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衍射线

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The tensile strength was tested by using the omnipotence testing machine and the fracture characteristics and phase were analyzed by scanning electron micros copy and X-ray diffraction.

摘 要:分析了钛与不锈钢相变扩散连接的工艺参数,利用万能拉伸试验机测试了接头拉伸强度,利用扫描电镜及X射线衍射分析了接头断口形貌及组成相。

In this work, nanostructure samples of La1-xCaxMnO3(x=0.2、0.3、0.4、0.5)were prepared by hydrothermal-precipitation method . The structural characterization of the powder samples were done by X-ray diffraction. XRD patterns showed that all the samples ate single perovskite-type phase withoutother impurity or secondary phase. The shape and size of samples were performed on Scanning Electron Microscopy. SEM photographs investigated that temperature of hydrothermal effects the phase of samples and alkalinity of the reaction mixture by ΔTad-T curve measurement device at low magnetic fielded

本论文采用水热共沉淀退火法制备了La1-xCaxMnO3(x=0.2、0.3、0.4、0.5)系纳米结构,用X射线衍射仪确定产物为单相钙钛矿结构,无任何杂峰及第二相;用扫描电子显微镜与透射电子显微镜分析了产物的大小和形貌,发现水热温度对产物的形成起决定作用,随着温度的升高,产物由薄膜状向丝状转变,而溶液的碱度可控制产物的形貌和大小,当碱度为6.35mol/L,水热温度为240 C时,La0.6Ca0.4MnO3的主要形貌为纳米丝并有少量纳米颗粒,纳米丝平均直径为40nm;最后测量了粉末样品在低磁场(1.4T)下的磁热效应,发现水热共沉淀退火法制备样品的最大绝热温度明显高于球磨法制备样品的最大绝热温变。

Their proper- ties have been investigated by means of IR spectrum, stability and molar conductance, thermogravimetric and differential thermal analysis and X-ray diffraction.

通过元素分析、摩尔电导、红外、差热-热重和X射线粉末衍射等分析该段研究了它们的有关性质,得到了一些新结果。

A total of fifteen metal complexes have been synthesized and characterized by means of elemental analysis, molar conductance analysis, IR, electronic spectra, EDS, X-ray powder diffraction analysis and TG-DTA analysis.

本文合成了15种金属配合物,应用元素分析、摩尔电导、红外光谱、能量色散谱、X-射线粉末衍射、热重-差热分析等手段对这些配合物进行了常规结构表征,确定了配合物的组成。

Rbs-3H2O was synthesized and itsstructure was analyzed with element analysis * UV, IR, NlVQ^ HPLC\ TG-DSC\molar conductance and X-ray diffraction analysis.

但是由于Sm-EDTMP的钠盐水溶性很大,不易形成沉淀或晶体,对于Sm-EDTMP的配合物结构研究尚未见详细报道,所以为了要表征其配合物结构,合成了Rbs·3H2O配合物,并通过元素分析、红外光谱、紫外光谱、高效液相色谱、热差分析、摩尔电导分析和X-射线粉末衍射对Rbs·3H2O的结构进行表征。

The complexes areneutral as shown by values of molar conductivity in aqueous solution, namely,〓 The crystal structure determinations show that, in complexes, metal ions werecoordinated by four nitrogen atoms and form slightly distorted square planar configuration,relationship between fluorene ring plane and coordination plane is similar to those betweenpeptide planes of β-folding in proteins. The complex molecules linked by hydrogen bonds formone dimension chain or two dimension network structure.

摩尔电导测定表明他们都是二氧四胺中酰胺氮去质子化后形成的产物。X-射线衍射晶体结构测定表明〓的铜、镍配合物的配位多面体都是稍微畸变的平面正方形,配合物分子中芴基平面与配位平面的关系类似于蛋白质β-折叠结构中肽平面之间的关系,配合物分子之间通过氢键连接成一维链状或二维网状结构。

The results indicated that the even mixture of catalyst C3, with the mixture of the coal ash and the paper-making black liquor in the ratio from 5:1 to 8:1 were dried on the resistance furnace, then calcinated in the muffle furnace at 750~800℃ for 10 minutes to obtain the silicon fertilizer with the soluble silicon above 30 percentage.

对黑液、粉煤灰及不同配比的硅肥进行了X射线衍射测试和扫描电镜测试,研究它们之间的不同,为硅肥制备工艺的进一步优化和硅肥的应用、机理研究提供一定的理论依据。

The composition of the Cr film was identified by X-ray diffraction, the interface of Chromium/Zircaloy was studied with scanning electron microscopy, the morphology of Cr film was observed with atomic force microscopy.

使用X-射线衍射仪对沉积薄膜进行了物相分析,采用扫描电子显微镜和原子力显微镜对薄膜的表面形貌及膜/基界面做了观察分析。

In accordance with the results of X-ray diffraction of the powder on mortar surface and pore structure tests of mortar covered with painting reagent s on exterior walIs of building, mechanism of painting reagent s protecting against acid rain corrossion has been theoretically analysie

根据涂刷涂抹剂的建筑外墙砂浆的结构和砂浆表面粉末的x-射线衍射测试结果,从理论上分析了涂抹剂抗酸雨侵蚀的机理。

Polyimide ; film ; orientation structure ; film property ; X-Ray diffraction ; pin hole photograph ; determination of structure

聚酰亚胺;薄膜;取向结构;薄膜性能; x 射线衍射;针孔照相;结构测定

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