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Methods This study contained a total of 16 culture groups, including one group as control and 5 groups treated by 5 drugs (calcium L-threonate, sodium L-threonate, alendronate, 17β-estradiol and calcium gluconate) each at the final concentrations of 10^(-9)mol/L, 10^(-7)mol/L, 10^(-5)mo1/L respectively. After 7 days, eight bone slices of every group were stained with toluidine blue and the areas of resorptive pits were analyzed under light microscope; the concentrations of C-telopeptide of type Ⅰ collagen CT(subscript x or Crosslaps in culture supernatants were measured by ELISA.

制备骨磨片,培养OC,并分别加入高中低浓度10^(-5、10^(-7)、10^(-9)mol/L的L-苏糖酸钙、L-苏糖酸钠、阿仑麟酸钠、17β-雌二醇、葡萄糖酸钙,实验设以上各浓度组及对照组(共16组,每组n=8),甲苯胺蓝染色一光镜观察分析骨片上骨吸收陷窝面积,ELISA测定上清液Ⅰ型胶原C-末端肽(CTx或Crosslaps)浓度。

The antiarrhythmic drug ibutilide fumarate was synthesized from aniline by methylsulfonylation, Friedel Crafts reaction, condensation, reduction and salification with an overall yield of 44%.

苯胺为起始原料,经甲磺酰化、傅克反应、缩合、还原和成盐反应等 5步合成了抗心律失常药富马酸伊布利特,总收率 4 4 %。

The results show that the electrical conductivity and the seebeck coefficient of PAn are strongly dependent on the preparation conditions and temperature.

结果表明,聚苯胺的电导率和塞贝克系数强烈依赖于制备条件和温度。

The polyaniline hybrid materials doped with cobalt substituted silicotungstate isomers α,β-Kβ(subscript 6-n)H[SiW11Co(H2O)O39]xH2O β(subscript i=β1,β2,β3 have been prepared.

以Keggin结构钴取代杂多硅钨酸盐异构体α,β-K(下标 6-n)H[SiW11Co(H2O)O39]xH2Oβ(下标 i=β1,β2,β3为掺杂剂,采用固相合成法制备了4种聚苯胺掺杂材料。

We suggested that a coordinate linkage should forms between the surface of skutterudite and a top of PAn chains based on the analysis of infrared spectra.

由复合材料红外光谱的蓝移及N-H红外振动模强度的变化提出了聚苯胺分子与方钴矿表面可能存在配位键的假设,很好地解释了实验中的现象。

Novel styryl derivatives with triphenylamine as donor and triazine as acceptor were synthesized. The two-photon absorption cross section for Ⅴ-1,Ⅴ-2 and Ⅴ-3 were determined to be 0.31×10〓cm〓/Gw, 0.365×10〓cm〓/Gw and 1. 64×10〓cm〓/Gw by femtosecond Z-san technology, respectively.

合成了以三苯胺为电子给体、三嗪为电子受体的新型二苯乙烯类化合物,用飞秒开口z-扫描测量化合物Ⅴ-1、Ⅴ-2和Ⅴ-3的双光子吸收截面分别为0.31×10〓cm〓/Gw、0.365×10〓cm〓/Gw和1.64×10〓cm〓/Gw。

Key words摘要: diazotizationcoupling reaction;resonance scattering spectra;nitrite;sulfanilic amide;N,Ndimethyl aniline

重氮化偶联反应;共振散射光谱;亚硝酸根;磺胺;N,N二甲基苯胺

The negatively charged sulfonic acid groups was readily introduced through the reaction of the terminal anhydride groups of the anhydride-terminated hyperbranched poly precursor with the amino groups of sulfanilic acid before chemical imidization.

研究表明,在聚合过程的聚酰胺酸阶段,采用过量的邻苯二甲酸酐或苯胺对超支化聚酰亚胺的端氨基或端酸酐基团进行的封端改性切实可行,改性反应可进行地相当彻底。

Synthesizc 2-methyl-5-acetamino benzene sulfochloride using p-toluidine primer reactant by aceylation and chlorosulfonation.

以对甲基苯胺为起始原料,通过乙酰化和氯磺化反应合成2-甲基-5-乙酰氨基苯磺酰氯。

But, to our knowledge, no systematic study with respect to the properties of doped polyaniline by sulfonic acid in magnetic field has yet been published.

但到目前为止,关于在磁场中用大分子酸掺杂聚苯胺的研究尚鲜见报道。

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