萃取的

Methods:Supercritical CO2 extraction was used with absolute alcohol as entrainer,and the L9(33)orthogonal experiment was designed,and the effects of extraction pressure,temperature and material-entrainer ratio on the extraction rate were investigated.

以无水乙醇做夹带剂，采用超临界CO2萃取法，并设计L9(33)正交实验，考察萃取压力、萃取温度和物料与夹带剂的料液比对萃取率的影响。

Methods The nereistoxin toxins were extraceted with ethyl acetate∶cyclohenane(1∶1),cleaned by the aluminite powder online and then by auto gel permeation chromatography.

方法取一定量的Al2O3放入萃取池中做吸附剂，通过快速溶剂萃取仪萃取血液中杀参毒素类农药，同时达到在线净化的效果，后运用凝胶色谱净化联用仪进一步净化浓缩到2ml，提取液经LC/MS/MS进行检验。

Acidic extraction method was used to condensate butyraldehyde and get high concentration organic wastewater,and the influences of pH value,temperature, extracting agent and its amount on extracting effect were also discussed.

利用酸化萃取法处理丁醛缩合高浓度有机废水的思路，探讨了不同废水pH值、温度、萃取剂及萃取剂用量对萃取效果的影响。

Optimum extraction conditions were selected by the condition experiments and the concentration of Cu, Pb, Zn in main components were also determined for revealing the distribution of the heavy metals in the suspended particulate matters. It was found that hydroxylamine hydrochloride (0.006 mol/L NH2OH·HCl+0.01 mol/L HNO3) can remove most of Mn oxides, and sodium dithionite 0.8 mol/L Na2S2O4

结果表明，0.006 mol/L NH2OH·HCl+0.01 mol/L HNO3萃取30 min可以单独萃取悬浮颗粒物中大部分的锰氧化物，0.8 mol/L Na2S2O4（pH=6.0）萃取40 min可以同时萃取铁、锰氧化物，而对非目的组分的影响较小；悬浮颗粒物对Cu、Pb、Zn重金属有明显的富集作用，其中Cu主要结合在悬浮颗粒物的有机质组分中，Pb主要富集在铁、锰氧化物中，锰氧化物和有机质对Zn的分布起主要的富集作用。

For lanthanides in Am at pH 2. 7～2. 8. According to empirical distribution ratio model and proposed calculation method, flow sheets are proposed for the separation of Am and fission product lanthanides from power reactor and production reactor waste respectively.

7级萃取、3级洗涤2级反萃的多级逆流分馏萃取实验表明HBTMPDTP-TBP-煤油能够很好地萃取分离镅和镧系元素，在pH值为2.7～2.8时，镧系元素中镅的分离系数大于5×10〓，镅中镧系元素的分离系数大于2.5×10〓。

The conclusions were as follows: theνO-H andνC=O IR absorption maxima shifted towards higher wave numbers after imprinting 17β-estradiol on TFMAA-co-TRIM copolymer with the red shift of theνO-H groups being apparent after precipitation polymerization for 16h while that forνC=O groups being observed after polymerization for 24h. A strong interaction between TFMAA and 17β-estradiol was confirmed by the high selectivity for 17β-estradiol, as indicted by the values of the separation factor of isomers of 17β-estradiol/17α-estradiol (2.28) and the imprinted factor (3.01). Particle diameter of TFMAA-co-TRIM polymer was between 300 nm and 1.5μm, which suited well for solid phase sorbent throughout at low column pressure. The recognition of imprinting TFMAA-co-TRIM polymer for sterol molecules was driven by enthalpy eluted with acetronitile, and low temperature was in favor of the separation of sterol structure analogues on imprinting column. TFMAA-co-TRIM polymer possessed of determinate anti-heat stability, with melting point beginning at 255.84℃, Tp=257.40℃, control TFMAA-co-TRIM polymer and imprinting TFMAA-co-TRIM polymer were respectively decompounded at 267.79℃and 343.11℃, and solid micro-extraction noddle prepared by the special polymerization also showed definite recognition for 17β-estradiol by GC/MS detecting at 270℃. By selection of various washing and elution solvents, elution reagents of close polymerization system were of more advantage in template molecules retention and recognition on molecularly imprinted solid phase extraction column. At a certain extent, progesterone, 17α-estradiol, 17β-estradiol and 4-androstene-3, 17-dione could be intercepted on the MISPE column. Especially, MISPE had high selectivity for progesterone, and imprinting TFMAA-co-TRIM polymer could achieve adsorption balance within 50 min by absorption kinetics test for 17β-estradiol. However, MISPE column showed better selectivity and enrichment property for 17β-estradiol than C18 and CSPE columns according to the data from HPLC and GC/MS analyses. Recovery of 17β-estradiol on MISPE column was up to 85.5% while when prime extracting solution of milk powder was sampled, the recovery of CSPE and C18 columns were 43.7% and 30.7%, respectively.

通过研究阐明：紫外聚合产物TFMAA-co-TRIM中的νO-H振动吸收峰在聚合16h后红移，νC=O振动吸收峰在聚合24h后红移；TFMAA-co-TRIM对雌二醇异构体的印迹因子达到了3.01，α为2.28，优于其它功能单体参与得到的聚合物识别特性；TFMAA-co-TRIM聚合物粒径介于300 nm至1.5μm之间，作为色谱固定相具有良好的通量和低的柱压；在乙腈流动相中，TFMAA-co-TRIM分子印迹固定相的分离过程主要被焓驱动，低温有利于分子印迹固定相分离甾醇结构类似物；TFMAA-co-TRIM分子印迹聚合物在255.84℃时开始熔融，Tp=257.40℃，聚合物CP的降解温度在267.79℃，MIP降解温度在343.11℃，制备的固相微萃取头初步经GC/MS 270℃的耐热性测定；不同的洗提溶剂筛选证明了选择接近聚合溶剂的洗脱体系更有利于MISPE发挥识别效应；分子印迹固相萃取柱对孕酮、17α-雌二醇、17β-雌二醇和雄烯二酮都具有不同程度的保留特性，可作为此类化合物的吸附材料，特别对孕酮强保留的富集特性，可作为孕酮的选择性识别吸附剂，其分子印迹聚合物对17β-雌二醇的吸附动力学测定显示在50 min内基本达到吸附平衡，具有作为传感器核心敏感材料的潜力；对比萃取奶粉中17β-雌二醇性能，MISPE柱比非分子印迹固相萃取柱和C18柱具有更高的保留，回收率依次为85.5%，43.7%和30.7%。

The mechanism of synergistic extraction was discussed, and the stoichiometry of the extracted complexes was determined.

探讨了CA-100与-盐基磷酸类萃取剂对锌和镉的协同萃取，研究了协同萃取机理，确定了协萃配合物的组成。

Using kerosene and 40%n octanol as diluents,some lanthanide and actinide can be extracted effectively by amido podand from nitric acid solutions.

以酰胺荚醚为萃取剂，正辛醇和煤油的混合物作稀释剂，研究了水相硝酸浓度和不同结构酰胺荚醚对镧系和锕系元素萃取分配比的影响，并对它们的萃取性能进行了比较，结果表明，适当的酰胺荚醚可以有效地从硝酸溶液中萃取镧系和锕系元

Effects of different extraction modes, extraction time, pressure and temperature on the extraction yield of onion essential oil and sulphur concentration were investigated,and the different extraction solvents and extraction times were researched in liquid-liquid extraction procedure. The optimal conditions of extraction of onion essential oil with subcritical water were static extraction, 100~150℃sequential program temperature increasing extraction for 30min, 5MPa, petroleum ether as extraction solvent for two times.

考察了提取方式、提取时间、温度、压力对洋葱精油的提取得率及含硫化合物浓度的影响，并对液液萃取中溶剂的种类和萃取次数进行了研究，得到了洋葱精油的亚临界水提取最佳工艺：静态提取、提取时间30 min，压力5 MPa，100～150 ℃的连续程序升温，石油醚为萃取溶剂，萃取2次。

But when the pressure is bigger than 30MPa, there is a contrary phenomenon. The flow rate, particle size distribution and void fraction of the extraction bed have the complicated effect. 3Based on the broken-intact cells model, a dynamic model based on differential mass balance equation is developed according to the law of conservation mass. The expression of mass transfer flux is given by the analysis the process and the necessary hypotheses. The extraction process is described, and the expression of extraction rate of diosgenin is given.

3在引入破碎—完整细胞结构理论的基础上，根据质量守恒原理建立了基于微分质量守恒方程的动力学模型，通过对萃取过程的分析和必要的简化、假设，给出了不同阶段传质通量的表达式，在此基础上描述了萃取过程，并给出了超临界流体萃取薯蓣皂甙元的萃取收率表达式。

As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸，那乌黑、忧郁的眼睛，她便会相信，他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失