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In the process, 2, 4-difluoroaniline is used to carry out ammoniated reaction. Then through a series of similar reactions, the important intermediate of temafloxacin, which is called 7-chloro-6-fluoro-1-(2, 4-difluorophenyl)-1, 4-dihydro-4-oxo-3-quinoline acid, is gained.

与环丙沙星和二氟沙星类似,用2,4-二氟苯胺进行胺化反应,再进行一系列类似的反应,制得合成替马沙星的关键中间体7-氯-6-氟-1-(2,4-二氟苯基)-1,4-二氢-4-氧代喹啉-3-羧酸。

Interface construction and preparation of new in situ polymerized polyaniline layer-by-layer self assembled films were also investigated.

拓展了聚苯胺LBL自组装膜的界面构建、新型膜的固定等基础性问题研究。

Adsorpytion of congo red and crystal violet can be described using the Langmuir isotherm, on the other hand, adsorption of methylene blue and aniline blue can be described using a Freundlich isotherm.

对刚果红和结晶紫的吸附服从Langumir吸附等温线,而对于亚甲基蓝和苯胺蓝的吸附则服从Freundlich吸附等温线,图4,表2,参9。

Results Besides the action of conduction anesthesia,chlordimeform has the cardiovascular toxicity and the antiarrhythmic action induced by barium chloride,parallel to 2,6-dimethyl aniline.

结果 杀虫脒有局部麻醉作用,杀虫脒和利多卡因的代谢物2.6-二甲基苯胺都有心血管毒性和抗氯化钡诱发的心律失常作用。

The key steps were the stereospecific conversion of both allylie carbamates 10 and 13 into 11 by Li_2Cu_3(CH_2)_5 and the stereoselective hydroxylation of unsaturated side chain by OsO_4-NMO.

合成的关键步骤是用Li_2Cu_3(CH_3)_5立体专一地转化烯丙醇苯胺基甲酸酯10和13成为11和用OsO_4-NMO在化合物16的不饱和侧链上立体选择性羟基化。

Because substituted anilines have Lewis acid or Lewis base group, extractions with complexing agent was conducted.

由于取代苯胺都具有Lewis酸性或Lewis碱性官能团,采用相应的络合剂进行了络合萃取的研究。

The rats were killed by cutting theirnecks and physical blood was taken for preparing serum, interleukin 2 (IL-2) was detected by radioimmunoassay ; the spleen was taken for measuring ConA-induced reaction of lympho- cyte proliferation and induced production of IL-2; and the activity of induced production of spleen's IL-2 was determined by the means of cell proliferation of mouse thymus; the skin and trachea were taten for slice with paraffin wax, dyeing with methybenzoamine blue so as to survey mast cells .

将大鼠断头留取躯干血制备血清,用RIA法检测白细胞介素2(IL-2);取脾脏行ConA诱导的淋巴细胞增殖反应测定和IL-2诱生;并用小鼠胸腺细胞增殖法检测脾IL-2诱生活性;取皮肤和气管做石蜡切片、甲苯胺兰染色检测肥大细胞,结果显示:应激组较对照组脾淋巴细胞增殖降低,cpm分别为9466±3.17和24019±3879(P.001);MC明显减少,分别为8.6±3.0/HP和25.4±3.7/HP(P.001),前组形态异常较其甚(MC多较小,呈多角或不规则状),且组织中可见分散的崩解颗粒。

The lung was fixed in 10% formalin solution and embedded in paraffin for Haematoxyffin-eosin staining to observed the form of embolisms, Masson staining to assess collagen and fibrin/fibrinogen distribution and Toluidine blue staining was to observe mast cell distribution.

以10%甲醛固定肺组织,制成组织切片,行苏木精-伊红染色观察血栓的形态,Masson染色观察栓塞血管的胶原纤维分布,甲苯胺蓝染色观察血管栓塞处肥大细胞分布。

The film made by PAn has some miraculous physical and chemical properties ( such as conductivity and electrochromism ,etc.), and could be potentially used in display devices ,secondary battery , gas separation, etc.

掺杂态聚苯胺特有的导电性、电致变色等物理化学性能,使其在显示器件、二次电极、气体分离等方面具有广阔的应用前景。

The good results can be obtained with the newalgorithm; the local minimal can be avoided in some degree. In this paper, neural networks also were applied to quantitativestructure-property relationships analysis:1Studies on the toxicity of aniline, nitrobenzene and phenol derivatives and their structures.2 Studies on HEPT compounds for their anti-aids.3 Studies on nitrogen mustards and 2-formylpyridine thiosemicarbazone compounds for their anti-cancer.4 Studies on phenol and aniline derivatives for their gas chromatographic retention values.5 Studies on discrimination of tea by Self-organizing feature map network.

本论文还利用上述方法进行了一些定量结构活性相关性研究,主要内容: 1环境中有毒有害有机物的定量结构活性相关性研究。2抗艾滋病类药物定量结构活性相关性研究。3抗肿瘤类药物(氮芥子气类化合物和2-甲酸吡啶缩氨基硫脲类化合物)定量结构活性相关性研究。4苯酚和苯胺类衍生物色谱比移值预测。5将神经网络用于茶叶的分类。

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