萃取

Optimal extraction pressure, extraction temperature, CO2 flow rate, extraction time and dosage of entrainer per gram of tobacco powder were 24 MPa, 55℃, 3.8 Lh^(-1), 3 h, 6 mL, respectively.

优化后的萃取工艺条件为：萃取压力24 MPa、萃取温度55℃、CO2流速3.8 Lh^(-1)、萃取时间3 h、每克烟末夹带剂用量为6 mL。

The optimum conditions of supercritical CO2 extraction were determined by orthogonal experiment as follows: extraction pressure 30 MPa, extraction temperature 40℃, 75% ethanol as entrainer (5% of solid material) and extraction time 2.0 h. The yield of volatile oil was 9.92%.

通过正交实验确定超临界CO2萃取挥发油的优化条件为：以75%乙醇（添加量为原料质量的5%）为夹带剂、萃取压力30MPa、萃取温度40℃、萃取时间2.0h，此时，挥发油的收率为9.92%。

In this study, a rapid method for the determination of trace estrogens (ethinyl estradiol, estradiol, estriol, and estrone) in cosmetic water by LPME coupled with high performance liquid chromatography was developed.

建立了液相微萃取-高效液相色谱联用测定爽肤水中痕量的雌三醇，雌二醇，炔雌醇和雌酮的分析方法，研究了萃取溶剂种类，接受相体积，搅拌速度，萃取时间等对萃取效率的影响。

The binary and ternary experimental equilibrium data of the composites of mesitylene,1-methyl-2-ethylbenzene and 1,2,4-trimethylbenzene and the infinite activity coefficients γ~∞ are measured in the solvent of DBP .

以邻苯二甲酸二丁酯为萃取精馏溶剂，测定了邻甲乙苯—均三甲苯—偏三甲苯体系的二元及三元汽液平衡数据；编程关联了W ilson模型参数；采用物料平衡三对角矩阵法对萃取精馏过程进行了模拟，得出了萃取精馏塔的最佳操作条件，为萃取精馏法生产均三甲苯提供了基础数据。

The conclusions were as follows: theνO-H andνC=O IR absorption maxima shifted towards higher wave numbers after imprinting 17β-estradiol on TFMAA-co-TRIM copolymer with the red shift of theνO-H groups being apparent after precipitation polymerization for 16h while that forνC=O groups being observed after polymerization for 24h. A strong interaction between TFMAA and 17β-estradiol was confirmed by the high selectivity for 17β-estradiol, as indicted by the values of the separation factor of isomers of 17β-estradiol/17α-estradiol (2.28) and the imprinted factor (3.01). Particle diameter of TFMAA-co-TRIM polymer was between 300 nm and 1.5μm, which suited well for solid phase sorbent throughout at low column pressure. The recognition of imprinting TFMAA-co-TRIM polymer for sterol molecules was driven by enthalpy eluted with acetronitile, and low temperature was in favor of the separation of sterol structure analogues on imprinting column. TFMAA-co-TRIM polymer possessed of determinate anti-heat stability, with melting point beginning at 255.84℃, Tp=257.40℃, control TFMAA-co-TRIM polymer and imprinting TFMAA-co-TRIM polymer were respectively decompounded at 267.79℃and 343.11℃, and solid micro-extraction noddle prepared by the special polymerization also showed definite recognition for 17β-estradiol by GC/MS detecting at 270℃. By selection of various washing and elution solvents, elution reagents of close polymerization system were of more advantage in template molecules retention and recognition on molecularly imprinted solid phase extraction column. At a certain extent, progesterone, 17α-estradiol, 17β-estradiol and 4-androstene-3, 17-dione could be intercepted on the MISPE column. Especially, MISPE had high selectivity for progesterone, and imprinting TFMAA-co-TRIM polymer could achieve adsorption balance within 50 min by absorption kinetics test for 17β-estradiol. However, MISPE column showed better selectivity and enrichment property for 17β-estradiol than C18 and CSPE columns according to the data from HPLC and GC/MS analyses. Recovery of 17β-estradiol on MISPE column was up to 85.5% while when prime extracting solution of milk powder was sampled, the recovery of CSPE and C18 columns were 43.7% and 30.7%, respectively.

通过研究阐明：紫外聚合产物TFMAA-co-TRIM中的νO-H振动吸收峰在聚合16h后红移，νC=O振动吸收峰在聚合24h后红移；TFMAA-co-TRIM对雌二醇异构体的印迹因子达到了3.01，α为2.28，优于其它功能单体参与得到的聚合物识别特性；TFMAA-co-TRIM聚合物粒径介于300 nm至1.5μm之间，作为色谱固定相具有良好的通量和低的柱压；在乙腈流动相中，TFMAA-co-TRIM分子印迹固定相的分离过程主要被焓驱动，低温有利于分子印迹固定相分离甾醇结构类似物；TFMAA-co-TRIM分子印迹聚合物在255.84℃时开始熔融，Tp=257.40℃，聚合物CP的降解温度在267.79℃，MIP降解温度在343.11℃，制备的固相微萃取头初步经GC/MS 270℃的耐热性测定；不同的洗提溶剂筛选证明了选择接近聚合溶剂的洗脱体系更有利于MISPE发挥识别效应；分子印迹固相萃取柱对孕酮、17α-雌二醇、17β-雌二醇和雄烯二酮都具有不同程度的保留特性，可作为此类化合物的吸附材料，特别对孕酮强保留的富集特性，可作为孕酮的选择性识别吸附剂，其分子印迹聚合物对17β-雌二醇的吸附动力学测定显示在50 min内基本达到吸附平衡，具有作为传感器核心敏感材料的潜力；对比萃取奶粉中17β-雌二醇性能，MISPE柱比非分子印迹固相萃取柱和C18柱具有更高的保留，回收率依次为85.5%，43.7%和30.7%。

In order to optimize the technology for supercritical CO2 extracting the oil from Korean pine nut, the influencing factors such as extraction pressure, temperature and time on yield of the oil were investigated, and the fatty acid composition in the oil were also analyzed.

为优化超临界CO2萃取红松种仁油的工艺，研究了萃取压力、萃取温度和萃取时间对红松种仁油得率的影响，并对试验得到的种仁油进行了气质联用分析。

Extraction of the essential oil and oleoresin from garlic with supercritical carbon dioxide was studied. The effects of grind degrees, pressur e, temperature and time on extraction efficiencies were investigated.

研究了大蒜精油及油树脂的超临界CO2提取工艺，探讨了粒度，萃取及分离的温度、压力和时间对各萃取率的影响，建立了萃取温度、压力与各萃取率的数学模型。

The effect of ultrasound on the degradation of pyrethrins and the velocity of extraction are studied through the supercritical carbon dioxide extraction of pyrethrins from pyrethrum.

本文以除虫菊花中的除虫菊酯萃取为对象，研究用超临界CO2对其萃取时，施加超声场对萃取物降解及萃取速率的影响。

The effects of extraction conditions on the rate of wheat germ oil , the content of vitamin E and the component of fatty acids were studied.

采用超临界CO2流体萃取技术，从小麦胚芽中萃取小麦胚芽油，探讨萃取工艺对油的萃取率、维生素E含量、脂肪酸组分的影响。

Ingredients: Hyaluronic Acid, Chamomile Extract, Aesculus Extract, Rosemary Extract, Salvia Extract

成份：玻尿酸、洋甘菊萃取、七叶树萃取、迷迭香萃取、鼠尾草萃取。

As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸，那乌黑、忧郁的眼睛，她便会相信，他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失