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Significant amorphous transformation and chemical chain scissions were observed, which depended strongly on ion fluence and electronic energy loss near the sample surface.

用35MeV/u的Ar离子室温下辐照多层堆叠的半晶质的聚酯膜,采用X射线衍射技术和X射线光电子谱仪分析研究了辐照引起的表面结构和组分的变化。

The morphology, occurrence and components of dawsonite were described, and the paragenetic sequence of sandstone and origin of CO2 forming dawsonite were investigated by polarization microscope, scanning electron microscope, Xray diffraction and MAT251 stable isotope mass spectrometer.

利用偏光显微镜、扫描电镜、X射线衍射分析仪和MAT251稳定同位素质谱仪,详细描述了片钠铝石的形貌、产状和成分,确定了含片钠铝石砂岩的成岩共生序列和形成片钠铝石的CO2的成因。

We used DGY 2 permanent measurement meter to measure the magnetic properties and demagnetization curve .

对 15 78B7基一系列不同工艺条件下制取的取向度不同的烧结磁体,用 X-射线衍射和磁性测量来分析永磁体织构和取向度与反磁化过程的关系,用 DGY- 2型永磁测量仪测试磁体退磁曲线。

Simulation experiments make sure that the dilatometer is able to detect the expansion changes in low temperature. The high temperature reheating process with dilatometer analysis indicate that the firing temperature are little higher than 900℃ for one sample and lower than 900℃ for other five samples with firing temperature ranges of 550~650℃, 650~750℃ and 750~900℃. The results from mineral composition analysis of the samples by X-ray diffraction provide further evidence of the reliability of the thermal expansion measurement.

模拟实验表明,所采用的热膨胀仪能适应低温法测温实验;用热膨胀高温法测出早期陶片中有一块样品原始烧成温度略高于900℃,其余5块样品皆低于900℃;通过热膨胀低温法较为准确地测出这五块样品原始烧成温度是分别介于550~650℃、650~750℃、750~900℃三个范围,而X射线衍射分析结果从物相成分的角度证明了测温结果的可靠性。

It is very difficult to eliminate these influence factors completely by conventional treatment. Surface properties and surface treatment of ultrafine red phosphorus and MMT and their interface properties with polymer matrices were studied in this thesis. The results were characterized by GC, FTIR, XRD, DTA, TG, XPS, UV, SEM, TEM and other physical and chemical methods. The main contents are as following: 1. The study of factors influencing ultrafine red phosphorus's invariability and phosphine liberation indicated red phosphorus undergone oxidation and dismutation reaction in air, and trace ion of iron, copper and nickel fastened water absorption and oxidation, in which the effect of copper ion was the most, while aluminium and zinc ion could slow down red phosphorus'oxidation, and silver ion had the best effect on red phosphorus moisture absorption. Inhibitors such as aluminium hydroxide, magnesium hydroxide, organic phenol and ferrous potassuim cyanide had a good effect on reducing red phosphorus moisture absorption and restraining phosphine liberation.

本文围绕纳微米材料的表面处理及其在高聚物基体中的应用这一主题,系统地研究了超细红磷和蒙脱土两种常见材料的表面特性、表面处理方法及其与高聚物基体的界面特性,通过气相色谱、红外光谱、X射线衍射、差热、热重、X射线光电子能谱仪、紫外光谱、扫描电镜、透射电镜等现代分析仪器以及其它物理、化学方法对实验结果进行了表征和分析,全文主要内容如下: 1、对影响超细红磷安定性的因素以及磷化氢的缓释研究表明:红磷在空气中发生缓慢氧化、歧化反应,微量的铜、铁、镍等金属离子增加了它的吸水和氧化速度,其中铜离子的作用最为明显,而铝、锌等离子减慢了红磷的氧化速度,银离子对减少红磷的吸湿性效果最好。

The effects of fluorination and side-chain identity on supramolecular and thermal behavior were investigated by wide-angle X-ray diffraction, differential scanning calorimetry, and polarized optical microscopy.

的影响和氟化侧链身份和超热行为进行调查广角X-射线衍射,差示扫描量热仪,偏光显微镜。

Using the classical Mie scattering theory and Fraunhofer diffraction theory , a detailed analysis of the differences of the light energy distribution on the multi-element concentric photodetector of a laser particle sizer is given.

本文用Mie散射理论和Fraunhofer衍射理论分别讨论了颗粒散射在激光测粒仪同心多环光电探测器上的能量分布,详细计算并比较了两者之间的差别,指出。。。

The oxide films were investigated by means of scanning electron microcopy, energy dispersion X-ray microanalyser, X-ray diffraction and X-ray photoelectron spectroscopy.

用扫描电镜、能谱仪、X封线衍射、X射线光电子能谱时氧化膜进行了研究。

These polymers exhibit typical fibrillar morphology in the films. During heating in DSC, all the polymers substituted with alkoxy on phenylene show a nematic phase.

三、通过X-射线衍射、示差扫描量热仪和形貌表征等手段研究了苯环上取代基烷基、烷氧基长度对聚合物形貌、相转变过程等的影响。

The institute equipped with 760 sets of all classes of large-scale apparatus, which included computer workstation, large format scanners,large format graphic plotter, X-ray Fluorescence Spectrometer, Inductively Coupled Plasma Atomic Emission Spectrometer, Atomic?Absorption?Spectrometry, powder X-ray diffraction, One-meter Plane-grating Spectrograph, Oscillographic Polarograph, ScanningElectron Microscope, Infrared Spectrometer, Electronic Precision Balance, Sspectrophotometer, semi-industrial ferromagnetic separator,semi-industrial scrubbing machine, semi-industrial continuous dense-medium separation apparatus; semi-industrial continuous gravityconcentrating table equipment and etc.

拥有计算机工作站、大幅面工程扫描仪、大幅面绘图仪、X荧光光谱仪等离子体时序式光电直读光谱仪、原子吸收分光光度计、粉晶X衍射、一米光栅摄谱仪、示波极谱仪、扫描电子显微镜、红外光谱仪、精密电子天平、分光光度计、半工业型强磁选机、半工业型擦洗、半工业型重介质、半工业型重选摇床等设备760 多台。

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