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Methods:Supercritical CO2 extraction was used with absolute alcohol as entrainer,and the L9(33)orthogonal experiment was designed,and the effects of extraction pressure,temperature and material-entrainer ratio on the extraction rate were investigated.

以无水乙醇做夹带剂,采用超临界CO2萃取法,并设计L9(33)正交实验,考察萃取压力、萃取温度和物料与夹带剂的料液比对萃取率的影响。

The results showed that the significance of the effects of these factors on the oil extraction efficiency decreaseed in the order:extraction pressure, time, temperature and entrainer dosage, and the maximum extraction efficiency of watermelon seed oil could reach 52.18% under the extraction pressure of 40 MPa, temperature of 45℃, time of 150 min and the ethanol dosage of 7%.

结果表明,影响西瓜籽油萃取率的因素主次顺序为:萃取压力>萃取时间>萃取温度>夹带剂用量;最佳提取条件为萃取压力40 MPa,萃取温度45℃,萃取时间150 min,夹带剂乙醇用量7%。在最佳条件下西瓜籽油萃取率为52.18%。

The diluent solution of glyoxylic acid and oxalic acid was used as the separation object.TOA (in n-octanol) was used as the solvent. The extraction characteristics of single acid and two-acid solution were studied,and the influence of pH and the concentration of complexing agent on the distribution coefficients were measured. The suitable mathematic models were proposed to describe the relationship between TOA and carboxylic acid based on assumed extraction reaction in organic phase.

摘 要:以草酸和乙醛酸的稀溶液为分离对象,采用三辛胺为萃取反应剂、正辛醇为稀释剂,研究了单溶质、双溶质有机酸的萃取分离特性,测定了溶液pH值、萃取反应剂的浓度等因素对双溶质有机酸萃取的影响,提出了萃取的化学反应发生在有机相中的假定,建立了TOA萃取草酸的数学模型。

The diluent solution of glyoxylic acid and oxalic acid was used as the separation object. TOA (in n-octanol) was used as the solvent. The extraction characteristics of single acid and two-acid solution were studied, and the influence of pH arid the concentration of complexing agent on the distribution coefficients were measured. The suitable mathematic models were proposed to describe the relationship between TOA and carboxylic acid based on assumed extraction reaction in organic phase.

以草酸和乙醛酸的稀溶液为分离对象,采用三辛胺为萃取反应剂、正辛醇为稀释剂,研究了单溶质、双溶质有机酸的萃取分离特性,测定了溶液pH值、萃取反应剂的浓度等因素对双溶质有机酸萃取的影响,提出了萃取的化学反应发生在有机相中的假定,建立了TOA萃取草酸的数学模型。

The extract of the culture filtrate of Mh5 was compared with the standards of ephedrine and pseudoephedrine by TLC scan in UV and visible spectrum.

对麻黄生物碱提取方法进行了选择和优化,得出在工业提取法的框架下,用氯仿作为萃取剂在40℃左右进行提取的效果最好。

With the extraction efficiency of rotenone and total substance obtained as estimated index, the technology conditions of extracting rotenone from the leaves of Tephrosia vogelii were investigated by SFE-HPLC method.

采用超临界流体萃取反相高效液相色谱法,以鱼藤酮萃取率和萃取产物总得率为评价指标,研究提出非洲山毛豆 Tephrosia vogelii Hook.f中鱼藤酮的超临界流体萃取较优工艺条件为:萃取物料粒径30目,静态萃取20min,萃取温度45℃,压力27.58MPa,流体总流量30mL/g,萃取前向萃取池中加入3mL甲醇作夹带剂。

Temperature and 30 mL CO:. Under this condition, the highest ratio of rotenone can meet 0.359% counted with engineering calculation. For total compounds extraction. 6000psi. 70癈. 40mL and the ratio is 10.06%. For rotenone content in total compounds. 3000psi. 35 癈. lOmL and the high content percent is 7.59%. So when conducting SC-CO: extraction of Tephrosia vogelii.

非洲山毛豆的SC-CO_2萃取应根据萃取目的选用相应的工艺条件SC-CO_2萃取非洲山毛豆生产杀虫剂,应选用压力5000psi,温度45℃,流量30mL的工艺条件;(5)通过夹带剂对萃取效果的影响研究,结果表明加入夹带剂可显著影响非洲山毛豆的SC-CO_2萃取效果。

Thirdly, the mechanism of extractant and diluent loss in aqueous phase was studied in both saponified organophosphorus acids and naphthenic acid extraction systems.

本文通过研究皂化有机磷酸、环烷酸从有机相到水相的转移及水相中胶团或o/w型微乳状液的形成,证明了皂化酸性萃取剂和有机溶剂的水相流失与水相聚集体的形成有关。

By the methods of direct viable count and plate count, this paper studied the effects of different selective extractants on the bacteria, algae and protozoan on the biomembrane in natural water body.

用平板计数法、显微镜直接计数法及培养法分别研究了选择性萃取剂对自然水体生物膜上细菌、原生动物和藻类的影响。

To review the theory and research situation of sub-critical water as HPLC mobile phase and extraction eluents,illustrate its ap-plication in pharmacy and analytical chemistry.

本文简述亚临界水作为高效液相色谱流动相及萃取剂的理论基础及其在药学及分析化学中应用研究的情况。

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