衍射光谱

The thermal behavior of silver behenate has been studied by infrared spectroscopy, X-ray diffraction, combined thermogravimetry-differential thermal analysis-mass spectrometry. The results indicated that complicated phase transitions took place while heating silver behenate,but there were two distinct thermal transitions. During the first transition at 138°C, the alkyl chains of silver behenate were transformed from an ordered into disordered state.

通过采用粉末X射线衍射、红外光谱、热重-差热分析与质谱联用技术，对山嵛酸银纳米晶体的热行为研究发现，山嵛酸银受热发生了一系列相转变，它有两个明显的突变：即在138℃左右，山嵛酸银的烷基链从高度有序转变为无序状态；在231℃左右，山嵛酸银发生了热分解，其主要分解产物为银纳米粒子和山嵛酸。

The structures of the two types of kaolinite and their benzamide intercalation compounds were characterized by the powder X-ray diffraction and Fourier-transformed infrared spectroscopy.

利用X射线粉末衍射和Fourier变换红外光谱实验分析了2种高岭石及其苯甲酰胺插层复合物的结构。

In our study, polyimide hybrid films containing bimetalic compounds were prepared by codoping poly with a bariumand titanium precursor prepared from Ba(CH_3COO)_2, Ti_4, and acetic acid followed by casting and thermal curing.

陶瓷粉BTL是由Ba(CH_3COO)_2，Ti_4和乙酸制成的钡钛前驱物，采用溶胶凝胶法合成，并由红外光谱和X-射线衍射图证明，在650℃BTL完全转化为BaTiO_3晶体。 3。通过两步法合成含陶瓷粉的聚酰亚胺复合材料。

Bipyridyl and 1,10-phenanthroline (L3), Cl3SnCH2CH2COORo L (L= L1, a; L2, b; L3, c), formed by low-heating solid-state reaction. The crystal structures of 1 and 2 show that the tin atom adopts a distorted trigonal bipyramid geometry via intramolecular carbonyl oxygen to tin coordination [the distances of Sn-0 bond are 0.2351(6) ran for 1 and 0.2362(3) nm for 2]. Compound 1 belongs to monoclinic with space group P2/c, a = 0.9842(2) nm, b =1. 0923(8) nm, c = 1.23948(11) nm,/?= 93.894(15)°, V= 1.3294(4) ran3, Mr = 366.23, 7 = 4. Compound2 belongs to monoclinic with space group P2{/c, a = 1.04443(9) nm, b = 1.04823(7) nm, c = 1.28113(9) nm,/= 90. 953(8)°, V= 1.40239(19) nm3, Mr = 380.25, Z = 4

利用元素分析、红外光谱、核磁共振对其结构进行了表征，并通过X射线单晶衍射测定了1和2的晶体结构，二者均为具有分子内羰基氧原子配位的畸变三角双锥结构。1属于单斜品系，空间群P21/c， a=0.9842(2)nm，b=1.0923(8)nm，c=1.23948(11)nm，β=93.894(15)°，V=1.3294(4) nm^3，Mr=366.23，Z=4.2属于单斜晶系，空间群P21/c，a=1.04443(9)nm，b=1.04823 (7)nm，c=1.28113(9)nm，β=90.953(8)°，V=1.40239(19)nm^3，Mr=380.25，Z=4。

A two-fold penetration coordination polymer n (1)(bpy=4,4'-bipyridyl) has been synthesized through hydrothermal reaction and structurally characterized by single crystal X-ray diffraction method.

利用水热反应，合成了一个具有二重穿插结构的一价铜配位聚合物n(1)(bpy=4，4'-联吡啶)，并利用元素分析，X射线单晶衍射，红外光谱以及热重分析等手段对标题化合物进行了表征。

The structure of products was characterized by means of infrared spectra, wide-angle X-ray diffraction and differential scanning caloriimetry and the effect of deacetylation in course of konjac glucomannan carboxy methylation was analyzed.

运用红外光谱、广角X-射线衍射和示差扫描量热法表征产物结构并探讨脱乙酰基对KGM羧甲基改性的影响。

The chalcogenidometalates were characterized by elemental analysis, IR and X-ray crystallographic, and their thermal stability and optical properties were also investigated.

三、用元素分析、红外光谱、热重分析和单晶X射线衍射仪对合成的化合物进行了表征，测定了化合物的热稳定性和光学性质。

The mineralogical characteristics of dioctahedral micas have been studied by chemical analysis, XRD, IR, DTA, SEM and IEM.

用化学分析、X射线衍射、红外光谱、差热和热重分析、扫描电镜及透射电镜等研究了白云母、绢云母和伊利石的基本矿物学特征。

FT-IR spectra shows that the polyaniline is present primarily in the emeraldine salt form, and the polymeric chains interact with inorganic framework, most likely via V=O…HN hydrogen bonding. XRD,TG and DSC indicate that the lamellar structure of the V_2O_5 is preserved, PAn chains eliminate water form the interlamellar region and are partially inserted between the layers, and exist with extended-chain conformation owing to the confined environment.Electrochemical investigation in the range of 1.8~3.8V vs.

红外光谱表明复合物中PAn主要以导电聚苯胺盐的形式存在，PAn链与V_2O_5晶格之间可能形成了V=O…HN氢键。X射线衍射、热重和差示扫描量热证实了PAn/V_2O_5复合物保持了较规整的层间排列结构，PAn取代了V_2O_5干凝胶中的层间水而部分嵌入其片层间，由于受空间的限制，PAn分子链以比较伸展的链构象存在。

Firstly,two novel rare earth complexes(CH_2=CHO)Ln~Ⅲ[2,6-_2PhNSiMe _3]_2Li_3Ln=Y(2,Yb(3)containing arylamido and enolate mixed ligands have been synthesized by treatment of 2 equiv of of 2,6-~iPr_2PhNHSiMe_3 with exces n-BuLi at -78℃in THF for 12h,followed by reaction with 1 equiv of LnCl_3at 80℃for 24h in one-pot.All the two compounds were characterized by spectroscopic methods,elemental analyses,and a single-crystal X-ray diffraction study.

首先，-78℃下，在两当量的2，6-~iPr_2PhNHSiMe_3(1)THF溶液中加入过量的n-BuLi，反应12小时，再加入一当量的LnCl_380℃下，反应24小时，一锅法合成了含胺基、乙烯醇基混合配体的新型稀土金属配合物(CH_2=CHO)Ln~Ⅲ[2，6-_2PhNSiMe_3]_2Li_3Ln=Y(2、Yb(3)，上述化合物结构经单晶X-ray衍射、光谱和元素分析表征，表明我们得到的是一类新型的三价稀土配合物。

However, as the name（read－only memory）implies, CD disks cannot be written onorchanged in any way.

然而，正如其名字所指出的那样，CD盘不能写，也不能用任何方式改变其内容。

Galvanizes steel pallet is mainly export which suits standard packing of European Union, the North America. galvanizes steel pallet is suitable to heavy rack. Pallet surface can design plate type, corrugated and the gap form, satisfies the different requirements.

镀锌钢托盘多用于出口，替代木托盘，免薰蒸，符合欧盟、北美各国对出口货物包装材料的法令要求；喷涂钢托盘适用于重载上货架之用，托盘表面根据需要制作成平板状、波纹状及间隔形式，满足不同的使用要求。