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Odoquinazolin-4(3H)-one,7-methyl-4(3H)-quinazolinone,7-bromoquinazolin-4(3H)-one were synthesized by using anthranilic acid、2-amino-5-nitrobenzoic acid、2-amino-4-nitrobenzoic acid,6-nitro--4(3H)-quinazoline-one、o-amino-terephthalic acid, 2-amino-4-hydroxy benzoic acid、2-amino-5-bromo-benzoic acid、2-amino-5-iodine acid,1、4-butynediol、L-glutamine、isatin anhydride、formamide as starting materials and utilizing microwave-assisted synthetic approach.

本文利用微波辅助合成的方法,以邻氨基苯甲酸、2-氨基-5-硝基苯甲酸、2-氨基-4-硝基苯甲酸、邻氨基对苯二甲酸、2-氨基-4-羟基苯甲酸、2-氨基-5-溴苯甲酸、2-氨基-5-碘苯甲酸、5-甲基-2-氨基苯甲酸等为原料与甲酰胺反应,以及以1,4-丁炔二醇、L-谷氨酰胺与靛红酸酐反应,共合成了13个喹唑啉酮衍生。。。

Low-valent titanium reagent induced the monomolecular reduction of N-substitutedphthalimides supplied a new method of synthesis hydroxyl lactams. This method was moreeconomic, convenient and in higher yields comparing with other methods reported before,therefore it has practical value.

4低价钛试剂引起邻苯二甲酰亚胺的单分子还原反应提供了一种合成羟基内酰胺的新方法,和文献方法相比,我们的方法试剂便宜易得,毋需溶剂,操作简便,收率也有所提高,具有实用价值。

Fe nanoparticles were treated by situ polymerization with Acrylic amide using sodium dodecylbenzenesulfonate as dispersant, and the Fe nanoparticles coated by AM were achieved.

采用丙烯酰胺处理纳米铁粉,通过原位聚合方法,以十二烷基苯磺酸钠作为分散剂,在纳米铁粉表面包覆上聚丙烯酰胺。

The wax crystal dispersing agent is abietic acid diethylene glycol dinitrateThe acid radical amines. they duplicate match with the host medicinal preparation need to have the adjustment slightly according to the diesel oil composition.

蜡晶分散剂为松香酸酯酰胺类和3,6-氧桥-1,2,3,6-四氢苯-1,2-二甲酸高级酯/酰胺类,它们与主剂的复配需要根据柴油组成略有调整。

The said glutamine synthetase is prepared by abrupt change of the 405th amino acid residue of amino end to phenylalanine corynebacterium glutamicum.

该谷氨酰胺合成酶是自氨基端第405位氨基酸残基突变为苯丙氨酸的谷氨酸棒杆菌的谷氨酰胺合成酶。

With benzoic acid, terephthalic acid, 2. 6naphthalene dicarboxylic acid, dimethyl-2, 6-naphthalene dicarboxylate as solutes, water, acetic acid, N, N-dimethylformamide, N, N-dimethylacemide, dimethyl sulphoxide, N-methl2-ketopyrolidine, and the mixture of water and acetic acid as solvents respectively, the solubilities of 15 binary systems and 4 ternary systems were determined.

实验以苯甲酸、对苯二甲酸、2,6-NDCA、2,6-萘二甲酸二甲酯为溶质,以水、醋酸、N,N-二甲基甲酰胺、N,N-二甲基乙酰胺、二甲基亚砜、N-甲基-2-吡咯烷酮以及水和醋酸的混合溶液为溶剂,测定了十五个二元物系和四个三元物系的溶解度数据。

A series of novel aromatic amide molecular tweezers with different chiral centers and cavities were designed and synthesized by using isophthalic acid as the spacer to bridge the different L-amino acid methyl esters under microwave irradiation.

以间苯二甲酸为隔离基,酰胺键桥联L-氨基酸甲酯构成手臂,在微波辐射下合成了具有不同手性中心和裂穴的新型手性芳酰胺类分子钳。

A high ordered ladderlike polyhydrosiloxane was successfully synthesized by the strong H-bonding template of N〓, N〓-bis (1-hydroxy-2-methylpropan-2-yl) terephthalamide.

通过强的酰胺氢键模板作用首次合成了高规整性、可溶的反应性有机桥基N,N-二(2-羟基-2-甲基丙基)对苯二甲酰胺聚氢基硅氧烷高分子。

The pathogenic bacterium of prepartum and intrapartum infectious pneumonia mostly were G- bacilli,the pathogenic bacterium of postpartum infectious pneumonia mostly were G- bacilli and staphylococcus aureus.6.The drug resistant rates of G- bacteria to penicillins,cephalosporins,and monocyclicβ-lactam antibiotic were high,However,their compound of addingβ-lactamase inhibitor agents was relatively low resistance,and all G- bacteria were sensitive to carbapenem antibiotics.

产前及产时感染性肺炎的病原菌以G-杆菌多见,而产后感染性肺炎的病原菌主要为G-杆菌和金葡菌。6.G-菌对青霉素类、头孢菌素类及单环类的β内酰胺类抗生素耐药率高,但对其添加β内酰胺酶抑制剂的复合制剂耐药率较低,对碳青霉烯类抗生素均敏感;金葡菌对苯唑西林耐药率低,对万古霉素均敏感。7。

The new oxalamide bridging ligands N, N'-bis (4-hydroxy-3-methoxy-benzyl) oxalamide (H4LB) was designed and synthesized.

设计合成一种新型对称的草酰胺桥联配体:N,N'-二(4-羟基-3-甲氧基苯甲基)草酰胺配体(H4LB)。

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Chapter Three: Type classification of DE structure in Sino-Tibetan languages.

第三章汉藏语&的&字结构的类型划分。