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衍射仪

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In-situ synthesis process was used to prepare copper nanoparticles and coppernanoparticles-polyethylene glycol oil solution by reduction of copper acetate by glycol in polyethylene glycol containing amido ligand as dispersant.

采用原位合成法以聚乙二醇400作为反应介质,以氢氧化钠和氨基配体作为分散剂,用乙二醇还原六水合乙酸铜制备出纳米Cu粉和纳米Cu聚乙二醇溶液,用X射线衍射仪和透射电子显微镜表征其结构,在四球摩擦磨损试验机上评价了含不同质量分数纳米铜粉的聚乙二醇溶液的摩擦磨损性能,并与分散剂进行对比。

AlPO4 was synthesized by a Sol-Gel method. Its coefficient of thermal expansion was measured by dilatometer. Its corrosion behavior was tested in an environment of 50vol%H2O/50vol%O2 with a flow rate of 0.085cm/s at 1350℃. The phases and composition of the samples were analyzed by X-ray diffraction and Energy Dispersive Spectroscope. The microstructures of AlPO4 were characterized by Scanning Electron Microscope.

采用溶胶凝胶法合成了一种AlPO4环境障碍涂层材料,测定了其热膨胀系数,在1350℃、50vol% H2O/50vol%O2、1.013×105 Pa、气体流速0.085cm/s的水氧耦合环境中研究了其抗水氧腐蚀性能,并利用X射线衍射仪、能谱分析仪和扫描电子显微镜分析了材料组成和微观结构。

By means of modern analysis and testing tools such as X-ray diffraction and flurescence spectrum research the crystal constitution and luminescence performance of materials.

结合X射线衍射仪、荧光分光光度计等现代分析测试手段,研究了其晶体结构和发光性能。

Guangzhou 510650, P.R.China)Abstract: A new type of photoelectrode was innovated by anodising titanium mesh in H2SO4 solution and named Ti/TiO2 mesh electrode.

摘 要:采用电解氧化金属钛网的方法制备新型光电极Ti/TiO2,采用X射线衍射仪、激光拉曼光谱仪与扫描电镜测试电极的表面晶体结构与表面形态。

The strength development of the system is also studied.The result shows that the strength of the minerals is obviously higher than calcium sulphoaluminate and the optimum composition is found.In addition,we have analysed the formation and hydration mechanism of the clinkers by means of XRD,IR,SEM,DTA and so on.

发现该系列部分矿物的强度明显高于硫铝酸钙,并找到了最佳矿物组成点﹔应用X射线衍射仪、红外光谱仪、扫描电子显微镜和差热分析等测试手段,对熟料矿物的形成和水化机理进行了初步分析研究。

To study high temperature corrosion behavior on materials during solid waste incineration, laboratory corrosion tests were performed to iron, cast iron, 20# carbon steel, stainless steel in oxidizing gaseous environments which included O〓, SO〓, H〓O, HCl, Cl〓and some ashes coming from self-designed incinerator, the Xunde's one and synthetic ashes. The synthetic ashes are used as corrodents composed of chlorides , sulfates and oxides.

最后,本论文为揭示材料垃圾焚烧过程中的高温腐蚀行为,借助于腐蚀重量实验,X-射线衍射仪,扫描电子显微镜,电子能谱等分析测试手段,研究了铁、铸铁、20#碳钢和不锈钢在垃圾焚烧环境中的高温腐蚀行为及腐蚀动力学。

The morphology and structure of the dendrite-like copper crystals with micrometer size and face-centered cubic structure were characterized by using scanning electron microscopy and X-ray diffraction.

用扫描电子显微镜和X射线衍射仪对枝晶铜进行了形貌和物质结构的表征;制得的枝晶铜尺寸达到微米级,为面心立方晶相。

The disordered solid solution Al was obtained for Fe_(25)Al_(65)Ni_(10) mixture powder. The mechanical alloying of Fe_(0.25)Al_(0.75-x)Ni_x(x=0.05,0.175,0.25) mixture powders result in intermetallic compounds. The results of mechanical alloyed_(1-x)Ni_x (x=0.4,0.6) and (FeAl_3)_(1-x)Ni_x(x=0.1,0.3) mixture powders indicate that the ratio of iron and aluminum determines the formation of intermetallic compounds. The FeNi intermetallic compound, cerium oxide and one unidentified phase were obtained by mechanical alloying FeCeNi_3 and Ce_2 mixture powders.

对于合金化过程中的结构演变采用X射线衍射仪、DTA或DSC热分析仪、SEM进行分析,对Al-Fe-Ni和Ce-Fe-Ni两个三元系的机械合金化过程的研究表明:对于Al-Fe-Ni三元系来说,成分为Fe_(25)Al_(65)Ni_(10)的混合粉末经机械合金化后可生成非晶与纳米晶的混合物;球磨成分为Fe_(0.25)Al_(0.75-x)Ni_x(x=0.05,0.175,0.25)混合粉末,可形成Al_3Ni_2,AlFe_3,AlFe_(0.23)Ni_(0.77),球磨成分为_(1-x)Ni_x(x=0.4,0.6)和(FeAl_3)_(1-x)Ni_x(x=0.1,0.3)混合粉末,Fe与Al比例相同时球磨所形成的金属间化合物也相同。

The effects of La-Pr-Ce mischmetal on the microstructure and mechanical properties of the testing cast Mg-7Li-1Al alloys have been investigated by means of mechanical property measurement,optical microscopy,scanning electron microscopy and X-ray diffractometer.Influence of the aging treatment on microstructure and mechanical properties of the test Mg-7Li-1Al-xLPC alloys have-been studied.Similarly,heat treatment strengthening mechanism of cast Mg-7Li-1Al-xLPC alloy and strengthening mechanism of La-Pr-Ce mischmetal cast Mg-7Li-1Al has also been discussed in depth.

通过进行力学性能测试试验,并采用光学显微镜、扫描电镜、X射线衍射仪等现代材料分析测试手段,研究镧镨铈混合稀土对Mg-7Li-1Al合金组织和性能的影响;分析时效处理对Mg-7Li-1Al-xLPC合金组织和力学性能的影响程度;并且探讨了镧镨铈混合稀土对Mg-7Li-1Al合金以及时效处理对Mg-7Li-1Al-xLPC的强化机理。

High-resolved X-ray diffraction measurements show that the crystal quality of high aluminum mole fraction(x=0.1) is poor and it may cause a large dark current. The window layer acts as a band-choice role. It induces a high responsivity and a wide response band for a higher aluminum mole fraction.

高分辨率X射线衍射仪对材料的测试结果表明,高铝组分(0.1)窗口层薄膜材料的晶体质量较差,导致暗电流增大,而其窗口层的窗口选择作用则可以得到较高的响应率和较宽的响应波段。

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然而,正如其名字所指出的那样,CD盘不能写,也不能用任何方式改变其内容。

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