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No entire nitrendipine crystals were observed visually in SEM photos. The results of X-ray diffraction and differential scanning calorimetry analysis indicated that the crystalline form of nitrendipine was highly dispersed in microspheres, so as amorphous state. The drug release rate of microspheres could be controlled with adjusting the ratio of solid dispersion carriers and retarding agents formulated. The agitation speed and temperature of the preparation process have distinct effect on micromeritic properties of microspheres. The release profiles of the microspheres were mainly affected by the stirring rate of paddle, the concentration of SDS and pH of dissolution medium. Cooling speed and time, however, have no evident influence on the drug release rate of the microspheres. The dissolution data showed that the mechanism of drug release from microsphers was mainly diffusion-controlled. The incorporation efficiencies of 3 batches sample were exceed 96. 8%, which implied that the current method was suitable for design sustained-release dosage form for poorly water-soluble drug.

在扫描电子显微镜下观察,在微球内外未发现尼群地平的完整结晶,X-射线粉末衍射和差示扫描量热试验结果也显示,尼群地平已经被高度分散在微球中;微球的释药速度可通过调整处方中固体分散体载体和阻滞剂的比例控制;制备温度和搅拌速度对微球的质量影响较大;溶出仪的搅拌速度,释放介质的浓度和pH对微球的释放有较大的影响;制备过程中的冷却速度和冷却时间对微球的释放行为影响不很明显;方程拟合的结果表明缓释微球的释药行为符合扩散机制;测定三批微球样品的包封率均在96.8%以上,表明该法适合于制备难溶性药物的缓释微球。

Meanwhile, the hardening process of phosphorous slag cement was also determined by trimethylsilylation method and mercury porosimeter.

利用X射线衍射、扫描电镜及差热分析等测试手段,对少熟料磷渣水泥的水化产物进行了分析,并结合三甲基硅烷化法和压汞仪对该种水泥的水化硬化过程进行了研究

The hydrated products and pore size distribution of high road fly ash cement s were studied by means of XRD,DTA,Mercury porosimeter,etc.

采用X -射线衍射、差热分析、微量热计及压汞测孔仪对公路粉煤灰水泥的水化产物、水化放热曲线、孔尺寸分布进行了研究。

The environmental transport of POPs in Dagu Drainage River selected as a typical example is reasonedly investigated in this article. Characteristics of sediment from DDR in Tianjin are analyzed. The mean value of TOC in sediments is as high as 8%, which is in favor of sorption POPs. The particle sizes of both suspended sediment and bottom sediment are mensurated by Malven Mastersizer. Silt accounts for about 60% in mass, while clay is about 10%. Particles of sediments belong to fine granule. Suspended sediment and bottom sediment mensurated by XRD mainly consist of quartz and illite, both account for 75.5% and 62.2%, respectively. The conformation of suspended sediment is very similar to bottom sediment from SEM photo.

采集自天津大沽排污河的底泥样品进行了特征分析:全河段底泥TOC含量较高,平均值约为8%,利于吸附POPs;Malven Mastersizer激光粒度仪测定了大沽排污河悬浮物和沉积物的粒径分布,结果表明主要以粉砂为主,占60%左右,其次为黏土,占30%左右,大沽排污河底泥颗粒属于细颗粒;悬浮物样品和表层沉积物样品经X射线衍射分析表明,石英和伊利石是大沽排污河底泥悬浮物及沉积物矿物的主要成分,两者之和分别占75.5%和62.2%;环境扫描电子显微镜结果表明,河流底泥悬浮物和沉积物的形态没有本质差别。

A functionalized superparamagnetic iron oxide nanoparticles were synthesized by reduction-precipitation method, and were modified by silicane coupling agent. The nanoparticles were evaluated by diffraction, scanning electron microscope and X-ray energy spectrometer.

用部分还原-共沉淀法制备了四氧化三铁Fe3O4纳米材料,用硅烷偶联剂进行了表面修饰,用扫描电镜,X-射线粉晶衍射,磁强计,X射线能谱仪等分析仪器对材料的相关性能进行了测定。

Effects of OREC contents on the dynamic rheological properties of modified asphalts were investigated by DSR.

采用熔融共混法制备了有机化累托石改性沥青,以X射线衍射表征了改性沥青微观结构,并通过动态剪切流变仪研究了OREC的用量对改性沥青流变性能的影响。

The membranes were characterized by X-ray diffraction, Fourier transform infrared, Scanning electron microscope, Transmission electron microscope, Differential Scanning Calorimetry and contact angle meter, and their swelling and sorption properties, diffusion properties, and pervaporation properties were investigated systematically.

利用X一射线衍射、红外光谱、扫描电镜和透射电镜、差示扫描量热仪以及接触角分析等手段对膜的微观形态进行表征,系统研究了膜的溶胀吸附、扩散以及渗透蒸发性能。

EDS results show that the content of carbon is 7.37% in nano-diamond/Ni brush electroplated composite coating. XRD results show that as the amount of nano-diamond increases, the grain size of coatings becomes smaller.

能谱仪分析结果表明,nano-diamond/Ni复合刷镀层中纳米颗粒特征元素C的质量分数为7.37%。X射线衍射分析结果表明,随着纳米金刚石加入量的增加,镀层表面晶粒尺寸逐渐减小。

The morphology, structure and composition of the final nano-products were characterized by scanning electron microscope, energy-dispersive spectroscope and x-radial diffraction analysis.

采用扫描电子显微镜、X射线衍射、EDS能谱仪和透射电子显微镜对其表面形貌、结构和成分进行分析,结果表明所得纳米线为In2O3。

The surface morphology and microstructure were observed by scanning electron microscope, X-ray diffraction and energy dispersive X-ray spectroscope, the surface resistivity was analyzed by avometer and SDHC digital.

用扫描电镜、X射线衍射、能谱等手段对镀层表面形貌、微观结构进行检测,并且使用万用电表和SDHC型数字点式测量仪对表面电阻率进行分析测量。

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