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The rutile TiO2 powder photocatalyst was prepared by hydrolysis process, and it was coated with WO3 by dipping process using tetrabutyl titanate (C16H36O4Ti) as raw material. The catalysts were characterized by XRD, Raman spectra, TEM and diffuse reflectance UV-Vis spectra.

以钛酸丁酯为钛源,采用水解法制备金红石型TiO2粉体,用浸渍法将制备的TiO2粉体包覆不同浓度的WO3(记为WO3-TiO2),并采用X射线衍射、拉曼光谱、透射电镜和紫外-可见漫反射光谱等手段对所得的光催化剂进行了表征。

The rutile TiO2 powder photocatalyst was prepared by hydrolysis process, and it was coated with WO3 by dipping process using tetrabutyl titanate(C16H36O4Ti) as raw material. The catalysts were characterized by XRD, Raman spectra, TEM and diffuse reflectance UV-Vis spectra.

摘 要:以钛酸丁酯为钛源,采用水解法制备金红石型TiO2粉体,用浸渍法将制备的TiO2粉体包覆不同浓度的WO3(记为WO3-TiO2),并采用X射线衍射、拉曼光谱、透射电镜和紫外可见漫反射光谱等手段对所得的光催化剂进行了表征。

The product structure, compositional information and spectral properties were carefully characterized by XRD, IR and DTA-TG, and the mineralization mechanism of mineralizer was studied during the process of calcium aluminates preparation.

借助于红外光谱、 X射线粉末衍射、差热-热重分析等手段对不同原料的铝酸钙粉的结构、组成及性能进行了表征和研究,并对矿化剂在合成铝酸钙中的矿化机理进行探讨。

Guangzhou 510650, P.R.China)Abstract: A new type of photoelectrode was innovated by anodising titanium mesh in H2SO4 solution and named Ti/TiO2 mesh electrode.

摘 要:采用电解氧化金属钛网的方法制备新型光电极Ti/TiO2,采用X射线衍射仪、激光拉曼光谱仪与扫描电镜测试电极的表面晶体结构与表面形态。

Proton and C-13 NMR spectroscopy analysis assessed the carbon aromaticity of the supercriticaly extracted bitumens to be 0.32-0.34, it appears in fair agreement with the aromaticity determined directly by using solid state C-13 NMR techniques.

然后,分别用核磁共振波谱法测定它们的芳碳率,结果分别为0.30和0.34。将超临界流体抽提沥青分离为族组分,用核磁共振与X-射线衍射法分析测定它们芳碳部分的主要结构参数及其聚集态。

The influence factors of the catalysed combustion process are discussed.

借助燃烧率测定,X射线衍射及差热分析等研究方法,讨论了无烟煤催化过程中的相关影响因素。

A chiral phase transfer catalyst, N-benzyl quinine bromide, was synthesized from natural chiral compound. And 2,5-bimethyl-4-(3-nitrobenzene)-1,4-bihydrogenation pyridine-3--4-methyl formate (viz. nitrendipine) was synthesized by this chiral phase transfer catalysis, and characterized by elemental analysis, infrared spectrum,1H nuclear magnetic resornace, and X-ray single-crystal diffraction.Key words: ammonium; chiral phase transfer catalyser; crystal structure

通过对天然手性物质进行修饰合成手性相转移催化剂N-苄基溴化奎宁,并对目标分子2,5-二甲基-4-(3-硝基苯)-1,4-二氢吡啶-3-甲酸乙酯-5-甲酸甲酯进行不对称催化合成,并通过红外光谱和核磁共振氢谱对化合物进行了表征,用X射线单晶衍射法测定了该化合物的晶体结构。

The strength development of the system is also studied.The result shows that the strength of the minerals is obviously higher than calcium sulphoaluminate and the optimum composition is found.In addition,we have analysed the formation and hydration mechanism of the clinkers by means of XRD,IR,SEM,DTA and so on.

发现该系列部分矿物的强度明显高于硫铝酸钙,并找到了最佳矿物组成点﹔应用X射线衍射仪、红外光谱仪、扫描电子显微镜和差热分析等测试手段,对熟料矿物的形成和水化机理进行了初步分析研究。

To study high temperature corrosion behavior on materials during solid waste incineration, laboratory corrosion tests were performed to iron, cast iron, 20# carbon steel, stainless steel in oxidizing gaseous environments which included O〓, SO〓, H〓O, HCl, Cl〓and some ashes coming from self-designed incinerator, the Xunde's one and synthetic ashes. The synthetic ashes are used as corrodents composed of chlorides , sulfates and oxides.

最后,本论文为揭示材料垃圾焚烧过程中的高温腐蚀行为,借助于腐蚀重量实验,X-射线衍射仪,扫描电子显微镜,电子能谱等分析测试手段,研究了铁、铸铁、20#碳钢和不锈钢在垃圾焚烧环境中的高温腐蚀行为及腐蚀动力学。

The influences of deposition time on the covercivity and saturation magnetization of electroless CoWP thin films were studied, and the surface topography, elemental composition, micro-structure and magnetic properties of CoWP thin films were tested respectively by FSEM , XRD and VSM.

研究了施镀时间对化学镀CoWP薄膜矫顽力和饱和磁化强度的影响,并利用场发射扫描电子显微镜、X射线衍射和振动样品磁强计研究了CoWP磁性薄膜的表面形貌、成分、微结构及磁学性能。

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