苯酰化

On the basis of these studies, sensitive and rapid determination methods of AM and MA in urine by gas chromatography with electron-capture detection combined with various acyl derivatization were developed.

在此基础上，建立了人尿中苯丙胺和甲基苯丙胺的酰基衍生化的气相色谱－电子捕获检测分析方法。

METHODS:This compound was synthesize by steps of ammonolysis,hydrogenize,diazotization and coupling from 4-nitrobenzoyl chloride.

以对-硝基苯甲酰氯为原料，经氨解、氢化、重氮化及偶合四步反应得到了巴柳氮。

Water, Beta-glucan, Ascorbic acid, Tri Sodium Ascorbyl Palmitate Phosphate, Magnesium L-ascorbyl -2-phosphate, PEG-60 hydrogenated castor oil, Lecithin, Coceth-7 / PPG-1-PEG 9 lauryl glycol ether/PEG 40 hydrogenated castor oil, DL-panthenol, Retinyl, palmitate, Anthemis Nobilis Flower extracts, Pinebark extract, Phellinus linteus extract, Phellinus linteus / Rice Ferment Extract, Onion extract, Aralia Elata Root Extract, Grape extract, Sandalwood oil, Myrtle oil, Orange oil, 1,3-Butylene glycol, Glycerin, Xanthan gum, Tocopheryl acetate, Ethanol, Methyl paraben

水， β-葡聚糖，抗坏血酸、三磷酸抗坏血酸棕榈酸酯钠、维他命 C 磷酸镁盐、聚乙二醇- 60氢化蓖麻油、卵磷脂、椰油醇聚醚-7 / PPG-1-PEG-9 月桂二醇醚/聚乙二醇40氢化蓖麻油，消旋泛酰醇，视黄醇，棕榈酸盐，白花春黄菊花提取物， Pinebark提取物，桑黄提取物，桑黄/水稻发酵提取物，洋葱提取物，辽东楤木根提取物，葡萄提取物，檀香油，桃金娘油，橙油， 1，3 -丁烯乙二醇，甘油，黄原胶，生育酚，乙醇，羟苯甲酯

The calixarenes used as PTC in the fluorination of tetrachlorophthahaloyl chloride to obtain dimethyl tetrafluoroterephthalate were studied in this paper.

研究了杯芳烃在四氯对苯二甲酰氯氟化制备四氟对苯二甲酸二甲酯反应中的相转移催化作用，发现以杯芳烃作相转移催化剂使产品收率得到了明显提高。

Compound 9 is glycosylated in the presence of TMSOTf with rhamose-derived trichloroacetimidates to provide target trisaccharide Saponin 1, oleanolic acid 3-yl-2,4-di-O-a-L-rhamnopyranosyl -p-D-glucopyranosideCoumpond 18 is prepared with oleanic acid and Bromide 11 through phase-thansfer catalysis glycosylation manner.

三糖皂苷Saponin 1是以葡萄糖齐墩果酸皂苷为起始原料，用BBTZ(1-苯甲酰苯并噻唑)选择性保护葡萄糖3′，6′-羟基得到化合物9，然后以化合物9为糖基受体，进行一步糖苷化可以在化合物9的2′，4′-羟基上同时引入两分子鼠李糖，最后脱掉所有的保护基得到目标化合物Saponin1。

Universal indicator paper,special indicator paper,ammonium fluoride,ammonium hydrogen difluoride,nbenzyldimethylamine,disinfectant paper,nacetylphenylhydrazine,mcresol purple,bromocresol green,fluorescein,eosin Y,ninhydrin,phenedons,potassium phthalate,pamimobenzene sulphonic acid anhydrous.

广泛试纸，精密试纸，氟化铵，氟化氢铵，N苄基二甲胺，消毒试纸，N乙酰苯肼，间甲酚紫，溴甲酚绿，荧光素，曙红Y，水合茚三酮，菲尼酮S，苯甲酸氢钾，无水对氨基苯磺酸。

In a similar way, using N,N\'-dibenzyl tartamide as auxiliary,-(2-methyl)allyl-2-chloro-phenyl-methyl azide, a vital intermediate of Repaglinide, can be prepared via asymmetric allylation of o-chlorobenzaldehyde in

产物经氧化和碘加成内酯化反应得到阿伐他汀中间体(3R，5S)-3-羟基-5-碘甲基戊内酯(10)；将N-苄基酒石酸二酰胺用于邻氯苯甲醛的不对称烯丙基化反应以较高光学收率得-甲基烯丙基-2-氯苯基-甲基醇

And then the intermolecular reductive cyclization reaction of N,N-diethyl-o-nitrobenzenesulfonamide with nitriles promoted by samarium diiodide was studied. 2H-1,2,4-Benzothiadiazine 1,1-Dioxides were prepared in good yields under mild and neutral conditions.

然后研究了二碘化钐促进的邻硝基N，N-二乙基苯磺酰胺与腈发生的分子间交叉还原偶联反应，一步合成了2H-1，2，4-苯并噻二嗪-1，1-二氧化物。

The alkylation of a-methylene of PhSO2CH2COPh with alkyl halides catalyzed by quaternary ammonium base resin in 50% aqueous sodium hydroxide solution was investigated.

本文以季铵碱树脂作为聚合物固载的相转移催化剂，在50%氢氧化钠水溶液中催化α-苯磺酰基苯乙酮(1)的α-亚甲基的烷基化反应。

Wedgeplug O-Seal plug valves with their positive, no-leak features are not only recommended as the best general purpose valves for handling hydrocarbons, vegetable oils, solvents, etc., but are ideal for such tough service as butane, propane, butadiene, acetone, ethyl alcohol, ammonia, anhydrous ammonia, benzene, vinyl chloride, dry chlorine, Dowtherm, ethane, ethylene, hydrogen chloride, napthalene, oxygen, hydrogen, phthalic anhydride, dry phosgene, phosphoric acid, potassium carbonate, styrene, molten sulphur, sulphur dichloride and related services within a temperature range from -300oF to + 450oF within pressure limits of the valves.

楔塞O形密封旋塞阀具有积极的、无泄漏特性，不但是最好的通用的阀门，用于处理碳化氢，植物油，溶剂等，还特别适用于严酷的应用环境，如丁烷，丙烷，丁二烯，丙酮，乙醇，氨，无水氨，苯，氯乙烯，干氯，道氏热载体，乙烷，乙烯，氯化氢，萘，氧，氢，邻苯二甲酸酐，干碳酰氯，磷酸，碳酸钾，苯乙烯，融化硫，二氯化硫，以及温度在-184oC至232oC之间，压力在阀门额定压力等级范围内的有关应用。

The labia have now been sutured together almost completely.The drains and the Foley catheter come out at the top.

此刻阴唇已经几乎完全的缝在一起了，排除多余淤血体液的管子和Foley导管从顶端冒出来。

To get the business done, I suggest we split the difference in price.

为了做成这笔生意，我建议我们在价格上大家各让一半。