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衍射线

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Products on the sulphurized surfaces of cerussite and smithsonite have been studied by means of infrared spectra,Auger electronic spectra,X-ray pho- toelectron spectroscopy and X-ray diffraction techniques etc.

本研究采用红外光谱、俄歇电子能谱、X 射线光电子能谱、X 射线衍射等手段测定了白铅矿、菱锌矿硫化表面产物。

Significant amorphous transformation and chemical chain scissions were observed, which depended strongly on ion fluence and electronic energy loss near the sample surface.

用35MeV/u的Ar离子室温下辐照多层堆叠的半晶质的聚酯膜,采用X射线衍射技术和X射线光电子谱仪分析研究了辐照引起的表面结构和组分的变化。

The electrodeposited films were characterized by X-ray diffraction, scanning electron microscopy and energy dispersive X-ray spectroscopy for structural, morphological and componential properties.

采用X射线衍射、扫描电镜和X射线能谱对预制层的结构、形貌和成分进行了表征。

It is very difficult to eliminate these influence factors completely by conventional treatment. Surface properties and surface treatment of ultrafine red phosphorus and MMT and their interface properties with polymer matrices were studied in this thesis. The results were characterized by GC, FTIR, XRD, DTA, TG, XPS, UV, SEM, TEM and other physical and chemical methods. The main contents are as following: 1. The study of factors influencing ultrafine red phosphorus's invariability and phosphine liberation indicated red phosphorus undergone oxidation and dismutation reaction in air, and trace ion of iron, copper and nickel fastened water absorption and oxidation, in which the effect of copper ion was the most, while aluminium and zinc ion could slow down red phosphorus'oxidation, and silver ion had the best effect on red phosphorus moisture absorption. Inhibitors such as aluminium hydroxide, magnesium hydroxide, organic phenol and ferrous potassuim cyanide had a good effect on reducing red phosphorus moisture absorption and restraining phosphine liberation.

本文围绕纳微米材料的表面处理及其在高聚物基体中的应用这一主题,系统地研究了超细红磷和蒙脱土两种常见材料的表面特性、表面处理方法及其与高聚物基体的界面特性,通过气相色谱、红外光谱、X射线衍射、差热、热重、X射线光电子能谱仪、紫外光谱、扫描电镜、透射电镜等现代分析仪器以及其它物理、化学方法对实验结果进行了表征和分析,全文主要内容如下: 1、对影响超细红磷安定性的因素以及磷化氢的缓释研究表明:红磷在空气中发生缓慢氧化、歧化反应,微量的铜、铁、镍等金属离子增加了它的吸水和氧化速度,其中铜离子的作用最为明显,而铝、锌等离子减慢了红磷的氧化速度,银离子对减少红磷的吸湿性效果最好。

X-ray ESCA and X-ray diffraction instrument are used to analyze elements and structure on EDMed surface.

采用X-射线能谱仪和X射线衍射仪对混粉电火花加工表面进行了成分和结构分析。

From the transform infrared spectroscopy and X-ray photoelectron spectroscopy spectra, the hydroxyl and ethoxyl groups of the silica sol drawn from partially hydrolysis and polycondensation between TEOS and MTES can react with PA6 precursor.

红外图谱和X射线光电子能谱分析结果显示,硅溶胶的羟基和未完全水解的烷氧基能够与PA6的前驱体发生杂化反应。X射线衍射结果显示,采用本实验方法制备出的PA6和疏水型PA6/SiO2有机无机杂化材均为α晶型,而DSC结果表明,PA6/SiO2有机无机杂化材料的熔点略高于PA6。

Pure iron specimens were implanted by nitrogen ions with a fluence of 7×1017 ions/cm2 using ion beam implantation at an extracted voltage of 40kV.Composition and valence studies were carried out by X-ray photoemission spectroscopy;Glancing angle X-ray diffraction was employed to examine the phase transformation.

采用40kV的氮等离子体离子注入工业纯铁,注入剂量为7×1017ions/cm2,X射线光电子能谱研究表面注入层元素的成分和价态,X射线衍射分析注入层的物相转变,采用恒电位极化腐蚀试验研究了离子注入后材料在人工模拟体液中腐蚀行为。

In this paper, the structural change and its product s of kaolinite at 680-980℃ have been studied by DTA.

作者采用差热分析、红外光谱、X射线衍射,X射线萤光分析等现代测试技术,对高岭石在680—980℃之间的结构变化及其产物进行了深入的研究。

The particles were characterized by transmission electron microscopy, X-ray diffraction, vibrating sample magnetometry, dynamic light scattering, thermogra- vimetric analysis, Fourier transform infrared spectroscopy, and X-ray photoelectron spectroscopy.

利用透射电子显微镜、X射线衍射、振动样品磁强计、动态光散射仪、热重分析仪、傅里叶变换红外光谱仪、X射线光电子能谱仪等对其进行表征。

The surfaces of the grids were analyzed by x-ray diffraction and x-ray photoelectron spectroscopy.

然后,对样品表面进行了X—射线衍射测量和X—射线光电子能谱的测量。

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