苯胺的

Results indicated that the content of polyaniline had significant influence on the anticorrosive performance of the coatings.

结果表明：聚苯胺含量对涂层的防腐蚀性能有较大影响，当涂层中聚苯胺含量较低时，随着聚苯胺在涂层中质量分数的增加，涂层的防腐蚀性能相应提高；随涂层中聚苯胺质量分数的进一步增大，涂层的防腐蚀效果开始下降；涂层中聚苯胺含量为5.0%时具有最佳的防腐蚀性能。

After sodium bisulfite reacted with methanal at 60-65℃ for 0.5h, aniline was dripped into the system to synthesize phenylaminomethyl-sodium sulfonate subsequently, the diazol solution of p-nitroaniline was dripped into phenylaminomethyl-sodium sulfonate synthesized to form 4'-nitro-4-aminoazobenzene. The compound was then added into diazol solution of p-chloroaniline to obtain the object product, which was identified by IR spectrum and element analysis.

在60~65℃温度下，亚硫酸氢钠与甲醛反应半小时之后滴入苯胺生成苯胺基甲基磺酸钠，另将硝基苯胺重氮化得到重氮盐溶液滴入苯胺基甲基磺酸钠中得到4'-硝基-4-氮基偶氮苯，然后将其滴入氯苯胺重氮化后的重氮盐溶液中，得经红外光谱检验和元素分析证实的目标产物。

A two-component carbon tetrachloride system and a two-component aqueous system have been treated with the proposed strategy where only 21 calibration samples are needed, and the result showed that the predictive ability was not obviously impaired for the former system while being clearly strengthened for the latter one in comparison with a conventional way that required a calibration set of 100 samples.5 An unlooked-for experimental observation that in near-infrared spectroscopy the second overtone of aniline adsorbed by 13X molecular sieve nearly disappeared led us investigate a fundamental problem: the behavior of NIR when the outside space surrounding a molecule is too small to allow the molecule to vibrate freely.

同时，最小相关样本设计能进一步减少所需的校正样本数，且能提供更多合适变量以建立多元校正模型。这两方面的改进使模型的预测能力得以提高，其预测精度即使在水体系中也有明显的改善。五、近红外漫反射光谱在线非接触监测气-固吸附过程中出现了一个意外现象，即在近红外光谱上，被13X分子筛吸附的苯胺的二级倍频几乎完全消失了。这促使笔者深入探讨了近红外光谱的空间效应(当一分子被一足够小的刚性空间限制时，其振动的受限导致一级倍频和二级倍频强度均减少，并且后者减少的程度比前者更大)。

This study concludes the following four parts:(1) acute toxicity of several chloroanilines to zebra fish;(2) effects of chloroanilines on antioxidant defense of crucian carp;(3) effects of chloroanilines on serum sex steroids in crucian carp;(4) effects of chloroanilines on lymphocyte proliferation in crucian carp, and the detailed results and main conclusions are concluded as follows

本论文以2-氯-4-硝基苯胺、4-氯-3-硝基苯胺、2-氯-5-硝基苯胺、2，4-二氯苯胺、3，4-二氯苯胺、2，5-二氯苯胺、2，3-二氯苯胺为研究对象，研究分为四部分：(1)氯代苯胺对鱼类的急性毒性；(2)氯代苯胺对鲫鱼抗氧化系统的影响；(3)氯代苯胺对鲫鱼血清性类固醇激素水平的影响；(4)氯代苯胺对鲫鱼淋巴细胞增殖的影响。

The acute toxicities of 2-chloro-4-nitroaniline, 4-chloro-3-nitroaniline, 2-chloro-5-nitroaniline, 2, 4-dichloroaniline, 3, 4-dichloroaniline, 2, 5-dichloroaniline, 2, 3-dichloroaniline to zebra fish were conducted in lab. 48h LC〓 values were 11. 18, 4. 62, 9. 23, 9. 55, 7. 07, 6. 68, 0.62mg/L respectively, and 96h LC〓 values were 6. 99, 2. 58, 8. 63, 7. 79, 6. 08, 5. 23, 0.49mg/L respectively.

1研究了2-氯-4-硝基苯胺、4-氯-3-硝基苯胺、2-氯-5-硝基苯胺、2，4-二氯苯胺、3，4-二氯苯胺、2，5-二氯苯胺、2，3-二氯苯胺对斑马鱼的急性毒性，经计算48h LC〓分别为11.18、4.62、9.23、9.55、7.07、6.68、0.62mg/L，96h LC〓分别为6.99、2.58、8.63、7.79、6.08、5.23、0.49mg/L，这7种化合物均属于高毒物质。

At first, Polyaniline was synthesized by the improved chemical oxidation technique, then, PANI/HCl, PANI/TSA and PANI/DBSA were obtained by doping emeraldine with HCl, 4-methyl benzene sulfonic acid and dodecylbenzene sulfonate acid, separately. Leucoemeraldine was obtained in the N-dimethylformamide by using phenylhydrazine deoxidizing emeraldine in N_2 atmosphere.

本文首先通过改进合成条件的化学氧化法合成了聚苯胺，经氨水脱掺杂获得本征态聚苯胺，再经盐酸、对甲苯磺酸、和十二烷基苯磺酸掺杂，分别获得到质子酸掺杂的聚苯胺样品，然后在N，N-二甲基甲酰胺中，利用苯肼，在N_2氛围下还原本征态聚苯胺得到还原态的聚苯胺。

In solvent and under the action of certain catalyst, anilino methyl siloxane is reacted to obtain solid cage anilino methyl sesquisiloxane octamer acid salt; and through filtering, washing, precipitation and reaction with amine desalting agent, cage anilino methyl sesquisiloxane octamer is finally prepared.

本专利提供了一种笼型八聚苯胺甲基倍半硅氧烷的制备方法，苯胺甲基硅氧烷在一定溶剂和催化剂作用下反应，过滤得到笼型八聚苯胺甲基倍半硅氧烷酸式盐固体，经过洗涤、沉淀，再与胺类脱盐剂作用，最终制得笼型八聚苯胺甲基倍半硅氧烷。

For example, when there is only an alcohol as dopant, fiber-shaped nanostructure polyaniline is easily formed; when there is only a metallic ion as dopant, sphere-shaped nanostructure polyaniline is easily formed; when alcohol and metallic ion coexist, fibrous and sphere-shaped nanostructure polyaniline are formed at the same time.

如仅有醇类掺杂剂存在下，苯胺易于聚合成纤维状纳米结构的聚苯胺；仅有金属离子掺杂剂存在下，苯胺易于聚合成球形纳米结构的聚苯胺；在醇和金属离子掺杂剂共存时，苯胺能同时聚合成纤维状和球形纳米结构的聚苯胺。

It has been proved that surface confined quinones can greatly impove the electrocatalytic activity for ORR.

本论文中研究的氨基蒽醌聚合物修饰电极，与其它方法得到的醌类修饰电极比较，具有性质稳定、制备过程简单、活性点位浓度高等优点，而且同时具有类似聚苯胺的长链结构和蒽醌官能团的特性，为制备具有高氧还原催化活性的蒽醌修饰电极的研究提供了新的思路。

Poly-aminoanthraquinone modified electrode is more stable, more easily prepared, and can provide higher surface concentration of reactive sites compared with other quinones modified electrode by adsorpsion or doping.

本论文中研究的氨基蒽醌聚合物修饰电极，与其它方法得到的醌类修饰电极比较，具有性质稳定、制备过程简单、活性点位浓度高等优点，而且同时具有类似聚苯胺的长链结构和蒽醌官能团的特性，为制备具有高氧还原催化活性的蒽醌修饰电极的研究提供了新的思路。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。