构。

The enthalpy change of the reaction of formation for the title complex in liquid-phase was determined by a microcalorimeter.

通过元素分析和单晶X射线衍射对生成的配合物进行了表征,采用微热量计测定了液相反应的焓变。

A thin film of titanium carbide is obtained by vacuum evaporating oftitanium. With diffusion treatment, the existance of titanium carbide is identified by X-raydiffraction analysis. Quantatitive analysis is made by XPS to invetigate diffusion ofcarbon atom between diamond and titanium film.

用真空蒸镀法在金刚石表面镀覆Ti层,并经扩散处理使金刚石表面形成TiC膜,实现了金刚石表面的金属化。X射线衍射分析证实了TiC的存在,利用XPS定量分析验证了在金刚石表面碳原子与钛镀层之间的反应扩散模型。

At certain temperature and hydrogen flow rate, the weight changing of tungsten trioxide during the reduction was investigated by thermo balance, and the phase transformation analyzed by means of XRD.

在一定的温度和氢气流量条件下,用热分析天平精确测量WO3 还原反应过程中,不同时间的质量变化,并用X射线衍射分析进行物相鉴定,绘制纳米级WO3 (粒径≤ 5 0nm)的还原动力学曲线。

Acording to the results for the analysis of component and structure of titanic iron ore with X-ray diffractometer and the fact in that titanic iron ore is prossessed of a dielectric property capable to absorb evidently microwave, a household microwave oven with power of 800W is applied to the decomposition of titanic iron ore sample under atmospheric pressure. It is shows that the sample with size of below 0.125nm can completely decomposed with phosphoric acid or mixture of phosphoric acid and sulfuric at about 160℃(corresponding to mid-low fire gear in microwave oven).

本实验根据X-射线衍射仪分析钛铁矿组成和结构的结果,利用钛铁矿显著吸收微波的介电特性,使用改装后的800W家用微波炉,在常压下选择中低火加热温度(160℃左右),分别用磷酸和磷硫混酸在微波辐照下消解粒度小于0.125mm的矿样,可快速将矿样消解完全。

Field emission scanning electron microscope, X-ray diffraction and poresizer indicate the nanotubes are formed due to the competition of tin monoxide formation and dissolution under the assistance of electric field. The formation mechanism of nanotubes agrees with the theoretic model of oxidation-dissolution.

经场发射扫描电镜、X射线衍射和孔径分析仪分析显示,阳极氧化的前聚体是氧化亚锡,通过在空气中加热转化为二氧化锡,在详细研究制备条件和氧化锡孔道形貌的基础上,提出了氧化锡纳米孔的生成机理符合氧化溶解理论模型。

Mesoporous tin oxide was synthesized by using cetyltrimethyl ammonium bromide or CTAB and Tween-20 as the template or hydrothermal process. Hollow tin dioxide micospheres were synthesized by using resorcinol-formaldehyde gel as the template or hydrothermal process. Thermogravimetric analysis, X-ray diffraction and electron microscopy have been used to characterize the materials.

本文分别采用十六烷基三甲基溴化铵模板法、CTAB和吐温20复合模板法及水热法来合成介孔氧化锡;用间苯二酚和甲醛凝胶模板法及水热法合成空心球氧化锡,并用热分析、X射线衍射、电镜等对以上材料作了形貌及结构表征。

Nano-SnO powders were prepared by sol-gel technique using tin dichloride, oxalic acid and dehydrated alcohol as raw materials, and characterized by thermogravimertric analysis and differential thermal analysis, X-ray diffraction, transmission electron microscope, scanning electron microscopy in combination with various electrochemical methods.

以氯化亚锡、草酸和无水乙醇为原料,采用溶胶-凝胶法制备了纳米SnO粉末,并用热重-差热分析、X-射线衍射分析、透射电镜和扫描电镜等多种电化学方法对其进行了表征。

The phase structure,hydrogen storage performance and electrochemical performance of the alloys were studied by XRD and three-electrode test system.

采用X射线衍射和三电极测试体系研究了合金的相结构、贮氢性能和电化学性能。

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However, as the name(read-only memory)implies, CD disks cannot be written onorchanged in any way.

然而,正如其名字所指出的那样,CD盘不能写,也不能用任何方式改变其内容。

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