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衍射线

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Their properties were characterized by X-ray diffraction, UV-Vis diffuse reflection spectroscopy, and scanning electron microscopy.

用扫描电镜、X射线衍射和紫外-可见漫反射光谱对样品进行表征。

The distribution of temperature stress was calculated by finite element analysis. The results showed when the surface temperature of concrete was higher than 110℃, the temperature stress was more than 4 MPa without regard to the creep. This might be lead to the damage of the surface of concrete. At the same time, a lot of microstructure analysiss such as XRD, SEM, IR, HSA etc. were done to analysis the difference of the component and microstructre of concrete before and after corrosion. The results indicated that the decomposion of CSH gel and calcium hydroxide and the creation of dilatability calcium oxide were the internal reason of the deterioration of concrete in the corrosion form of high heat.

该文通过有限元方法计算了由于温度而产生的结构应力分布,计算结果表明当混凝土表面温度超过110℃时,如不考虑徐变时表层混凝土受到的温度应力将超过4MPa,这使得表层混凝土很容易因温度应力而破坏;同时通过X射线衍射分析、扫描电子显微分析和混凝土孔结构分析等多种微观结构测试手段,分析了混凝土受热前后的宏观性能以及微观组成和结构的变化,指出混凝土原水化产物如水化硅酸钙凝胶和氢氧化钙的分解以及膨胀性产物氧化钙的产生是高热腐蚀形式下混凝土破坏的内在原因。

Simulation experiments make sure that the dilatometer is able to detect the expansion changes in low temperature. The high temperature reheating process with dilatometer analysis indicate that the firing temperature are little higher than 900℃ for one sample and lower than 900℃ for other five samples with firing temperature ranges of 550~650℃, 650~750℃ and 750~900℃. The results from mineral composition analysis of the samples by X-ray diffraction provide further evidence of the reliability of the thermal expansion measurement.

模拟实验表明,所采用的热膨胀仪能适应低温法测温实验;用热膨胀高温法测出早期陶片中有一块样品原始烧成温度略高于900℃,其余5块样品皆低于900℃;通过热膨胀低温法较为准确地测出这五块样品原始烧成温度是分别介于550~650℃、650~750℃、750~900℃三个范围,而X射线衍射分析结果从物相成分的角度证明了测温结果的可靠性。

The single crystal X-ray diffraction analysis showed that the asymmetric diol 8 isan "abnormal" McMurry reaction product.

单晶X-射线衍射分析结果证明,不对称的二醇8是一种新型的偶联产物。

Iron-based perovskite-type compounds modified by Cu, Zn, Ni were prepared through sol-gel process to investigate their catalytic activities of NO direct decomposition. XRD analysis reveals that the samples calcined at 750℃ are pure perovskite phase.

采用溶胶-凝胶方法合成了Cu,Zn,Ni改性的钙钛矿复合氧化物系列催化剂。X射线衍射分析表明,750℃焙烧的此类催化剂在掺杂范围内均具有钙钛矿基本结构。

The products are characterized by scanning electron microscopy, X-ray diffraction and energy dispersive spectroscopy.

用X-射线衍射、扫描电子显微镜和能谱对产物进行表征。

Scanning electron microscopy observed that the mesoporous silica single crystal had a regular rhombic dodecahedron morphology with a uniform particle size of 5 μm.

扫描电子显微镜观察到这种介孔二氧化硅单晶具有菱形十二面体形貌, X射线衍射和透射电子显微镜测试结果证实这种介孔单晶属于简单立方Pm3n对称结构。

The construction of branched-chain sugar was carried out by hydroboration-oxidation of a double bond in the corresponding hexose.

通过相应的烯糖9的硼氢化-氧化反应构建了支链糖11,同时分离到一系列还原的副产物7c-e,通过X-射线晶体衍射确定了7c和7e新的手性中心的构型。

This paper also studied the relation between structures and properties of PVAC/PP composite filaments by X-ray and double refraction.

同时用X射线衍射及双折射等方法研究了PVAC/PP复合纤维的结构与力学性能的关系。

According to XRD analysis, the high concentration doping of dysprosium ions in Fe3O4 can not be obtained due to the difference of ionic radius, and Fe^3+ ions are replaced by only a small amount of dysprosium ions.

通过X射线衍射分析发现,由于离子半径的不匹配,Fe3O4中稀土离子的高浓度掺杂不能实现,仅有极少量的稀土离子取代了Fe3O4中的Fe^3+。

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