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The structure was investigated by XRD and TEM, combining with the calculated metastable phase diagram. The results show that it is possible to obtain coupled structure in Zn-2%Cu peritectic alloy by rapidly unidirectional solidification method.

利用X射线衍射仪及透射电镜对层片状组织进行了相组成的分析,并结合计算亚稳相图对该组织的相及组织形成规律进行了分析,结果表明在快速凝固条件下Zn-2%Cu包晶合金中实现共生生长是可能的。

The samples were characterized by XRD and SEM, and the permeant selectivity of the membrane was characterized by single-gas at room temperature.

用X射线衍射和扫描电镜表征分析了沸石膜的形态,并通过单组分气体渗透实验对合成膜管的渗透性能进行了测试。

The scale inhibition mechanism of PESA was proposed on the basis of characterization of transformation of calcium carbonate crystal by means of X-ray Diffraction and scanning electron microscopy. The effect of temperature on corrosion inhibition efficiency of PESA was investigated and the Bockris substitution model is proposed to study the thermodynamics of inhibiting process of PESA. The calculation results show the adsorption of PESA on carbon steel is a spontaneous exothermic process with the increase of entropy.

通过X射线衍射和扫描电镜分析手段研究了聚环氧琥珀酸加入前后碳酸钙垢晶型的变化,在此基础上探讨了聚环氧琥珀酸的阻垢机理;考察了温度对聚环氧琥珀酸缓蚀性能的影响,根据Bockris置换模型,计算出中性水质中聚环氧琥珀酸在碳钢表面吸附的热力学函数,计算结果表明:聚环氧琥珀酸在碳钢表面的吸附是一个放热、熵增、自动发生的过程。

Researchers have validated the mass deposition process in small biomolecules and pharmic molecules induced by heavy ion implantation, and researches on modification of...

将来可先应用稳定性和放射性重离子束注入生物和药物分子,然后用X射线衍射、电子显微镜放射自显影和图像处理等技术对重离子注入质量沉积开展进一步的研究。

In this research, two novel compounds in which alkylenedithiomethylene Malonic acid act as the main coordination agents and the compounds containing N atom (such as pyridine, Phenanthroline Ethanediamine and 4,4'-Bipyridinyl) act as the associating coordination agents have been synthesized by the means of solution and solid-liquid diffusing reactions. 9 coordination complexes and polymers have been designed and synthesized in which the transition metals Cu and Zn acted as the centre ions. These compounds have been characterized by X-ray single crystal diffraction analysis, and some properties of them have been tested and analyzed.

本论文设计合成了两种结构新颖的含有二硫缩烯酮结构的丙二酸类化合物,以此为主要配体,以含氮化合物(吡啶、邻菲罗啉、乙二胺和4,4'-联吡啶)为辅助配体,采用常规溶液合成和固-液相扩散等方法,设计合成了9个过渡金属Cu和Zn离子配合物和配位聚合物,采用单晶X-射线衍射等技术对晶体结构表征,并对其部分性质进行了测试和分析。

The photoluminescent properties and structure of the samples were studied by fluorescence spectroscopy and X-ray diffraction, respectively.

用X射线衍射仪和荧光光谱仪对其结构和光致发光性能进行了测试分析。

In the present paper, the silver-intermediate in development process of PTG material-disilver phthalate (Ag2PA) was prepared by the liquid deposition method, and Ag2PHZ2PA·H2O complex was synthesized successfully by liquid dispersion means using Ag2PA and phthalazine as the reactants. The composition of Ag2PA and Ag2PHZ2PA·H2O was determined by ICP-AES and elemental analysis,...

采用液相沉淀法合成了PTG材料热显成像过程的含银中间体邻苯二甲酸二银(Ag2PA),并进一步使其与酞嗪络合形成了Ag2PHZ2PA.H2O配合物,通过元素分析、电感耦合等离子体原子发射光谱分析对Ag2PA与Ag2PHZ2PA.H2O配合物的元素组成进行了确定,采用X射线粉末衍射分析、傅里叶变换红外光谱分析以及热分析等方法对Ag2PA与Ag2PHZ2PA.H2O进行了表征,实现了对PTG材料热显成像过程含银中间体的定性分析。

The effects of the crystallization degree, the uniformity of charge distribution, the surrounding hydration cation and the pillaring mode of organic molecule on the interlamellar space of hydrobiotite were finally discussed.

通过X射线衍射与红外光谱进行表征分析,讨论了结晶度、电荷分布均匀性、水合阳离子及不同有机分子柱撑模式对晶层层间距的影响。

The effect of preparation method of Al-pillared agent、rectorite suspending concentration、Al-pillared agent dosage、pillaring reacting temperature、pillaring reacting time are investigated;The optimum process condition is determined. The capability has compared with the nature rectorite. It is characterized by X-ray Diffraction and infrared spectrum.

探讨了铝交联剂制备方法、累托石悬浊液浓度、铝交联剂的用量、交联反应温度、交联反应时间等各因素对其制备的影响规律,确定了铝交联改性的最佳工艺条件;进行了与天然累托石的性能比较;运用红外光谱、X-射线衍射对所制铝交联累托石进行了表征。

In this paper, two different methods have been used to synthesize the LiInS2 polycrystalline materials.

本文采用两种方法合成了LiInS2多晶原料,对所获LiInS2多晶原料进行了X射线粉末衍射和差示扫描量热分析。

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