苯胺的

P-π conjugated polyamic acid was synthesized by the poly-condensation of benzoguanamine and pyromellitic dianhydride under microwave irradiation. Then PAA was grafted with different side-chain containing azobenzol groups through azo coupling reaction.

选取苯代三聚氰胺和均苯四酸二酐为单体进行微波辐射溶液聚合反应，所得的聚酰胺酸与对位取代基不同的苯胺重氮盐偶合接枝，从而合成了一系列新的具有三阶非线性光学活性的侧链型聚合物。

For the PEO-grafted polyaniline series with different contents of EO units, the benzenoid absorption peaks exhibited blue shifts in comparison with polyaniline, the shifts became greater as the content of EO units increased.

与聚苯胺相比，在共聚物的UV-Vis吸收光谱中，原来320nm处的苯环吸收峰出现了蓝移，其蓝移程度随着共聚物EO单元含量的增大而加剧，且Poly较Poly发生更大的蓝移。

At present, the investigation about this aspect is concentrate on the pure inorganic cathodal electrochromic materials like WO3 and organic electrochromic materials like Prussian blue and Polyaniline.

关于这方面的研究却主要集中在以WO_3为代表的一元无机阴极电致变色材料和普鲁士兰、聚苯胺为代表的有机电致变色材料上，对多元的电致变色材料的研究较少。

Methods: A 5ml bone marrow was extracted from the lilac of human volunteers. By Percoll fluid and density gradient centrifugation, the MSC was obtained; after the cells filled the bottom of vessel, subcultured them, when they subculture in third generation, redigested them, 500 R/min centrifugate, alter the completed medium to chemical definition medium, examined the form change and prolifration of cells by invert microscope, toluidine blue stain、immunocytochemical stain and RT-PCR to test the type Ⅱ collagen mRNA and proteoglycan.

取健康成人髂后上棘处骨髓5ml，经percoll液分离后密度梯度离心，〓／ml密度接种培养，观察原代细胞的贴壁、增殖状况，细胞长满瓶底后进行传代培养；传至第三代细胞，重新消化后以500转／分钟轻度离心5分钟，〓／ml接种，改用化学限定培养基代替完全培养基培养，倒置显微镜观察细胞生长情况及形态变化，甲苯胺蓝染色观察诱导细胞合成细胞外基质中的蛋白多糖，免疫细胞化学染色检测ECM中Ⅱ胶原的蛋白合成，RT-PCR鉴定诱导细胞Ⅱ胶原mRNA的表达。

The aim are:lTo examine the proliferation ability and potential chondroblast differentiation ;2To find an ideal condition stimulated BMSC differentiate into chondroblast;3To examine the chondroblast proliferation in porous scaffolds and to explore the interaction between cells and materials;4To examine the release of cytokine in vitro.

取健康成人略后上棘处骨髓 5ml，经 percoll液分离后密度梯度离心，10'砌l密度接种培养，观察原代细胞的贴壁、增殖状况，细胞长满瓶底后进行传代培养；传至第三代细胞，重新消化后以500转／分钟轻度离心 5分钟，10V加 l接种，改用化学限定培养基代替完全培养基培养，倒置显微镜观察细胞生长情况及形态变化，甲苯胺蓝染色观察诱导细胞合成细胞外基质QCM）中的蛋白多糖，免疫细胞化学染色检测ECM中＊胶原的蛋白合成，RT干CR鉴定诱导细胞＊胶原mRNA的表达。

The synthesis of 4,5,7-trichloroquinoline makes use of ethyl orthoformate, cyanoacetic ester and 3,5-dichloroaniline as the raw materials. The synthesis is completed by four steps: condensation, cyclization, hydrolyzation and chlorination. Several conditions concerned in the process are studied, the whole yield of 4,5,7-trichloroquinoline is about 53%, and the purity of it is about 96%. All the products are testified by IR, NMR and HPLC.

介绍了以3，5-二氯苯胺、原甲酸三乙酯和氰乙酸乙酯为原料，经过缩合、成环、水解和氯代4步反应制备4，5，7-三氯喹啉的方法，对相关的试验条件进行了考察，通过红外光谱、核磁共振谱和液相色谱对4，5，7-三氯喹啉的结构和纯度进行表征和测定，试验结果为4，5，7-三氯喹啉的纯度大于96%，总收率达到53%。

The disubstituted ureas and the catalyst could be separated by addition of water and the catalyst could be reused without deactivation.

新型高效的菲咯啉钯-离子液体含氮化合物羰化催化剂体系，以苯胺为反应物时该体系的转化频率可以达到6000mol/mol/h；氢氧化铯-离子液体催化剂体系，可以在不加入化学计量脱水剂的条件下活化二氧化碳与脂肪族胺反应得到二取代脲，反应结束后可以通过加入水实现产品和催化剂体系的分离，催化剂体系可以重复使用。

In this dissertation, electrophilic reactions of Nitrosonium with imines, aza-Diels-Alder reactions of N-arylimines with a variety of electron rich olefinic compounds induced by NO~+, and photoreactions of N-nitrosodiphenylamine with aromatic amines were studied.

本文研究了：(1)NO~+与亚胺双健发生的亲电反应；(2)NO~+引发的芳香亚胺和富电子碳碳双键作为亲二烯体的氮杂Diels-Alder反应，高选择性地得到了一系列四氢喹啉的衍生物；(3)N—亚硝基二苯胺与芳香胺发生光化学反应得到了一系列偶氮苯类化合物。

The novel methods for the synthesis of Camptothecin intermediates were described as Friedlandle. Second, we synthsized the key compound—BI, and then made some improvements and innovations of the methods from the reference. The method of using more economically phenylaldehyde derivatives and phenylamine derivatives instead of o-aminobenzaldhyde was worked out.

然后成功合成重要的中间体BI，并且在参考原始文献的基础上作出了改进和创新，使用更便宜的苯甲醛衍生物和苯胺衍生物代替了邻氨基苯甲醛，合成了一系列未关B环的喜树碱中间体衍生物，并获得成功。

The charges on the substituents affected OWF〓 greatly for some azobenzene derivatives, pyridone derivatives, nitrodiphenylamine derivatives, some reactive dyes and 1, 4-diamino anthraquinone derivatives, in this instance, OWF〓 changed linearly with the change of the charges.

2给电子取代基或吸电子取代基的电荷对OWF〓有较大的影响，OWF〓随电荷的变化而线性变化，如某些偶氮苯衍生物、吡啶酮类染料母体、硝基二苯胺类化合物、偶合组分和重氮组分之间夹角α变化不大的活性染料、1，4—二氨基蒽醌衍生物等。

For a big chunk of credit-card losses; the number of filings (and thus charge-off rates) would be rising again, whether

年美国个人破产法的一个改动使得破产登记急速下降，而后引起了信用卡大规模的亏损。

Eph. 4:23 And that you be renewed in the spirit of your mind

弗四23 而在你们心思的灵里得以更新