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In this experiment, high quality PTC powder was prepared by oxalate coprecipitation process.

本实验采用草酸盐共沉淀法制备含掺杂物的高性能PTC粉体。

Used the main eight kinds of phenolic acids with plant-defensive function as a control,and a high performance liquid chromatography to detected the leaves of corn that containing vanillic acid, caffeic acid, syringic acid and coumaric acid.

以植物中主要具有防御功能的8种酚酸作为对照,采用高效液相色谱法测得玉米叶片中主要含有香草酸、咖啡酸、丁香酸及香豆酸4种酚酸类化合物。

Materials and methods: Postoperative specimens from human parotid and submandibular glands were used. The glyoxylic catecholaminergic histofluores-cence method was employed on the tissues to study the sympathetic innerve-tion. One percent neutral red was used as a counterstain.

本研究以人类下颌下腺及腮腺切除的标本,应用甘草酸与儿茶胺形成之组织萤光法(glyoxylic catecholaminergic histofluorescence method),并采用1%中性红作对照染色,探讨2大唾液腺的交感神经分布。

Based on the problem of various types of catalyst and according to the features of carbonylation catalysts reactions, our team has been designed a series of new metal complexes of benimidazoles, which can be used for carbonylation catalyst of industry. Seven new benzimidazole derivatives were prepared by the o-phenylenediamine、oxalic acid、glycolic acid、monomethyl monopotassium malonate、ethyl cyanoacetate、succinic anhydride. The structures of them were confirmed by IR、Elemental analsis. The crystal structures of d and e were determined by X-ray single crystal diffraction of Germanic Bruker Smart APEX II CCD. The catalysis of them was tested by carbonylation reactions.

本文设计以邻苯二胺和草酸、羟基乙酸、丙二酸单甲酯、氰基乙酸乙酯、丁二酸单甲酯为原料采用PPA催化和无机酸催化法,合成了4种苯并咪唑-2-羧酸衍生物并进行了表征;培养了2个化合物d、e的晶体并测定和讨论了晶体结构;制备了3种未见报道的苯并咪唑金属配合物,对配合物在羰基化法制醋酐-醋酸反应的催化作用进行了初步试验。

A novel one-step green process for synthesis of glutaric acid by selective oxidation of cyclopentene was investigated.

研究了以环戊烯为原料、草酸为有机络合剂、H2O2为氧化剂,在催化剂钨酸(H2WO4)的作用下一步合成戊二酸的绿色新过程,考察了氧化剂的含量、反应物配比、催化剂用量、反应温度、反应时间等对反应的影响。

The result indicated, In the MS culture medium, and the damagement increased with Pb(superscript 2+) concentrition, when Pb(superscript 2+) concentration was up to 1000μmol/L, the callus was geatly damaged and its character is small, hard, skin drying; Organic acid of suitable concentration was able to improve the induction and growth of rice callus under the Pb(superscript 2+) stress, i.e. ascorbic acid, critic acid and oxalic acid The effect was the best which added 750 mol/L citric acid in MS culture medium, the callus was fresh, light yellow, loose, the surface moist. and survival was as higher as controlled treatment.

而添加不同有机酸(抗坏血酸、柠檬酸和草酸)均可明显改善Pb(上标 2+)胁迫下愈伤组织的生长,尤以750μmol/L柠檬酸对Pb(上标 2+)毒害的缓解效果最佳,其愈伤组织块颜色浅黄,表面湿润,愈伤组织成活率高,与对照愈伤组形态较接近。

For glycyrrhizic acid extraction and purity, Ammonia-water has superior efficient than decoct method at the best conditions.

在最佳条件下,氨水法提取的甘草酸纯度和提取率明显高于水酸法。

The use of carbon monoxide from coal or natural gas to produce dialkyl oxalate is an important research area in C1 chemical technology. The chemical reactions and performance in the coupling reaction system for synthesis of diethyl oxalate from carbon monoxide and ethyl nitrite were tested in the presence of hydrogen under the typical coupling reaction conditions.

摘 要:实验研究了在氢气存在下,一氧化碳与亚硝酸乙酯偶联合成草酸二乙酯反应体系在典型操作条件下的化学反应和反应性能,结果表明氢气只与反应体系中的亚硝酸乙酯反应生成乙醇。

Methods: Uses carbon tetrachloride (CC14) 2ml/kg, thioacetamide 200mg/kg, the abdominal cavity to inject separately, Establish model which the rat acute liver damages; Guarantees the liver profit stomach mixture, the polyene phosphatide acid radical choline capsule, the glycyrrhizic acid diamidogen capsule fills the stomach.

分别用四氯化碳(CC14)2mL/kg,硫代乙酰胺200mg/kg,腹腔注射,建立大鼠急性肝损伤的模型;保肝益胃合剂,多烯磷脂酰胆碱胶囊,甘草酸二胺胶囊灌胃治疗。

OBJECTIVE To investigate the optimum techniques for preparation of diammonium glycyrrhizinate injection by orthogonal test .

目的用正交设计方法优选甘草酸二铵注射液的制备工艺。

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