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Objective To optimize the extraction process by determing the volatile oil yield of steam distillation and supercritical CO2 extraction from flowers of Elaeagnus angustifolia L..

目的 比较水蒸气蒸馏法和超临界CO2萃取技术从沙枣花中提取挥发油的得率,确定最佳提取工艺。

ConclusionThe extraction rate of volatile oils from Heracleum hemsleyanum Diels by supercritical CO2extraction process is higher than that of water vapor distillation,and the optimized extraction conditions are:extraction pressure 25MPa,extraction temperature 45℃ and flow rate of CO2 20L/h, and the yield of volatile oils is 0.65%.

结果通过各因素级差大小的比较可知:萃取压力的变化对萃取率的影响最大,萃取温度次之,而CO2流量对萃取率的影响最小。结论超临界CO2萃取牛尾独活挥发油的萃取率较水蒸气蒸馏法高,最佳萃取条件为萃取压力25MPa,萃取温度45℃,CO2流量20L/h,挥发油收率为0.65%。

ConclusionMicrowave extraction has the highest yield in the shortest time. But volatile oil in Heracleum hemsleyanum Diels extracted by supercritical CO2 extraction or steam distillation has better quality.

结论微波萃取挥发油得率最高,时间最短;超临界CO2和水蒸馏法萃取挥发油的质量最好,因此使用超临界CO2是萃取牛尾独活挥发油的最佳途径。

ConclusionThe extraction rate of volatile oils from Heracleum hemsleyanum Diels by supercritical CO2extraction process is higher than that of water vapor distillation,and the optimized extraction conditions are:extraction pressure 25MPa,extraction temperature 45℃ and flow rate of CO2 20L/h, and the yield of volatile oils is 0.65%.

超临界CO2萃取牛尾独活挥发油的萃取率较水蒸气蒸馏法高,最佳萃取条件为萃取压力25MPa,萃取温度45℃,CO2流量20L/h,挥发油收率为0.65%。

ConclusionMicrowave extraction has the highest yield in the shortest time. But volatile oil in Heracleum hemsleyanum Diels extracted by supercritical CO2 extraction or steam distillation has better quality. Thus the supercritical CO2 extraction is the best way.

结论微波萃取挥发油得率最高,时间最短;超临界CO2和水蒸馏法萃取挥发油的质量最好,因此使用超临界CO2是萃取牛尾独活挥发油的最佳途径。

F. based on gas chromatography-mass spectrometer method. Essential oil from cultivated variety Inula racemosa Hook. f. was extracted by steam distillation and analyzed by applying GC-MS.

方法]采用水蒸气蒸馏法从藏木香栽培品种中提取挥发油,并用GC-MS联用仪对其挥发油的化学成分进行研究。

This experiment extract essential oil of ledum palustre by distilling with steam.

采用水蒸馏法提取杜香挥发油,制备了杜香祛斑霜。

Results In Vero cell system,under lucifugal and illumination conditions,fullerene C60 has direct virucidal activity and infection block effect,but it does not has any multiplication inhibition action to HSV-1F strain.

以逆相蒸馏法合成了富勒烯脂质体,用药物对病毒所致细胞病变的抑制实验以及病毒的空斑减数实验,观察C60脂质体对HSV-1F株的直接杀灭、感染阻断及增殖抑制作用。

METHODS The volatile oil was obtained from Mallotus apelta by steam distillation.

方法采用水蒸气蒸馏法提取白背叶中的挥发油。

Coumarin in melilotus was extracted in the method of steam distillation, and the content of coumarin in product was less than 2% and plentiful tar as the by-product was found at the same time.

采用水蒸气蒸馏法对草木樨中的香豆素进行提取,其提取物中香豆素的含量不到2%,并伴有大量的焦油产生。

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