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Notably, compounds 12–14 can be described as a 3D open–framework with nano–channels, compound 15 can be described as a 3D open–framework with double helical channels, while compound 16 can be described as a 3D heterochiral coordination polymer with double helical channels, which can be obtained by spontaneous resolution from the racemic phosphonic acid.X–ray powder diffraction analysis shows that compound 16 is a pure phase. Surface photovoltage spectroscopy of compound 16 indicates that it possesses positive SPV response in the range of 300–600 nm and shows p–type semiconductor characteristic.

值得注意的是,化合物12-14为具有一维纳米孔道结构的三维开放骨架结构,化合物15是具有双螺旋孔道的三维开放骨架结构,而化合物16是外消旋的有机膦酸配体通过自发拆分而形成的具有双螺旋孔道的多手性三维开放骨架结构。X-射线粉末衍射分析表明化合物16为纯相;化合物16的表面光电压光谱分析中,在300-600nm范围内有3个正的光(来源:ABC论文12网www.abclunwen.com)伏响应带,表明它具有p型半导体的特征;化合物16的诱导表面光电压谱进一步确定它的p型半导体的特征;磁性研究表明,化合物16中两Mn原子之间存在弱的反铁磁相互作用。

A series of studies by using X-ray monocrystal analysis as the main methods on rare earth complexes with p-amino acids, heteronuclear complexes with a-amino acids and some complexes with different ligands were reported in this paper.

本论文以单晶X-射线衍射为主要手段对β-氨基酸稀土配合物、α-氨基酸异核金属配合物和以α-氨基酸为混合配体的金属配合物进行了较为系统的研究。

Effects of hexamethylene tetramine surfactant on morphology of the products are studied by using X-ray diffraction pattern, scanning electron microscopy.

制得的样品利用X射线衍射仪、扫描电镜及紫外分光光度计进行表征。

The mechanisms of phosphate sorption on hydrotalcite and its calcined product are different, which has been confirmed by X-ray diffraction examination.

水滑石及其焙烧产物对磷的吸附具有不同的机理,并得到了X射线衍射的证实。

ABSTRACT Using the θ-θ X-ray diffractometer, the structure of liquid Al-Fe system alloys at different composition was investigated at a constant temperature 1550℃. The relationship between parameters of the pre-peak in the structure factor and composition was studied. In addition, the structural change of the liquid hypoeutectic Al-Fe alloy and pure Al etc.

本文利用θ-θX射线衍射仪,在1550℃研究了不同成分Al-Fe合金的熔体结构,探讨了结构因子上的预峰参数随成分变化的规律,以及亚共晶Al-Fe合金和纯。。。

In this paper,we describe the preparation of YBCO coated conductor by IBAD technology route and the latest research results in the world.

采用X射线衍射仪分析YSZ缓冲层的取向;利用原子力显微镜和扫描电镜观察其表面形貌。

Using Gassian98 with LANL2DZ basis sets, the quantum chemistry calculation of the model was performed.4. A series of ligands which all include imidazolyl group were designed and synthesized. The crystal structure of one of them was determined by X-ray diffraction.

设计并合成了一系列含有咪唑基的配体,应用X-射线衍射方法测定了其中一种配体的晶体结构,并用Gaussian98程序包进行了量子化学计算。

The results show that the polymer determines the electricity conducting of coal filled polymer composites. The coal filled PP composites is an insulating material, and be independent of coal type, its direct current resistivity is above 10〓Ω·cm. The resistivity drops with the content of coal when using anthracite, but it is also above 10〓Ω·cm, and the surface modification of coal, especially alkylated, resumes the insulance of composites.

X射线衍射测试表明即使在高变质程度下煤中的石墨晶区含量仍较低,煤填充聚合物复合材料电性能主要由基体材料性能决定,通过动电容静电计对煤填充聚丙烯复合材料直流电导性研究表明,煤填充聚丙烯复合材料是绝缘材料,其绝缘电阻在10〓Ω·cm以上,在高含量情况下,仍能保持良好的绝缘性,而与煤种无关。

The structure of the composite was characterized and analyzed by XRD, FTIR and TG. The test results proved that the structure of bentonite did not change except that the interlamellar spacing increased a little during its aggregation. The dispersion property and thermal stability of the composites was enhanced thereby.

使用X射线衍射、红外和热重对复合材料的结构进行了表征和分析,结果表明,膨润土在聚合过程中除了层间距有所增大外,基本结构不变,而且分散度提高;吸水性复合材料的热稳定性提高。

The fresh and discharged catalysts from the isoamylene unit are characterized by XRD,TG-DTA,FT-IR and the pore structure analysis.

利用X射线衍射、热重分析、红外光谱和孔结构分析对新鲜的和从装置卸出的催化剂进行表征,并对催化剂活性下降的机理进行了讨论。

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47:5 法老对约瑟说,你父亲和你弟兄们到你这里来了。

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