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Through condensing o-aminobenzoic acid, ethyl oxalyl chloride and ethylenediamine(or 1,2-propylenediamine), two new ligands N-benzoato-N′-(2- aminoethyl)oxamido(H3oxbe) and N-benzoato-N-(2-amino-2-methylethyl)oxamido(H3oxbt) have been synthesized. Their mononuclear complexes Na·1.5H2O and Na·1.5H2O have also been obtained.

2以邻氨基苯甲酸、草酸乙酯酰氯和乙二胺(或1,2-丙二胺)缩合制得了两种具有不对称草酰胺结构配体N-(2-苯甲酰基)-N&-(2-氨乙基)草酰胺(H3oxbe)和N-(2-苯甲酰基)-N&-(2-氨丙基)草酰胺(H3oxbt),并得到了它们的单核配合物:Na·1.5H2O和Na·1.5H2O。

A new method for the synthesis of 1 methyl 3 propyl pyrazol e 5 carboxlic acid from 2 pentanone and diethyl oxalate is reported.

以 2 -戊酮和草酸二乙酯为起始原料,经缩合、与甲基肼环合、水解等三个步骤合成了 1 -甲基-3-丙基吡唑-5 -羧酸。

The data indicate an adaptive role of calcium oxalate crystals in photosynthesis in Peperomia.

本研究结果显示玲珑椒草叶片之光合作用的进行,其栅状细胞内的草酸钙晶体扮演著相对的适应性。

A series of Pd/α-Al2O3 catalysts for CO coupling reaction were prepared with α-Al2O3 made from different methods. The effect of pore-foaming agent and peptizer on the support and the effect of alumina pore structure on the dispersion and activity of catalysts were studied.

考察了不同制备方法得到的α-Al2O3载体对CO催化偶联制草酸二甲酯反应的影响,研究了致孔剂和胶溶剂对载体的影响以及氧化铝孔结构对催化剂分散度和活性的影响。

Several types of ligand reactions observed under hydrothermal condition were summed up:(1) hydrolysis of pyridine nitrile, aldehyde and ester in mixed water and alcohol into pyridine-carboxylate;(2) replacement of carboxylate group with sulfonic group;(3) coupling of phenanthroline by dehydrogen;(4) oxidative coupling of methanol into oxalic acid;(5) hydroxylation of isophthalate.

总结了以往在水热条件下观察到的几类配体反应:(1)吡啶腈、醛和酯在醇和水混合溶液中水解成吡啶羧酸;(2)磺基取代羧基反应;(3)邻菲啰啉的脱氢的聚合:(4)甲醇被氧化偶合生成草酸:(5)间苯二甲酸的羟基化反应。

The content of ferulaic acid is least, its range is 0.496~12.566μg·g~(-1), the content in old-growth Chinese fir soil is more than 5μg·g~(-1), and others are less than 5μg·g~(-1). The content of three phenylic acids in 0~20cm depth soil is larger than 20~40cm. Along the ecosystem conversion direction, in 0~20cm and 20~40cm depth soil, the laws of P-hydroxybenzoic acid, ferulic acid and vanillic acid content are complex, does not exist apparent refularity.

其中对羟基苯甲酸含量最大,大小范围为2.233~19.589μg·g~(-1),其中只有二代杉木人工林的20~40cm层土壤的酚含量小于5,其他的都大于5;香草酸次之,大小范围为0.912~5.683μg·g~(-1),其中只有天然更新常绿阔叶林的酚含量大于5,其他的都小于5;阿魏酸含量最小,大小范围为0.496~12.566μg·g~(-1),其中老龄杉木林的0~20cm和20~40cm层土壤的酚含量大于5,其他的都小于5。

The photooxidative degradation of Direct Fast Scarlet dyes in aqueous solution under solar irradiation by H 2O 2/ferrioxalate complexes has been studied.

以 H2 O2 /草酸铁络合物作光氧化剂,利用太阳光对水溶液中的直接耐酸大红进行了光氧化降解试验研究。

The interaction between diammonium glycyrrhizinate and bovine serum albumin was studied in physicological solution by spectroscopic methods including fluorescence spectra and UV visible absorption spectra. Synchronous fluorescence and three-dimensional fluorescence spectra were used to investigate the conformation change of bovine serum albumin due to the addition of diammonium glycyrrhizinate.

在模拟人体生理条件下,用常规荧光光谱和紫外-可见吸收光谱研究甘草酸二铵和牛血清白蛋白的相互作用机制,并利用同步荧光光谱和三维荧光光谱研究了药物对牛血清白蛋白构象的影响。

The process parameters of the separation and purification of shikimic acid from Picea meyeri with ion exchange resin were established.

建立了离子交换树脂分离纯化白扦中莽草酸的工艺条件和参数。

Several Chinese herbal medicine were selected to combine aerosol compound, such as Honeysuckle, Forsythia suspense Vahl, Glycyrrhiza uralensis, Platycodon grandi florum and Ophiopogon japonicus.

提取中药材连翘、甘草、桔梗、麦冬中的活性成分连翘酯甙、甘草酸、桔梗皂甙、麦冬多糖与绿原酸组合,研制成复方气雾剂。

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It has been put forward that there exists single Ball point and double Ball points on the symmetrical connecting-rod curves of equilateral mechanisms.

从鲍尔点的形成原理出发,分析对称连杆曲线上鲍尔点的产生条件,提出等边机构的对称连杆曲线上有单鲍尔点和双鲍尔点。

The factory affiliated to the Group primarily manufactures multiple-purpose pincers, baking kits, knives, scissors, kitchenware, gardening tools and beauty care kits as well as other hardware tools, the annual production value of which reaches US$ 30 million dollars.

集团所属工厂主要生产多用钳、烤具、刀具、剪刀、厨具、花园工具、美容套等五金产品,年生产总值3000万美元,产品价廉物美、选料上乘、质量保证,深受国内外客户的青睐

The eˉtiology of hemospermia is complicate,but almost of hemospermia are benign.

血精的原因很,以良性病变为主。