衍射线

Three single crystals of N-nitrobenzene, N-acyl dehydroabietic hydrazine 7c single water compounds, N, N-acyl dehydroabietic hydrazine 7l and 2,5 - dehydroabietic-1, 3,4 - oxadiazole 8g were obtained for the first time. X-ray diffraction analysis of these crystals showed dehydroabietic acid skeletons were contained in these crystal molecules.

首次得到N-去氢枞基，N-对硝基苯基双酰肼7c一水化合物、N，N-二去氢枞基双酰肼7l和2，5-二去氢枞基-1，3，4-噁二唑8g 3个单晶，并用X射线单晶衍射进行了解析，晶体中均含有去氢枞酸分子骨架。

Finally, the cytotoxic and antibacterial activities of the oxamido-bridged binuclear complexes were studied in vitro.. This dissertation consists of three sections as follows:1. The crystal structure of a oxamide dinitrate,(1) [H_4dmaeoxd](NO_3)_2 H_2dmaeoxd = N,N\'-bis[2-ethyloxamide, has been obtained. The diversity of complexes with different structures is carried out by successful synthetic strategy of controlling species of metal ions, counter anions, pH values and solvents in the course of synthesis. Four dinuclear complexes bridged by trans-dmaeoxd2-: [Cu_2_2](ClO_4)_2 (2), [Cu_2_2](ClO_4)_2 (3),、[Cu_2(Me_2phen)_2](ClO_4)_2 (4), [Cu_2_2(H_2O)_2] (5); Four dinuclear complexes bridged by cis-dmaeoxd2-: [NiNi_2](ClO_4)_2 (6), [CuNi_2](ClO_4)_2·2CH_3OH (7), [CuZn_2]-(ClO_4)_2·2H_2O (8), [Cu(H_2O)Ni_2](ClO_4)_2.0.5CH_3OH (9); three 1-D polynuclear complexes: [Cu_2]_n·nH_2O (10), [Cu_2(H_2O)_2-]_n·4nH_2O (11), [Cu_2(H_2O)]_n(NO_3)_n·2nH_2O (12); one 2-D polynuclear complex,[Cu_6_3(μ_3-OH)_2(H_2O)_2]_n(ClO_4)_(4n).2nH_2O (13); the others: [VO(H_2O)]·2H_2O (14), [Zn_2_4](ClO_4)_2·H_2O (15), [Cu_2]·2DCM (16) have been synthesized and characterized by X-ray single crystal diffraction, elemental analysis, IR spectra.

本论文主要包括以下三部分：一、合成得到了一个草酰胺配体硝酸盐的单晶结构，[H_4dmaeoxd](NO_3)_2 (1)；通过调控金属离子的种类、端基配体、抗衡阴离子、溶剂、pH值等条件定向合成了四个反式草酰胺桥联双核铜配合物：[Cu_2_2](ClO_4)_2 (2)、[Cu_2_2](ClO_4)_2 (3)、、[Cu_2(Me_2phen)_2](ClO_4)_2 (4)、[Cu_2_2(H_2O)_2] (5)；四个顺式草酰胺桥联同/异双核配合物：[NiNi_2](ClO_4)_2 (6)、[CuNi_2](ClO_4)_2·2CH_3OH (7)、[CuZn_2]-(ClO_4)_2·2H_2O (8)、[Cu(H_2O)Ni_2](ClO_4)_2.0.5CH_3OH (9)；三个一维聚合物： [Cu_2]_n·nH_2O (10)、[Cu_2(H_2O)_2-]_n·4nH_2O (11)、[Cu_2(H_2O)]_n(NO_3)_n·2nH_2O (12)；一个二维聚合物： [Cu_6_3(μ_3-OH)_2(H_2O)_2]_n(ClO_4)_(4n)。2nH_2O (13)；单核钒配合物[VO(H_2O)]·2H_2O (14)、草酸根桥联双核锌配合物[Zn_2_4](ClO_4)_2·H_2O (15)、美洛西康铜配合物[Cu_2]·2DCM (16)，利用元素分析、摩尔电导、红外光谱、电子光谱和单晶X-射线衍射对上述所得化合物进行了结构表征，探讨了结构影响因素，并研究了其超分子结构。

Based on the failure analysis of hot roll, this paper optimizedly adjusts alloy system and summarizes the experience of rolling wiresand improves ail processing properties. Then, it analyses the effects on some natural parameters such as alloy transfer coefficient, surfacing layers, welding current and arc voltage etc.. It confirms the fitting ageing technique. Also, it discusses the microscopic structural transformation back and forth ageing and the effects on hardness change of overlaying metal by some alloying elements including C, Cr, V, W, Mo, Ni, Mn, B, Re through OM, SEM and X-ray diffraction analyses. Finally the abrasive resistance, red hardness, thermal fatigue property and anti-high temperature oxidability are investigated in experimentation.

全文在热轧辊失效分析的基础上优化调整合金体系，总结了焊丝轧制的经验，改善各种工艺性能，分析了几个特性参数的影响，确定了适宜的时效工艺，并通过光学显微镜、扫描电镜和X-射线衍射对时效前后的显微组织转变以及部分合金元素如C、Cr、V、W、Mo、Ni、Mn、B、Re对堆焊层硬度变化的影响进行分析，最后通过试验考察了堆焊层金属的耐磨粒磨损性能、红硬性、耐热疲劳性和抗高温氧化性。

From 500℃ to 550℃, the oxide scale presents a relatively compact morphology, the oxidational wear is the principal wear mechanism and the wear rate is very slow at 500℃ owing to the anti-friction effect of the oxide scale.

本文研究了5CrNiMo在400℃、500℃、550℃及600℃温度下的滑动磨损行为，利用扫描电镜，波谱仪及X射线衍射仪对磨损面形貌及成分进行了分析，结果表明：5CrNiMo钢磨损机制随温度的变化而变化，400℃时表现为疲劳剥落和磨粒磨损，500℃至550℃时表现为氧化磨损，600℃时主要是粘着磨损。

The result shows the mechanical property of electrical porcelain sintered in reduce-atmosphere is better than in oxygenic.

采用 X射线衍射、扫描电镜等测试技术对材料内部的晶体结构进行了分析，讨论了不同气氛下铁、钛杂质在电瓷材料中的作用机

The structure and morphology of the PANI were characterized by IR spectra, XRD patterns, and SEM images.

通过红外光谱、X射线粉末衍射以及电子扫描电镜对掺杂态PANI的结构和形态进行了表征。

The structure of the polymer was preliminarily studied by FT-IR, 1H-NMR, UV. The crystallization behaviour and thermal property of the polymer were also studied by X-ray diffraction and DSC, TG. The results shows that the polymer is the structure of PASI.

通过红外、核磁、紫外对聚合物的结构进行了初步表征，通过DSC、TG初步测试了聚合物的热性能，通过X射线衍射初步表征了聚合物的结晶性。

The X-ray diffraction shows that the resin is crystalline. The heat analysis shows that the resin is well heat-resistant and has very good thermal stability and T=101℃. The T is better 10℃ than polyphenylene sulfide. The PASI resin will be applied abraod.

表征结果表明，聚合物为设计聚芳硫醚酰亚胺结构；X射线衍射表明聚合物为结晶性聚合物；热性能测试表明，聚合物的玻璃化温度为101.91℃，高于聚苯硫醚(87.00℃)，聚合物具有良好的热性能。

The analysis of X-ray diffraction and scanning electron microscope energy dispersion spectra show that the primary hydrolysis products of antimony pentachloride and its hydrochloric acid solution are amorphous antimony oxide rather than SbO2Cl.

X射线衍射和扫描电镜能谱分析表明：五氯化锑及其盐酸溶液的初始水解产物不是SbO2Cl，而是一种非晶态锑氧化合物；随着水解母液酸度的降低，五氯化锑溶液水解产物陈化五天后的晶型由非晶态向晶态变化；五氯化锑溶液水解产物经无水乙醇洗涤后水解产物仍为非晶态，而经蒸馏水洗涤虽主要为非晶态，但有少部分结晶的Sb2O5·4H2O晶体存在。

Mesoporous Ti02 is also synthesized with glycerol and pentaerythrite as temp-lates separately.It is characterized by TEM,XRD,BET and FTIR etc.

以多元醇类化合物结构相近的丙三醇，季戊四醇有机小分子化合物为模板剂制备出了中孔纳米二氧化钛粉体，对所得粉体进行了透射电镜，傅立叶红外，N2吸附一脱吸，粉末X一射线衍射等的测试。

And Pharaoh spoke to Joseph, saying, Your father and your brothers have come to you.

47：5 法老对约瑟说，你父亲和你弟兄们到你这里来了。

Additionally, the approximate flattening of surface strip using lines linking midpoints on perpendicular lines between geodesic curves and the unconditional extreme value method are discussed.

提出了用测地线方程、曲面上两点间短程线来计算膜结构曲面测地线的方法，同时，采用测地线间垂线的中点连线和用无约束极值法进行空间条状曲面近似展开的分析。