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衍射仪

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The changes in phase structure and Curie temperature of the Sm2Fe17 compound after nitrogen absorption were studied by using X-ray diffraction, differential thermal/thermo-gravimetric analyzer and magnetic measurement. The results of X-ray diffraction showed that the diffraction peaks of the Sm2Fe17 compound shifted toward lower angle after nitrogen absorption, and the characteristic peaks of α-Fe were observed. This showed that the unit cell of Sm2Fe17 expanded, the compound was decomposed to a certain extent and the characteristic peaks of α-Fe appeared.

通过X-射线衍射、差热-热重联用仪以及磁测量等手段,研究了Sm2Fe17化合物吸氮后的相结构及居里温度的变化行为。X-射线衍射表明,吸氮后Sm2Fe17化合物的衍射峰向小角度方向偏移,并且出现了α-Fe的衍射峰,这说明吸氮后化合物的晶胞有所膨胀,并且化合物有一定的分解,产生了α-Fe。

In order to improve performance of uncooled thermal imager, diffractive optical elements are applied in high relative aperture IR lenses.

将衍射光学元件应用于非制冷热像仪的大相对孔径红外镜头与传统设计相比,衍射光学元件的引入,增强了此类镜头的色差校正能力,提高了镜头的成像质量,提高了镜头的透过率,减少了光学零件的数量,减轻了系统重量,为提高非制冷热像仪的性能奠定了坚实基础。

We are also distributor of the following companies:Pfeiffer Vacuum-turbo molecular pump, other types of pumps, gauges, Helium leak detector, mass spectrometer; Maxtek, Inc-Quartz crystal thin film deposition controller and sensors; Telemark Inc-E-beam source and power supply, optical thin film monitor; Comdel, Inc-DC and RF power supply; Angstrom Sciences-Magnetron target and materials; Oxford Scientific Limited-Atom sources; Plasma Quest Ltd-Plasma systems for coating and etching; Sentech Instruments GmbH-Ellipsometers.

我们代理的产品包括德国普发真空的全线真空产品(分子泵等各种真空泵,真空计,检漏仪,质谱仪,各种真空零部件);美国美泰克公司的石英晶体膜厚监测仪,传感器;美国泰利玛科公司的电子枪和光学膜厚控制仪等;美国康戴尔公司的射频,中频和直流电源;英国牛津科学公司的微波等离子体源,电子束蒸发源,原子源,高能电子衍射枪;英国PQL公司等离子体溅射镀膜设备,美国安斯超科学公司的磁控溅射阴极及溅射靶材,德国森泰科仪器公司的椭偏膜厚测量仪和等离子刻蚀沉积设备等。

EDS and Surface-profile results indicate that the stoichiometries of all the samples approach 2:3 and the thicknesses are over 500nm. XRD results indicate that the major diffraction peaks of the film match those of Bi2Te3.The film growth exhibits preferred orientation at (015) phase and many Bi, impurity peaks are observed. Hall and Seebeck coefficient measurement reveals that all the samples are n-type with the carrier density of 10^23cm^-3 and conductivity of 10^-5Sm^-1 which confirm the samples have nice thermoelectrically properties.

能谱分析和台阶仪测量结果显示本文所制备的薄膜Bi:Te原子比接近2:3,厚度都大于500nm;XRD测量结果显示薄膜的主要衍射峰与Bi2Te3标准衍射峰相同,在(015)晶面上择优选向明显,有少量的Bi、杂质峰存在;霍尔系数测试及Seebeck系数测量结果显示,薄膜都为n型半导体薄膜,载流子浓度量级为10^23cm^-3,电导率量级10^-5Sm^-1,具有良好的电学性能。

Their properties of homopolymer and copolymers have been studies by DSC, polarizing hot stage microscope and X -ray techniques.

用DSC热台偏光显微镜和X射线衍射仪等对合成的均聚物和共聚物进行了表征。

A kind of imitated chicken-blood stone is studied by XRF,XRD,FTIR and polarizing microscope in this paper.

利用X射线荧光光谱仪、X射线衍射仪、红外光谱以及偏光显微镜等实验技术对近期市场上一种常见的仿鸡血石的矿物组成、内部结构等特征进行了研究,对其宝石学性质进行了测定。

The phase composition and microstructure of sintered materials were inv...

采用X射线衍射仪和扫描电镜研究了合成产物的相组成和显微结构。

The hollow Ni2 microspheres were prepared via the hydrothermal reaction of NiCl2 with aqueous ammonia at 140 ℃ for 12 h.

采用X射线衍射仪、扫描电镜和透射电子显微镜对产物进行表征,并在室温下测试了它的磁学性能,结果表明, Ni2空心微球的直径约为3~4 μm,它是由尺寸1.1~1.3 μm左右的六方相结构的Ni2纳米片组装而成; NiO空心微球是由立方相纳米片和多孔纳米片组装而成,它具有弱的铁磁性,其矫顽力为583 Oe,剩余磁化强度为0.213 emu/g。

Their surface morphology and phase were analyzed by SEM and XRD.

用扫描电镜和X射线衍射仪对涂层表面形貌和物相进行了分析。

In order to disclosure the reason why the electrocatalysis activeness and selectivity droped after being used several hundred hours continuously, the x-ray diffraction, scanning electron microscopy and energy dispersive spectroscope have been used to characterize the surface condition variations of Monel metal. The results indicated: Monel metal belongs to the Cu-Ni alloy around the electrolysis experiment.And after being used for 600hr, the surface layer element composition and geometry distribution of the alloy changed, namely in the alloy the Cu element /which superficial free enthalpy was smaller,"concentrated" to the alloy surface,and formed one kind of marble structure microcrystallite.Thus the electrode surface becamed rough a

为了揭示蒙乃尔合金阴极在连续使用数百个小时后电催化活性剂选择性下降的原因,采用X射线衍射仪、电子扫描电镜和电子能谱分析仪对电解实验所用的蒙乃尔阴极材料在电解实验前后的表面状态进行了表征,结果表明:所使用的蒙乃尔合金阴极材料在电解实验前后均属于Cu-Ni合金,使用600hr后,由于表面层元素组成和几何排布发生了变化,即合金中表面自由焓较小的Cu元素向合金表面&富集&,形成一种大理石结构的微晶,表面粗糙、不均一,这是造成其对硝基苯电还原的催化活性及选择性随着使用时间延长而逐渐下降的主要原因,同时也为此类电极的修饰改进提供了方向。

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