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This paper established a method of analysis of taurine by spectrophotometry and discussed the factors that affected spectrophotometry.

本文研究了毛细管电泳测定牛磺酸的方法,采用萘-2,3-二甲醛和牛磺酸反应,衍尘为电化学活性的物质,进行电泳测定,并对衍生反应条件和电泳分析条件进行了优化,建立了一种测定牛磺酸的新方法。

It was found that sulfuric acid, 2-naphthalenesulphonic acid and sulfurous acid could be effectively separated by competitive exchange adsorption in views of action force difference of the components with the resin. The exchange adsorption dynamic diffusion parameters were calculated with diffusion equation for solids and liquid films, and the rate-determining step was determined. The model of breakthrough curve for the resin bed was suggested, and applied to simulate the breakthrough process for each component.

通过单组分、双组分和多组分平衡数据的测定,发现对于硫酸-萘磺酸-亚硫酸混合体系,可以利用不同组分与树脂作用能的不同,通过竞争交换吸附实现分离;以固相扩散方程和液膜扩散方程对交换吸附动力学参数进行了估算,确定了交换吸附过程的控制步骤;建立了床层穿透曲线模型,并对各组分穿透过程进行了模拟。

Products: 3 - benzoyl-ethyl acrylate (97% min), acyl phosphorus acid methyl ester (98% min), P acyl three ethyl acetate (98% min), a phosphorus acid acyl The ethyl esters (98% min), 3 - bromine -1,3,4,5 - tetrahydrocannabinol -2 H-1-benzo-Aza Zhuo -2, 1 - naphthalene-tetrahydrocannabinol (98% min), 3,5 - dimethyl benzoyl chloride (99% min), 3,5 - dichloro benzoyl chloride (97% min), the ethyl benzoyl chloride (99% min), a TCA Ester (99.5% min), o-benzoyl methyl benzene (99% min), 4 - phenyl benzophenone (99% min): glacial acetic acid (99% min), methanol (99% min), liquid chlorine (99.5% min), caustic soda (30% min), isopropyl alcohol (99% min), anthranilic acid (99% min), dichloroethane (99% min ), Chunben (99% min), toluene 99% min

3-苯甲酰基丙烯酸乙酯(97%min)、磷酰基乙酸三甲酯(98%min)、磷酰基乙酸三乙酯(98%min)、磷酰基乙酸甲酯二乙酯(98%min)、3-溴-1,3,4,5-四氢-2H-1-苯并氮杂卓-2酮、1-四氢萘酮(98%min)、3,5-二甲基苯甲酰氯(99%min)、3,5-二氯苯甲酰氯(97%min)、对乙基苯甲酰氯(99%min)、氯乙酸甲酯(99.5%min)、邻苯甲酰基苯甲酸甲酯(99%min)、4-苯基二苯甲酮

In this dissertation, firstly, the conditions of isolation and purification of specific toxin fractions produced by Exserohilum turcicum has been studied, and a high-efficient method has been established;secondly, the toxins were analysed by UV-Vis spectrophotometry;then the effect of specific toxin on death rate of corn leaves protoplast was studied by FDA as a tinct reagent;finally, using ANS as a probe and SDS-PAGE to study the membrane protein of the corn leaves with Htl gene. In a word, the aim of the research is to search some existent evidences of the toxin binding site on protoplasmic membrane, and provide proofs for nosogenesis of specific toxin in terms of cytology and the molecular biology.

本研究对玉米大斑病菌1号小种毒素的特异性组分进行分离,建立了高效的特异性毒素分离纯化方法,并对其进行了紫外波谱分析;用荧光素双醋酸酯染色法,测定了毒素特异性组分对原生质体死亡率的影响;进而用1-苯胺基-8-萘磺酸荧光探针标记法和SDS-PAGE电泳法对特异性毒素组分与Htl基因玉米细胞互作过程中的质膜蛋白进行了研究,旨在证明Htl基因玉米细胞质膜上存在特异性毒素组分结合蛋白,为从细胞和分子生物学角度阐明毒素的致病机理提供证据。

The chemical plant of it ,which has more than 20 years history of triphenyl phosphate production and with capacity of 4,000 tons/year,is our fine chemical production base and the biggest professional TPP plant.It is also the only one of refine naphthalene producer in Hebei Province with yields of 10,000 tons/years,Our group has sufficient raw material supply for its own production.

其中,化工厂作为精细化工生产基地,生产磷酸三苯酯已有20余年历史,其规模为4000吨/年,目前在国内属于最大专业生产厂,精萘是河北省唯一生产厂家,现生产规模10000吨/年,并有充足的自备原料。

A series of indexes reflecting free radical changes, anti-oxidations, Immune function, endocrine function was studied by Chemiluminescence method, immunoturbidimetry, ANAE dye method, micro-hemagglutination inhibition test and radio immunoassay in the chicken with encephalomalicia induced by giving the feed being deficient in VE and extra fish oil artificially. The pathological changes including microscopic and ultramicroscopic changes in the relative organs and tissues were observed.

本实验以一日龄150只海兰兰蛋鸡为实验动物,用低维生素E且添加鱼油日粮饲喂雏鸡,复制脑软化症动物模型,采用化学发光法、免疫浊度测定法、酸性α-醋酸萘脂酶染色法、微量血凝抑制试验、放射免疫测定技术等方法系统地检测了脑软化雏鸡的自由基代谢和抗氧化功能、红细胞免疫功能、细胞免疫功能、体液免疫功能及非特异性免疫功能等指标,并对患雏病理组织进行了显微及超微结构观察。

A series of selective acylation of 1'-OH dl-shikonin derivatives and structure simplified derivatives were synthesized.

我们设计并合成了一些消旋紫草素1'位羟基的酯衍生物和结构简化的紫草素萘醌类似物。

ABSTRACT OBJECTIVE: To study the antiasthmatic effect of domestic salmeterolin comparison with sulbutamol.

目的:考察羟萘甲酸沙美特罗的平喘作用,并与硫酸沙丁胺醇进行比较。

In the same time, a number of barbituric acid derivatives have been designed. The relations of structure-properties was studied by connecting anthraquinone, benzene and furan.

并以1H-NMR,FTIR,UV-vis,Mass进行了表征,确定了其结构,另外设计了几种巴比妥酸衍生物分子,通过在巴比妥酸衍生物中引入萘、苯以及芳香杂环等不同的共轭桥,研究了结构性能关系。

The method is based on a diazotion-coupling reaction between benzidine and hydrochloric acid naphthyl ethylenediamine in a hydrochloric acid medium.

在酸性条件下,亚硝酸盐与联苯胺重氮化,再与盐酸萘乙二胺偶联生成蓝色产物,该产物在578 nm处有最大吸收值,并由此建立了一种简单、快速、灵敏的亚硝酸盐测定方法。

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Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书,王祥生,李德昌。安徽省首次发现嗜群血蜱。

Chapter Three: Type classification of DE structure in Sino-Tibetan languages.

第三章汉藏语&的&字结构的类型划分。