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茴香醚

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Green products in small fennel with yellow, bright color, particle filled evenly, smells aromatic, containing 2.3-2.4% of volatile organic Anethole rather thin, and many other ingredients Anethole is widely used in medicine, food chemicals and cosmetic industries, is the main condiment

小茴香产品绿中带黄,色泽鲜亮,颗粒均匀饱满,气味芳香,含有2.3—2.4%的挥发有机茴香脑、宁稀、茴香醚等多种成份,广泛应用于医学、食品化工及化妆工业,也是主要调味品

Anethole accounted for 82.65% of the whole oil. Selective isolation of anethole form the volatile oil was carried out using an inclusion crystalline method with 1,1,6,6- tetraphenylhexa- 2,4-diyne-1,6-diol inclusion complex with anethole . The crystal structure of the inclusion complex was determined by IR, 1^H NMR and single crystal XRD techniques.

采用包结结晶方法对小茴香挥发油中的对-丙烯基茴醚进行了选择性分离,以1,1,6,6-四苯基-2,4-已二炔-1,6-二醇作为主体分子,小茴香挥发油中的对-丙烯基茴香醚作为客体分子,D.D选择性地与之形成超分子包结物晶体。

A method for analysis of butyl hydroxy anisole in simvastatin had been established by HPLC.

建立了测定辛伐他汀中抗氧化剂叔丁基羟基茴香醚含量的高效液相色谱方法。

In the chapter 2 of this dissertation, we studied the cross-coupling reaction of aryl halides and vinyl iodides with sodium azide under the catalysis of copper and amino acids.

在4-碘茴香醚与叠氮化钠的模型反应中,我们考察了不同溶剂、氨基酸、碱、铜盐对反应的影响,最后筛选出了最佳的反应条件:CuⅠ/脯氨酸/NaOH/DMSO。

It showed that main constituents are linalool, geraniol, farnesol , safrole, citral, t-anethole , decanal and lauric aldehyde respectively and with high cont.

从它们的利用部位花、果、叶和根中,可提取芳香油,主要成分分别为芳樟醇、香叶醇、金合欢醇、黄樟素、柠檬醛、茴香醚及癸醛、十二碳醛等,含量相当高,为重要调香原料,有的作药用,颇具发展种植和开发利用价值。

The effects of the food additive butylated hydroxyanisole and the antibiotic Norfloxacin on swordtail fish were measured by considering a number of parameters, including glutathione S\|transferase, catalase, 7-ethoxyresorufin-o-dealkylases and malondialdehyde contents.

研究了叔丁基对羟基茴香醚(butylated hydroxyanisole, BHA)和诺氟沙星(norfloxacin, NFLX)对剑尾鱼的急性毒性及其肝脏谷胱甘肽硫转移酶、丙二醛、过氧化氢酶及7-乙氧基异吩恶唑酮-脱乙基酶活性的影响。

In part one, the reactions of some active fluorine-containing compounds such as 2, 2-dihydropolyfluoroalkanoic acids and ethyl 2-hydropolyfluoroalkenoates were studied and various fluorine-containing heterocyclic compounds were synthesized. Using 2, 2-dihydropolyfluoroalkanoic acids as the starting material, 4-fluoroalkyl quinolin-2-ols, 2- [ -1-hydropolyfluoro-1-alkenyl] -4H-3, 1-benzoxazin-4-ones, 1-aryl -4, 9-dihydro-3-fluoro-alkyl-1H-pyrazo [3, 4-b] quinolin-4-ones, 5-fluoroalkyl-12H-quin olino [2, 1-b] quinazolin-12-ones, 4-fluoroalkyl-1, 3-dihydro-1, 5-benzodiazepin-2-ones and 4-fluoroalkyl-2H-pyrido [1, 2-a] pyrimidin-2-ones were synthesized through its condensation reaction with anilines, anthranilic acid, N'-aryl-o-aminobenzamides, o-nitro aniline, o-amino pyridine and their derivatives and the subsequent transformations. 5-Fluoroalkyl isoxazolidines, 3-fluoro-3-fluoroalkylisoxazolidino [4, 3-c] quinolin-4-ones, 3-fluoroalkylisoxazolino [4, 3-c] quinolin-4-ones and 2-aryl-3per fluoroacylindoles were synthesized by inter-and intramolecular 1, 3-dipolar cycloaddition of fluorine-containing olefins and nitrones.

第二部分,我们研究了α,α-二氟苄基卤类化合物的亚磺化脱卤反应、产物的转化及全氟烷基亚磺酸盐与芳环化合物的全氟烷基化反应,发现全氟苄基碘或溴及α,α一二氟苄基溴在保险粉等亚磺化脱卤试剂引发下可生成相应的亚磺酸盐;全氟苄基亚磺酸盐与氯气或溴反应可生成全氟苄基磺酰氯或磺酰溴;在烯烃存在下,全氟苄基碘则与烯烃发生加成反应,生成相应的1:1加成产物;在三价醋酸锰的作用下,部分芳香化合物如茴香醚,二甲氧基苯,吡啶,喹啉等可以和过量的全氟烷基亚磺酸盐发生双全氟烷基化反应,反应表现出一定的区域选择性,产率良好。

Forbesii, monoterpenes and sesquiterpenes account for 41.30% and 32.65%, respectively, in which (1R)-α-pinene (3.98%), sabinene (2.51%),(1S)-β-pinene (5.78%), m-cymene (4.05%), limonene (3.55%), 3, 7-dimethyl-1, 3, 7-octatriene (3.98%),γ-terpinene (8.70%), anisole (1.78%) and (1S)-endo-bornyl acetate (2.62%) as the monoterpenes and its derivatives, and-β-elemene (1.17%),α-bulnesene (1.40%),-β-bisabolene (1.21%),-elemol (1.42%), guaiol (1.14%), dehydroxyisocalamendiol (1.13%),-aristolene (1.99%), bulnesol (9.48%),γ-eudesmol (1.77%), guai-1(10)-en-11-ol (1.12%) and α-bisabolol (5.35 %) as the sesquiterpenes and its derivatives are the main components.

1R-α-蒎烯(3·98 %)、桧烯(2·51 %)、(1S)-β-蒎烯(5·78 %)、m-月桂烯(4·05 %)、柠檬烯(3·55 %)、3,7-二甲基-1,3,7-庚三烯(3·98 %)、γ-萜品烯(8·70 %)、茴香醚(1·78 %)和(1S)-桥环醋酸冰片酯(2·62 %)为单萜类化合物及其衍生物中的主要成分;-β-榄香烯(1·17 %)、异愈创木烯(1·40 %)、-β-没药烯(1·21 %)、-榄香醇(1·42 %)、愈创木醇(1·14 %)、去羟基异菖蒲二醇(1·13 %)、-土青木香烯(1·99 %)、异愈创木醇(9·48 %)、γ-桉醇(1·77 %)、愈创木-1(10)-烯-11-醇(1·12 %)和α-没药醇(5·35 %)为倍半萜类化合物及其衍生物中的主要成分。

The chemical composition of th essential oil from Illicium verum Hook.f.was determined by the means of GC-MS.

采用GC-MS对八角茴香挥发油的化学成分进行分析,其中反式茴香醚的含量最高。

The chemical components of volatile oil from Foemiculum Vulgare Mill were determined by GC-MS.

用GC-MS方法测定了小茴香挥发油的全组分,其中对-丙烯基茴香醚的含量为82.65%。

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The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应,而且减少跟风的可能性。

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